CN203663799U - High-pressure reaction kettle - Google Patents
High-pressure reaction kettle Download PDFInfo
- Publication number
- CN203663799U CN203663799U CN201320884195.1U CN201320884195U CN203663799U CN 203663799 U CN203663799 U CN 203663799U CN 201320884195 U CN201320884195 U CN 201320884195U CN 203663799 U CN203663799 U CN 203663799U
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- kettle
- kettle body
- magnetic stirring
- stirring apparatus
- water pipe
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- Mixers With Rotating Receptacles And Mixers With Vibration Mechanisms (AREA)
Abstract
The utility model relates to a high-pressure reaction kettle which comprises a kettle body and a kettle cover, wherein a U-shaped liquid-phase pipe is arranged in the kettle body; a liquid-phase valve is arranged at the upper end of the liquid-phase pipe; a thermocouple is arranged at the upper part of the kettle body; a magnetic stirrer is arranged above the kettle body; a stirrer is connected to the bottom end of the magnetic stirrer; a cold water pipe is wound on the stirrer; the stirrer is arranged in the kettle body; a temperature measurement sleeve pipe is arranged in the kettle body; the magnetic stirrer is connected with a servomotor through a triangular belt; a heating furnace is arranged outside the kettle body, covered with a heat preservation layer and connected with a connector socket. According to the reaction kettle, the reaction kettle body is cooled through the cold water pipe wound on the stirrer, so that the uncontrollable risk of the temperature rise is lowered and the side reaction due to over-high temperature is inhibited.
Description
Technical field
The utility model relates to reactor, and being specifically related to one can homogeneous heating, can't be to the autoclave of environment.
Background technology
Reactor is the key reaction mixing plant in Chemical Manufacture, major function be make that material stirring mixes, chemical reaction, dissolving, crystallization, heat transfer, cooling etc.
In chemical industry, autoclave is commonly used to produce industrial chemicals, is widely used, and traditional reactor heating is inhomogeneous, temperature in reaction kettle body is unable to find out, and temperature is uncontrollable, reacts abnormally dangerous, therefore in heating process, can not continue to heat, with prevent exploding.
Summary of the invention
The purpose of this utility model is in order to overcome above-mentioned defect, and a kind of homogeneous heating is provided, and improves the efficiency that reaction occurs, and explosion-proof performance is good, temperature in reaction kettle body is controlled, the autoclave that security is good.
For achieving the above object, a kind of autoclave of the utility model design, comprise kettle and kettle cover, in described kettle, be provided with U-shaped liquid-phase tube, the upper end of liquid-phase tube is provided with liquid phase valve, described kettle top is provided with thermocouple, described kettle top is provided with magnetic stirring apparatus, the bottom of described magnetic stirring apparatus is connected with agitator, on described agitator, be wound with cold water pipe and be positioned at kettle, in described kettle, be provided with temperature-measuring casing, described magnetic stirring apparatus is connected with servomotor by V belt, described kettle is provided with heating furnace outward, described heating furnace is coated with one layer of heat preservation layer outward, described heating furnace is connected with connector socket.
In technique scheme, the middle part of described magnetic stirring apparatus is arranged with cooling water pipe, and described cooling water pipe is connected with cooling water source.
In technique scheme, the top of described magnetic stirring apparatus is provided with velometer.
In technique scheme, described kettle top is connected with Pressure gauge.
In technique scheme, described kettle top is provided with blasting piece device.
Reaction kettle body of the present utility model top is provided with thermocouple, temperature in can Real-Time Monitoring reaction kettle body, on agitator, be wound with cold water pipe and be positioned at kettle, in the time that the temperature in reaction kettle body exceedes controlled boundary, connect cooling water source, by the cold water pipe being wound around on agitator, reaction kettle body is lowered the temperature, reduce the uncontrollable danger of temperature rise, also suppressed the side reaction producing because of excess Temperature.The utility model is connected with Pressure gauge and blasting piece device on kettle top, can be by the force value in pressure apparatus Real Time Observation reaction kettle body, blasting piece device can effectively prevent that reaction kettle body pressure value beyond the mark from blasting, and has increased the security of reaction kettle body.
Brief description of the drawings
Fig. 1 is section of the present utility model (partly cuing open) structural representation;
In figure: 1-kettle; 2-magnetic stirring apparatus; 3-cooling water pipe; 4-Pressure gauge; 5-thermocouple; 6-blasting piece device; 7-cold water pipe; 8-temperature-measuring casing; 9-agitator; 10-connector socket; 11-liquid-phase tube; 12-heat-insulation layer, 13-heating furnace; 14-velometer; 15-flange; 16-liquid phase valve; 17-kettle cover; 18-bolt; 19-V belt; 20-servomotor.
