CN204237898U - A kind of Novel liquid-phase tack producing device - Google Patents

A kind of Novel liquid-phase tack producing device Download PDF

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Publication number
CN204237898U
CN204237898U CN201420699188.9U CN201420699188U CN204237898U CN 204237898 U CN204237898 U CN 204237898U CN 201420699188 U CN201420699188 U CN 201420699188U CN 204237898 U CN204237898 U CN 204237898U
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CN
China
Prior art keywords
liquid
phase
shaped body
conically shaped
phase tackifying
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201420699188.9U
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Chinese (zh)
Inventor
俞盛
毛启文
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
WUXI XINGSHENG NEW MATERIAL SCIENCE & TECHNOLOGY Co Ltd
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WUXI XINGSHENG NEW MATERIAL SCIENCE & TECHNOLOGY Co Ltd
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Priority to CN201420699188.9U priority Critical patent/CN204237898U/en
Application granted granted Critical
Publication of CN204237898U publication Critical patent/CN204237898U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

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Abstract

The utility model relates to a kind of Novel liquid-phase tack producing device, it comprises disk reactor, melt cooler and filter, described filter is connected with liquid-phase tackifying reactor top by pipeline, described liquid-phase tackifying reactor comprises up-narrow and down-wide barrel-type casing, charging aperture is provided with in described case top, bottom is provided with discharging opening, distributor is provided with above described enclosure interior, joint pin is provided with below described distributor, described joint pin is provided with liquid-phase tackifying conically shaped body that row are arranged with one heart from top to bottom, the arithmetic progression that the radius size of described liquid-phase tackifying conically shaped body is 50-80cm by tolerance from top to bottom successively increases, angle between the outer surface of described liquid-phase tackifying conically shaped body and connecting rod is 60 °, the vertical height of described each liquid-phase tackifying conically shaped body is between 10-15cm.The utility model vibrational power flow is reasonable, and greatly increase the contact area between liquid vapour, reaction speed is fast, promotes melt quality well.

