CN203329735U - Ion exchanging device for minitype laboratory - Google Patents
Ion exchanging device for minitype laboratory Download PDFInfo
- Publication number
- CN203329735U CN203329735U CN2013202530959U CN201320253095U CN203329735U CN 203329735 U CN203329735 U CN 203329735U CN 2013202530959 U CN2013202530959 U CN 2013202530959U CN 201320253095 U CN201320253095 U CN 201320253095U CN 203329735 U CN203329735 U CN 203329735U
- Authority
- CN
- China
- Prior art keywords
- glass
- ion exchange
- exchange column
- valve
- eluent
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
- 238000005342 ion exchange Methods 0.000 title claims abstract description 29
- 239000011521 glass Substances 0.000 claims abstract description 41
- 239000005338 frosted glass Substances 0.000 claims abstract 2
- 239000003480 eluent Substances 0.000 abstract description 18
- 239000000945 filler Substances 0.000 abstract description 5
- 238000004255 ion exchange chromatography Methods 0.000 abstract description 5
- 238000010828 elution Methods 0.000 abstract 1
- 238000012856 packing Methods 0.000 description 17
- 239000000463 material Substances 0.000 description 13
- 244000025254 Cannabis sativa Species 0.000 description 6
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 5
- 238000005259 measurement Methods 0.000 description 3
- 238000000034 method Methods 0.000 description 2
- 238000000746 purification Methods 0.000 description 2
- 238000004458 analytical method Methods 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 239000012472 biological sample Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000000605 extraction Methods 0.000 description 1
- 238000009434 installation Methods 0.000 description 1
- 125000003010 ionic group Chemical group 0.000 description 1
- 238000002955 isolation Methods 0.000 description 1
- 238000000926 separation method Methods 0.000 description 1
- 239000002699 waste material Substances 0.000 description 1
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- Treatment Of Liquids With Adsorbents In General (AREA)
Abstract
本实用新型公开一种小型实验室用离子交换装置，涉及离子交换层析技术领域。它由前端玻璃转子流量计通过带玻璃导管的磨砂口玻璃塞与上端带有磨砂口的玻璃离子交换柱相连组成。玻璃离子交换柱内设置刻度；同时在离子交换柱下端与玻璃阀门连接处设置砂芯。进行离子交换层析时，色谱填料装入离子交换柱通过交换柱刻度准确读出填料体积；洗脱液先经过玻璃转子流量计，用玻璃阀门控制流量时可通过转子流量计准确设置合适流速；交换柱下端的砂芯可以防止色谱填料由于洗脱速度快被冲入玻璃阀门导致阀门堵塞，防止洗脱液溢出。本实用新型的离子交换装置还可串联使用，使用方便，易于拆卸。
The utility model discloses a small-sized laboratory ion exchange device, which relates to the technical field of ion exchange chromatography. It consists of a glass rotameter at the front connected to a glass ion exchange column with a frosted opening on the upper end through a frosted glass plug with a glass conduit. A scale is set inside the glass ion exchange column; at the same time, a sand core is set at the connection between the lower end of the ion exchange column and the glass valve. When performing ion exchange chromatography, the chromatographic filler is loaded into the ion exchange column and the volume of the filler can be read accurately through the scale of the exchange column; the eluent first passes through the glass rotameter, and when the flow is controlled by a glass valve, the appropriate flow rate can be accurately set through the rotameter; The sand core at the lower end of the exchange column can prevent the chromatographic filler from being washed into the glass valve due to the fast elution speed, causing the valve to be blocked and preventing the eluent from overflowing. The ion exchange device of the utility model can also be used in series, which is convenient to use and easy to disassemble.
Description
Technical field
The utility model relates to a kind of ion interchange unit, relates to the ion-exchange chromatography field.
Background technology
The principle of ion-exchange chromatography is that charged biomolecule and the ionic group on chromatograph packing material exchange and realize separation and purification.Ion exchange technique is widely used in water treatment, the extraction of biological sample, purification isolation analysis.
At present, the use for laboratory small ion exchange column is mainly by a upper end open, and the glass column that lower end is connected to glass valve forms.Control the flow velocity of eluent in ion exchange process by the glass valve of pillar lower end.The calculating of flow velocity be mainly by manual measurement in the unit interval effluent volume by chromatograph packing material try to achieve.The height, the unit interval eluent that need to measure chromatograph packing material in pillar internal diameter, pillar flow out the indexs such as volume, and the flow velocity error calculated is larger.And because the cylinder lower end directly is connected with the glass valve of coutroi velocity, and the volume of chromatograph packing material is generally less than normal, in ion exchange process, often there is filler to stop up the situation of glass valve, cause exchange process blocked, even make eluent overflow.In addition, because most of chromatograph packing material has swellability, the chromatograph packing material volume of actual dress column volume and measurement has larger error, causes errors of analytical results to reach more greatly the filler waste.
