CN203790609U - Super-gravity separation device - Google Patents

Super-gravity separation device Download PDF

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Publication number
CN203790609U
CN203790609U CN201420122032.4U CN201420122032U CN203790609U CN 203790609 U CN203790609 U CN 203790609U CN 201420122032 U CN201420122032 U CN 201420122032U CN 203790609 U CN203790609 U CN 203790609U
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CN
China
Prior art keywords
liquid phase
distributor
hypergravity
mass transfer
separator according
Prior art date
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Expired - Fee Related
Application number
CN201420122032.4U
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Chinese (zh)
Inventor
马庆芬
刘方平
卢辉
何文晋
廖宇兰
陈致水
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Hainan University
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Hainan University
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Priority to CN201420122032.4U priority Critical patent/CN203790609U/en
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Publication of CN203790609U publication Critical patent/CN203790609U/en
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Abstract

The utility model relates to a super-gravity separation device. The super-gravity separation device is divided into an inner uniform liquid distributor and an outer gas-liquid mass transfer separation layer. The super-gravity separation device comprises an inner rotation shaft, an outer rotation shaft, a rotor, a static liquid phase distributor and a dynamic liquid phase distributor. A liquid phase inlet and outlet and a gas phase inlet and outlet are formed in a shell of a super-gravity two-phase mass transfer separation rotation bed. The super-gravity separation device has the advantages that the dynamic liquid phase distributor is matched with the static liquid phase distributor, so that liquid can be uniformly distributed in the rotor peripherally and axially, and the mass transfer efficiency is improved; by the structure with the inner rotation shaft and the outer rotation shaft, the requirement on different rotation speeds of the two rotation shafts is met while a transmission structure is simplified; the efficient mass transfer and separation of two phases are achieved, and the super-gravity separation device can be used in the processes of rectification, absorption and the like.