Description

A kind of Novel liquid-phase tack producing device
Technical field
The utility model relates to a kind of tack producing device, is specifically related to a kind of liquid-phase tackifying device.
Background technology
Low sticky PBT melt is flowed out from the low sticky material outlet being provided with plunger valve control in the appropriate location of gathering bottom reactor at the final minification of PBT; through melt cooler cooling by after metre filter, then carry out thickening through the conveyance conduit of melt booster pump feeding heating agent jacket pipe protection to liquid-phase tackifying still.Existing liquid-phase tackifying still structure is single, and result of use is undesirable, does not meet actual operation requirements.
Summary of the invention
Goal of the invention: the purpose of this utility model is to overcome deficiency of the prior art, provides a kind of vibrational power flow reasonable, and greatly increase the contact area between liquid vapour, reaction speed is fast, promotes the Novel liquid-phase tack producing device of melt quality well.
Technical scheme: in order to solve the problems of the technologies described above, a kind of Novel liquid-phase tack producing device described in the utility model, it comprises disk reactor, melt cooler and filter, they connect successively according to the order of sequence, described filter is connected with liquid-phase tackifying reactor top by pipeline, described liquid-phase tackifying reactor comprises up-narrow and down-wide barrel-type casing, charging aperture is provided with in described case top, bottom is provided with discharging opening, distributor is provided with above described enclosure interior, joint pin is provided with below described distributor, described joint pin is provided with liquid-phase tackifying conically shaped body that row are arranged with one heart from top to bottom, the arithmetic progression that the radius size of described liquid-phase tackifying conically shaped body is 50-80cm by tolerance from top to bottom successively increases, angle between the outer surface of described liquid-phase tackifying conically shaped body and connecting rod is 60 °, the vertical height of described each liquid-phase tackifying conically shaped body is between 10-15cm.
Described liquid-phase tackifying conically shaped body is provided with 3 or 4.
Gap is provided with between described distributor and minimum liquid-phase tackifying conically shaped body.
The bottom surface of described housing is lower domatic bottom surface.
Pipeline between described filter and liquid-phase tackifying reactor is provided with melt booster pump.
The utility model is provided with the bullet of superposition cone cylindricality multilayer drop with one heart in housing, the low sticky melt of PBT enters from the top of housing and distributes, utilize self gravitation equably stably natural landing is downward gradually at leisure from the surface of bullet, form melt film, like this by the drop of each layer cone, guarantee to form the uniform continuous film of thickness.Simultaneously, the utilidor of heating agent chuck is set up online Viscosity Monitoring, the viscosity of the low sticky melt sending into thickening reactor is controlled between 0.5-0.6dl/g, the too high thermal degradation that can aggravate melt melt long distance delivery of viscosity, too low, the tackifying ability of liquid-phase tackifying reactor can be exceeded, after causing thickening, melt does not reach the target viscosities requirement needed for spinning, and this viscosity can carry out stability contorting by the low cohesive end speed of agitator and vacuum regulating disk reactor.For the thermal degradation of melt in course of conveying is dropped to minimum, through test, on-line temperature monitoring is set, to ensure that the melt conveying temperature in utilidor is strict controlled between 225-245 DEG C, specifically by regulating melt jacket pipe heat medium temperature and melt cooling actuator temperature to realize, and the vacuum of liquid-phase tackifying reactor and feed inlet and outlet material viscosity also realize " tandem " on DCS controls.Viscosity-increasing reactor interior reaction temperature is between 235-255 DEG C, and the time of staying, operating pressure was at 0.15-0.20Kpa between 0.5-1.3h.After thickening, flow out after monitoring from discharging opening, by gear pump, height is glued melt and send device for spinning spinning.
Beneficial effect: the utility model compared with prior art, its remarkable advantage is: the utility model vibrational power flow is reasonable, adopt the liquid-phase tackifying conically shaped body arranged with one heart, and the arithmetic progression that the radius size of liquid-phase tackifying conically shaped body is 50-80cm by tolerance from top to bottom successively increases, angle between the outer surface of described liquid-phase tackifying conically shaped body and connecting rod is 60 °, the vertical height of described each liquid-phase tackifying conically shaped body is between 10-15cm, considerably increase the contact area between liquid vapour like this, small molecule by-product can discharge reaction system fast, effectively accelerate reaction speed, shorten melt residence time, and ensure melt first in first out, make melt in reactor, obtain consistent reaction condition, improve the quality of melt well, set up online Viscosity Monitoring and on-line temperature monitoring, control accuracy can be improved further.
Accompanying drawing explanation
Fig. 1 is general frame schematic diagram of the present utility model;
Fig. 2 is the structural representation of the reactor of liquid-phase tackifying described in the utility model.
Detailed description of the invention
Below in conjunction with drawings and Examples, the utility model is further described.
As depicted in figs. 1 and 2, a kind of Novel liquid-phase tack producing device described in the utility model, it comprises disk reactor 1, melt cooler 2 and filter 3, they connect successively according to the order of sequence, described filter 3 is connected with liquid-phase tackifying reactor 4 top by pipeline, described liquid-phase tackifying reactor 4 comprises up-narrow and down-wide barrel-type casing 5, charging aperture 6 is provided with at described housing 5 top, bottom is provided with discharging opening 7, distributor 8 is provided with in described housing 5 inner upper, joint pin 9 is provided with below described distributor 8, described joint pin 9 is provided with liquid-phase tackifying conically shaped body 10 that row are arranged with one heart from top to bottom, the arithmetic progression that the radius size of described liquid-phase tackifying conically shaped body 10 is 50-80cm by tolerance from top to bottom successively increases, angle between the outer surface of described liquid-phase tackifying conically shaped body 10 and connecting rod 9 is 60 °, the vertical height of described each liquid-phase tackifying conically shaped body 10 is between 10-15cm, described liquid-phase tackifying conically shaped body 10 is provided with 3 or 4, gap is provided with between described distributor 8 and minimum liquid-phase tackifying conically shaped body 10, the bottom surface of described housing 5 is lower domatic bottom surface, pipeline between described filter 3 and liquid-phase tackifying reactor 4 is provided with melt booster pump 11.The utility model vibrational power flow is reasonable, adopt the liquid-phase tackifying conically shaped body arranged with one heart, and the arithmetic progression that the radius size of liquid-phase tackifying conically shaped body is 50-80cm by tolerance from top to bottom successively increases, angle between the outer surface of described liquid-phase tackifying conically shaped body and connecting rod is 60 °, the vertical height of described each liquid-phase tackifying conically shaped body is between 10-15cm, considerably increase the contact area between liquid vapour like this, small molecule by-product can discharge reaction system fast, effectively accelerate reaction speed, shorten melt residence time, and ensure melt first in first out, make melt in reactor, obtain consistent reaction condition, improve the quality of melt well, set up online Viscosity Monitoring and on-line temperature monitoring, control accuracy can be improved further.
The utility model provides a kind of thinking and method; the method and access of this technical scheme of specific implementation is a lot; the above is only preferred embodiment of the present utility model; should be understood that; for those skilled in the art, under the prerequisite not departing from the utility model principle, some improvements and modifications can also be made; these improvements and modifications also should be considered as protection domain of the present utility model, and all available prior art of each part not clear and definite in the present embodiment is realized.