Summary of the invention
In order to overcome existing small-size glass ion exchange column, eluent outflow speed can not accurately be set, easily cause glass valve to stop up, eluent overflows and deficiency that can not Accurate Determining chromatograph packing material volume, the utility model provides a kind of ion interchange unit, this small-size laboratory not only can accurately arrange eluent flow rate with ion interchange unit, effectively avoids glass valve to stop up, and can measure the volume of chromatograph packing material, and easy to use, be easy to dismounting.
The utility model solves the technical scheme that its technical problem adopts: by centre, the frosted mouth glass stopper with grass tube is connected with the front glass spinner flowmeter glass ion exchange column of upper end band frosted mouth.Eluent first enters ion exchange column through grass tube again by glass rotameter, and the flow of eluent is directly measured by glass rotameter.
In the utility model, described glass ion exchange column lower end, arrange one deck 3-4mm core with the glass valve junction, stops chromatograph packing material to enter glass valve, and eluent can pass through core simultaneously, effectively avoids stopping up, and prevents that eluent from overflowing.
In the utility model, described ion exchange column is designed to the scale glass column, and minimum scale is accurate to 0.5mL, thereby directly reads the chromatograph packing material volume of packing into.
The beneficial effects of the utility model are, can pass through glass rotameter Accurate Measurement eluent flow rate, by core, effectively prevent that glass valve from stopping up and eluent overflows, can directly accurately read the volume of chromatograph packing material after the ion exchange column of packing into, and simple in structure, for convenience detach.
The accompanying drawing explanation
The structural representation that accompanying drawing is ion interchange unit described in the utility model.
In figure, 1 ion exchange column with scale, 2, glass rotameter, 3, the middle frosted mouth glass stopper with grass tube, 4, the frosted mouth, 5, core, 6, water supply hose.
The specific embodiment
In accompanying drawing, ion exchange column (1) upper end with scale arranges frosted mouth (4), frosted mouth glass stopper (3) by centre with grass tube is connected with front glass spinner flowmeter (2), flowmeter (2) lower end connects water supply hose (6), simultaneously, 3-4mm core (5) is set between exchange column lower end and speed control valve door.
When ion interchange unit described in the utility model carries out ion-exchange chromatography, by ion exchange column upper end frosted mouth (4) chromatograph packing material of packing into, the happy packing volume of reality of dress post can directly be read by the scale on exchange column.Eluent enters glass rotameter by water supply hose, through grass tube, enters ion exchange column, and the eluent flow can, by the spinner flowmeter Accurate Determining, reduce error.Flow out ion exchange column through core after the eluent exchange finishes, core can effectively stop chromatograph packing material to stop up glass valve, prevents that eluent from overflowing.
Ion interchange unit described in the utility model also can use in several device series connection.Simultaneously, with the ion exchange column (1) of scale, the middle frosted mouth glass stopper (3) with grass tube, glass rotameter (2) and water supply hose (6) are all detachable, and easy for installation.
Claims (3)
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013202530959U CN203329735U (en) | 2013-04-25 | 2013-04-25 | Ion exchanging device for minitype laboratory |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2013202530959U CN203329735U (en) | 2013-04-25 | 2013-04-25 | Ion exchanging device for minitype laboratory |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203329735U true CN203329735U (en) | 2013-12-11 |
Family
ID=49698436
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2013202530959U Expired - Fee Related CN203329735U (en) | 2013-04-25 | 2013-04-25 | Ion exchanging device for minitype laboratory |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203329735U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106018574A (en) * | 2016-05-05 | 2016-10-12 | 同济大学 | Fractionation device for carrying out simple and rapid ion exchange on peptide or protein mixture |
| CN109655037A (en) * | 2019-02-27 | 2019-04-19 | 山东大学 | A kind of combination type sedimentation observation device and method |
-
2013
- 2013-04-25 CN CN2013202530959U patent/CN203329735U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN106018574A (en) * | 2016-05-05 | 2016-10-12 | 同济大学 | Fractionation device for carrying out simple and rapid ion exchange on peptide or protein mixture |
| CN109655037A (en) * | 2019-02-27 | 2019-04-19 | 山东大学 | A kind of combination type sedimentation observation device and method |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20131211 Termination date: 20160425 |