Description

A kind of hypergravity separator
Technical field
The utility model relates to high-gravity technology field, specifically, the present invention relates to a kind of hypergravity separator.
Background technology
Super gravity field technology is a disruptive technology of strengthening transmission and heterogeneous reaction process.In practical application, the method that realizes Elevated Gravity is to produce centrifugal force by rotation, and this slewing through particular design is called hypergravity machine or high-gravity rotating bed, also because its breakthrough advantage is described as " transistor of chemical industry ".But the liquid distribution trough that is applied at present the hypergravity swinging bed device in industry is for static or dynamically, within these two weeks, all cannot realize being uniformly distributed of liquid truly.And the high-gravity rotating bed of prior art can be divided into two large classes according to its rotor structure: individual layer is high-gravity rotating bed and multilayer is high-gravity rotating bed.The long revolving bed Chinese patent of individual layer hypergravity has material filling type CN 1059105A, CN 1062098A, CN1064338A, CN 2229833Y, anti-blocking material filling type CN 201529411U, disc-type CN2581060Y, deflector type CN 117488C, tubular type CN 1438067A; The high-gravity rotating bed Chinese patent of multilayer has deflector type CN 1686591A, concentric ring type CN 101234261A, donut multiple filling layers formula CN 101869776A, multistage atomizing formula CN 201108754Y, multistage absorption CN 202173801.
Existing revolving bed mostly is stationary cloth liquid mode, and be about to liquid distribution trough and be connected with casing or other fixed support, feed tube transfixion, liquid sprays to rotor inner peripheral surface by the pressure of pump by the spray hole on liquid distribution trough liquid distributor.For example, in US Patent No. 4382900 and Chinese patent CN 1507940A, by pump, liquid is sent in pipe, by spray hole, sprayed to ring packing inner peripheral surface.
Chinese patent CN 101254355A and CN 1116125A disclose a kind of liquid distribution trough of rotational distribution form, its rotating shaft is hollow-core construction and is furnished with fluid aperture, liquid enters hollow shaft by feed tube, liquid in rotating shaft rotates with rotating shaft, under the effect of centrifugal force, by the hole in rotating shaft, send into packing layer.This liquid distribution trough is due to the restriction of rotating shaft radius, and the centrifugal force that liquid is subject in hollow shaft is little, and liquid handling amount is little.
Chinese patent CN 1060415A has proposed the rotation cloth liquid type revolving bed device that liquid distribution trough is fixedly connected with rotor or epitrochanterian parts, the centrifugal force distribution liquid producing by rotation, improved fluid flow opereating specification, but need movable sealing structure between liquid distribution trough and liquid phase inlet tube, structure of distributor is complicated, fabrication and installation trouble.
In Chinese patent CN 201752587U, liquid distribution trough is the multi-layer cylinder formula structure being fixed on rotor, be connected by the hollow feed well of stationary cylindrical shape being fixed on housing with liquid-inlet, by set fluid hole on the inwall of feed well and the inwall of every one deck cylinder, reach the atomization of liquid and initial distribution.Although this liquid distribution trough has been avoided the movable sealing structure between liquid distribution trough and feed pipe, be easy to manufacture and install, when fluid flow is larger, can cause liquid distribution trough flow resistance larger, atomization of liquid effect weakens.
Utility model content
The purpose of this utility model is to inherit the high-gravity rotating bed advantage of prior art, expand high-gravity rotating bed function, a kind of hypergravity two-phase mass transfer separating rotary rotated bed with quiet moving convolution liquid phase uniform device is provided, thereby by being uniformly distributed of liquid phase improved to mass-transfer efficiency.
In order to realize the purpose of this utility model, the utility model provides a kind of hypergravity two-phase mass transfer separating rotary rotated bed, comprising:
The housing of hypergravity two-phase mass transfer separating rotary rotated bed;
Outer shaft, arranges mechanical seal between described outer shaft and described housing;
Rotor, described rotor is arranged on described outer shaft, and within being positioned at described hypergravity two-phase contact mass transfer section, described rotor and between described housing, mechanical seal is set;
Interior rotating shaft, arranges mechanical seal between described interior rotating shaft and described rotor;
The liquid phase inlet tube and the gas phase outlet that are arranged on described housing top, described liquid phase inlet tube is fixed on described gaseous phase outlet pipe;
Static liquid phase distributor, described static liquid phase distributor is arranged on described liquid phase inlet tube, on described static liquid phase distributor, flow-guiding structure is set;
Dynamic liquid phase distributor, described dynamic liquid phase distributor is arranged in described interior rotating shaft, forms liquid phase uniform device with described static liquid phase distributor;
Be arranged on the gas phase inlet tube on described housing;
Be arranged on the liquid-phase outlet pipe on described housing;
Between described gaseous phase outlet pipe and described housing, arrange and be rotationally connected.
Preferably, described hypergravity two-phase contact mass transfer section is cylindric.
Preferably, the distance between two clamping plate of described rotor is 6mm~5000mm, and internal diameter is 12mm~3000mm, and external diameter is 16mm~6000mm.
Preferably, described static liquid phase distributor cylinder number is 2~100, and maximum drum diameter is 4~1000mm.
Preferably, the flow-guiding structure external diameter of described static liquid phase distributor is 8mm~1400mm.Thickness is 0.5mm~20mm.
Preferably, described flow-guiding structure quantity equates with described static liquid phase distributor cylinder quantity.