Claims (5)

1. a Novel liquid-phase tack producing device, it comprises disk reactor (1), melt cooler (2) and filter (3), they connect successively according to the order of sequence, it is characterized in that: described filter (3) is connected with liquid-phase tackifying reactor (4) top by pipeline, described liquid-phase tackifying reactor (4) comprises up-narrow and down-wide barrel-type casing (5), charging aperture (6) is provided with at described housing (5) top, bottom is provided with discharging opening (7), distributor (8) is provided with in described housing (5) inner upper, joint pin (9) is provided with in described distributor (8) below, described joint pin (9) is provided with liquid-phase tackifying conically shaped body (10) that row are arranged with one heart from top to bottom, the arithmetic progression that the radius size of described liquid-phase tackifying conically shaped body (10) is 50-80cm by tolerance from top to bottom successively increases, angle between the outer surface of described liquid-phase tackifying conically shaped body (10) and connecting rod (9) is 60 °, the vertical height of described each liquid-phase tackifying conically shaped body (10) is between 10-15cm.
2. Novel liquid-phase tack producing device according to claim 1, is characterized in that: described liquid-phase tackifying conically shaped body (10) is provided with 3 or 4.
3. Novel liquid-phase tack producing device according to claim 1, is characterized in that: be provided with gap between described distributor (8) and minimum liquid-phase tackifying conically shaped body (10).
4. Novel liquid-phase tack producing device according to claim 1, is characterized in that: the bottom surface of described housing (5) is lower domatic bottom surface.
5. Novel liquid-phase tack producing device according to claim 1, is characterized in that: the pipeline between described filter (3) and liquid-phase tackifying reactor (4) is provided with melt booster pump (11).
CN201420699188.9U 2014-11-19 2014-11-19 A kind of Novel liquid-phase tack producing device Expired - Fee Related CN204237898U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420699188.9U CN204237898U (en) 2014-11-19 2014-11-19 A kind of Novel liquid-phase tack producing device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420699188.9U CN204237898U (en) 2014-11-19 2014-11-19 A kind of Novel liquid-phase tack producing device

Publications (1)

Publication Number Publication Date
CN204237898U true CN204237898U (en) 2015-04-01

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105111424A (en) * 2015-08-10 2015-12-02 中国纺织科学研究院 Device for producing high-viscosity melt
CN105671645A (en) * 2014-11-19 2016-06-15 无锡市兴盛新材料科技有限公司 Novel liquid-phase tackifying device

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105671645A (en) * 2014-11-19 2016-06-15 无锡市兴盛新材料科技有限公司 Novel liquid-phase tackifying device
CN105111424A (en) * 2015-08-10 2015-12-02 中国纺织科学研究院 Device for producing high-viscosity melt
CN105111424B (en) * 2015-08-10 2017-03-29 中国纺织科学研究院 A kind of high viscous melt process units

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20150401

Termination date: 20171119

CF01 Termination of patent right due to non-payment of annual fee