Preferably, the S type that is shaped as of described dynamic liquid phase distributor, streamlined or plate shape, the quantity of the guide vane having is 2~12, and internal diameter is than the large 1mm~3mm of the internal diameter of described static liquid phase distributor, and external diameter is 10mm~2000mm.
Preferably, described interior rotating shaft is multidiameter, optical axis or hollow shaft, and diameter is 4mm~100mm, and length is 20mm~2000mm.
Preferably, described outer shaft is multidiameter or hollow shaft, and internal diameter is than the large 1~5mm of described interior rotating shaft, and external diameter is 24mm~160mm.
Preferably, in described flow-guiding structure, be full of silicone oil or other thermal sensitivity fluid media (medium).
Hypergravity three-phase mass transfer separating rotary rotated bed described in the utility model has following advantages: in the time of 1,, realize the efficient mass transfer of two-phase with separated, can be applicable to the multiple unit processes such as rectifying, absorption; The liquid distribution method of 2, being association of activity and inertia makes liquid distribution realize homogenising, can make mass transfer separative efficiency greatly improve; 3, exterior and interior axle sleeves has even met speed discrepancy requirement, simplifies the structure simultaneously.
Accompanying drawing explanation
Fig. 1 is the structural representation of hypergravity two-phase mass transfer separating rotary rotated bed of the present utility model;
Fig. 2 is a kind of structural representation of the static liquid phase distributor of hypergravity two-phase mass transfer separating rotary rotated bed of the present utility model;
Fig. 3 is a kind of structural representation of the static liquid phase distributor of hypergravity two-phase mass transfer separating rotary rotated bed of the present utility model
Fig. 4 is a kind of structural representation of the dynamic liquid phase distributor of hypergravity two-phase mass transfer separating rotary rotated bed of the present utility model;
Fig. 5 is a kind of structural representation of the dynamic liquid phase distributor of hypergravity two-phase mass transfer separating rotary rotated bed of the present utility model;
In figure: 1, housing; 2, rotor; 3, hypergravity two-phase contact mass transfer section; 4, gas phase inlet tube; 5, interior rotating shaft; 6, outer shaft; 7, mechanical seal; 8, dynamic liquid phase distributor; 9, static liquid phase distributor; 10, gaseous phase outlet pipe; 11, liquid phase inlet tube; 12, liquid-phase outlet pipe; 13, mechanical seal; 14, mechanical seal; 15, deflector.
The specific embodiment
Following examples are used for illustrating the utility model, but are not used for limiting scope of the present utility model.
Fig. 1 schematically shows hypergravity two-phase mass transfer separating rotary rotated bed of the present utility model, comprising: the housing 1 of hypergravity two-phase mass transfer separating rotary rotated bed; Outer shaft 6, arranges mechanical seal 7 between described outer shaft 6 and described housing 1; Rotor 2, described rotor 2 is arranged on described outer shaft 6, and within being positioned at described hypergravity two-phase contact mass transfer section 3, described rotor 2 and between described housing 1, mechanical seal 14 is set; Interior rotating shaft 5, arranges mechanical seal 13 between described interior rotating shaft 5 and described rotor 2; Be arranged on liquid phase inlet tube 11 and the gas phase outlet 10 of described housing 1 top, described liquid phase inlet tube 11 is fixed on described gaseous phase outlet pipe 10; Static liquid phase distributor 9, described static liquid phase distributor 9 is arranged on described liquid phase inlet tube 11, on described static liquid phase distributor 9, flow-guiding structure 15 is set; Dynamic liquid phase distributor 8, described dynamic liquid phase distributor 8 is arranged in described interior rotating shaft 5, forms liquid phase uniform devices with described static liquid phase distributor 9; Be arranged on the gas phase inlet tube 4 on described housing 1; Be arranged on the liquid-phase outlet pipe 12 on described housing 1; Between described gaseous phase outlet pipe 10 and described housing 1, arrange and be rotationally connected.
Described hypergravity two-phase contact mass transfer section 3 is cylindric.Distance between two clamping plate of described rotor 2 is 500mm, and internal diameter is 100mm, and external diameter is 600mm.Described static liquid phase distributor 9 cylinder numbers are 5, and maximum drum diameter is 40mm.Flow-guiding structure 15 external diameters of described static liquid phase distributor 9 are 60mm.Thickness is 2mm.Described flow-guiding structure 15 quantity equate with described static liquid phase distributor 9 cylinder quantity.The S type that is shaped as of described dynamic liquid phase distributor 8, streamlined or plate shape, the quantity of the guide vane having is 6, and internal diameter is than the large 1mm of the internal diameter of described static liquid phase distributor 9, and external diameter is 90mm.Described interior rotating shaft 5 is multidiameter, optical axis or hollow shaft, and diameter is 40mm, and length is 200mm.Described outer shaft 6 is multidiameter or hollow shaft, and internal diameter is than the large 2mm of described interior rotating shaft 5, and external diameter is 80mm.In described flow-guiding structure 15, be full of silicone oil.
When using hypergravity two-phase mass transfer separating rotary rotated bed, gas or enter hypergravity two-phase contact mass transfer section 3 from gas phase inlet tube 4 with the gas of solid particle polluter, outer shaft 6 rotor drivens 2 rotate.Liquid enters static liquid phase distributor 9 from liquid phase inlet tube 11, through the liquid distributing for the first time, enter again dynamic liquid phase distributor 8 and realize being uniformly distributed of liquid, equally distributed liquid is got rid of at a high speed meets into hypergravity two-phase contact mass transfer section 3 and gas that to realize two-phase contact mass transfer separated, gas after mass transfer is discharged from gaseous phase outlet pipe, and the liquid after mass transfer flows out from liquid-phase outlet.

Claims (10)

1. a hypergravity separator, is characterized in that, comprising:
The housing (1) of hypergravity two-phase mass transfer separating rotary rotated bed;
Outer shaft (6), arranges mechanical seal (7) between described outer shaft (6) and described housing (1);
Rotor (2), described rotor (2) is arranged on described outer shaft (6), and within being positioned at described hypergravity two-phase contact mass transfer section (3), described rotor (2) and be positioned at mechanical seal (14) is set between described housing (1);
Interior rotating shaft (5), arranges mechanical seal (13) between described interior rotating shaft (5) and described rotor (2);
The liquid phase inlet tube (11) and the gas phase outlet (10) that are arranged on described housing (1) top, described liquid phase inlet tube (11) is fixed on described gaseous phase outlet pipe (10);
Static liquid phase distributor (9), it is upper that described static liquid phase distributor (9) is arranged at described liquid phase inlet tube (11), and flow-guiding structure (15) is set on described static liquid phase distributor (9);
Dynamic liquid phase distributor (8), it is upper that described dynamic liquid phase distributor (8) is arranged at described interior rotating shaft (5), forms liquid phase uniform device with described static liquid phase distributor (9);
Be arranged on the gas phase inlet tube (4) on described housing (1);
Be arranged on the liquid-phase outlet pipe (12) on described housing (1);
Between described gaseous phase outlet pipe (10) and described housing (1), arrange and be rotationally connected.
2. hypergravity separator according to claim 1, is characterized in that, described hypergravity two-phase contact mass transfer section (3) is cylindric.
3. hypergravity separator according to claim 1, is characterized in that, the distance between two clamping plate of described rotor (2) is 6mm~5000mm, and internal diameter is 12mm~3000mm, and external diameter is 16mm~6000mm.
4. hypergravity separator according to claim 1, is characterized in that, described static liquid phase distributor (9) cylinder number is 2~100, and maximum drum diameter is 4~1000mm.
5. hypergravity separator according to claim 4, is characterized in that, flow-guiding structure (15) external diameter of described static liquid phase distributor (9) is 8mm~1400mm, and thickness is 0.5mm~20mm.
6. hypergravity separator according to claim 5, is characterized in that, described flow-guiding structure (15) quantity equates with described static liquid phase distributor (9) cylinder quantity.
7. hypergravity separator according to claim 1, it is characterized in that, the S type that is shaped as of described dynamic liquid phase distributor (8), streamlined or plate shape, the quantity of the guide vane having is 2~12, internal diameter is than the large 1mm~3mm of internal diameter of described static liquid phase distributor (9), and external diameter is 10mm~2000mm.
8. hypergravity separator according to claim 1, is characterized in that, described interior rotating shaft (5) is multidiameter, optical axis or hollow shaft, and diameter is 4mm~100mm, and length is 20mm~2000mm.
9. hypergravity separator according to claim 1, is characterized in that, described outer shaft (6) is multidiameter or hollow shaft, and internal diameter is than the large 1~5mm of described interior rotating shaft (5), and external diameter is 24mm~160mm.
10. hypergravity separator according to claim 1, is characterized in that, is full of silicone oil or other thermal sensitivity fluid media (medium) in described flow-guiding structure (15).
CN201420122032.4U 2014-03-18 2014-03-18 Super-gravity separation device Expired - Fee Related CN203790609U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201420122032.4U CN203790609U (en) 2014-03-18 2014-03-18 Super-gravity separation device

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201420122032.4U CN203790609U (en) 2014-03-18 2014-03-18 Super-gravity separation device

Publications (1)

Publication Number Publication Date
CN203790609U true CN203790609U (en) 2014-08-27

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Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104436737A (en) * 2014-12-09 2015-03-25 温州创兴化工设备有限公司 Efficient rotation rectifier
CN114749001A (en) * 2022-03-22 2022-07-15 四川蜀兴鸿阳环保科技有限公司 Oil storage reservoir hypergravity absorbs adsorbs oil gas processing apparatus
CN114849266A (en) * 2022-05-07 2022-08-05 浙江镇田机械有限公司 Hypergravity centrifugal separator capable of improving separation efficiency

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN104436737A (en) * 2014-12-09 2015-03-25 温州创兴化工设备有限公司 Efficient rotation rectifier
CN114749001A (en) * 2022-03-22 2022-07-15 四川蜀兴鸿阳环保科技有限公司 Oil storage reservoir hypergravity absorbs adsorbs oil gas processing apparatus
CN114849266A (en) * 2022-05-07 2022-08-05 浙江镇田机械有限公司 Hypergravity centrifugal separator capable of improving separation efficiency

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20140827

Termination date: 20160318