Detailed description of the invention
Below in conjunction with the drawings and specific embodiments, the utility model is described in further detail:
Autoclave as shown in Figure 1, comprise kettle 1 and kettle cover 17, between kettle cover 17 and kettle 1, be connected by flange 15, and fixedly secure by bolt 18, kettle cover 17 is provided with feed pipe, in kettle 1, be provided with U-shaped liquid-phase tube 11, the upper end of liquid-phase tube 11 is provided with liquid phase valve 16, kettle 1 top is provided with thermocouple 5, kettle 1 top is provided with magnetic stirring apparatus 2, the bottom of magnetic stirring apparatus 2 is connected with agitator 9, on agitator 9, be wound with cold water pipe 7 and be positioned at kettle 1, in kettle 1, be provided with temperature-measuring casing 8, magnetic stirring apparatus 2 is connected with servomotor 20 by V belt 19, the outer heating furnace 13 that is provided with of kettle 1, the outer one layer of heat preservation layer 12 that is coated with of heating furnace 13, play the effect of insulation, evenly preheating reaction kettle body, also guaranteed to heat evenly, heating furnace 13 is connected with connector socket 10.
The middle part of magnetic stirring apparatus 2 is arranged with cooling water pipe 3, and cooling water pipe 3 is connected with cooling water source.The top of magnetic stirring apparatus 2 is provided with velometer 14.Kettle 1 top is connected with Pressure gauge 4.Kettle 1 top is provided with blasting piece device 6.
When use, reaction liquid enters in kettle 1 from feed pipe, by heating furnace 13, kettle 1 is heated, start servomotor 20, magnetic stirring apparatus 2 is worked simultaneously, drives agitator 9 Stirrings, the thermocouple 5 on kettle 1 top is measured the temperature in kettle 1 chamber, Pressure gauge 4 is measured the pressure in kettle 1 chamber, and blasting piece device 6 is blast protection in advance, when magnetic stirring apparatus 2 cooling water pipe 3 when overweight that generates heat cools to magnetic stirring apparatus 2.Temperature-measuring casing 8 in kettle 1 is measured the temperature of reactant in kettle 1 chamber, when temperature, opens cooling water water source and by cold water pipe 7, reactant in kettle 1 chamber is lowered the temperature higher than cut-off when temperature, reacts safe and reliable.
The content not being described in detail in this description belongs to the known prior art of professional and technical personnel in the field.
Claims (5)
1. an autoclave, comprise kettle (1) and kettle cover (17), it is characterized in that: in described kettle (1), be provided with U-shaped liquid-phase tube (11), the upper end of liquid-phase tube (11) is provided with liquid phase valve (16), kettle (1) top is provided with thermocouple (5), described kettle (1) top is provided with magnetic stirring apparatus (2), the bottom of described magnetic stirring apparatus (2) is connected with agitator (9), on described agitator (9), be wound with cold water pipe (7) and be positioned at kettle (1), in described kettle (1), be provided with temperature-measuring casing (8), described magnetic stirring apparatus (2) is connected with servomotor (20) by V belt (19), the outer heating furnace (13) that is provided with of described kettle (1), the outer one layer of heat preservation layer (12) that is coated with of described heating furnace (13), described heating furnace (13) is connected with connector socket (10).
2. autoclave according to claim 1, is characterized in that: the middle part of described magnetic stirring apparatus (2) is arranged with cooling water pipe (3), and described cooling water pipe (3) is connected with cooling water source.
3. autoclave according to claim 1 and 2, is characterized in that: the top of described magnetic stirring apparatus (2) is provided with velometer (14).
4. autoclave according to claim 1 and 2, is characterized in that: described kettle (1) top is connected with Pressure gauge (4).
5. autoclave according to claim 1 and 2, is characterized in that: described kettle (1) top is provided with blasting piece device (6).
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320884195.1U CN203663799U (en) | 2013-12-31 | 2013-12-31 | High-pressure reaction kettle |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201320884195.1U CN203663799U (en) | 2013-12-31 | 2013-12-31 | High-pressure reaction kettle |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203663799U true CN203663799U (en) | 2014-06-25 |
Family
ID=50960134
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201320884195.1U Expired - Fee Related CN203663799U (en) | 2013-12-31 | 2013-12-31 | High-pressure reaction kettle |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203663799U (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104048869A (en) * | 2014-07-03 | 2014-09-17 | 中国海洋石油总公司 | High-temperature, high-pressure and high-speed agitator |
| CN104741041A (en) * | 2014-07-10 | 2015-07-01 | 季永东 | High-pressure reactor |
| CN107446617A (en) * | 2016-10-27 | 2017-12-08 | 王延睿 | A kind of analogue experiment installation |
| CN111715146A (en) * | 2020-03-31 | 2020-09-29 | 同济大学 | Solid-liquid dual-purpose high-temperature high-pressure carbonization reaction kettle capable of indicating carbonization degree |
-
2013
- 2013-12-31 CN CN201320884195.1U patent/CN203663799U/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104048869A (en) * | 2014-07-03 | 2014-09-17 | 中国海洋石油总公司 | High-temperature, high-pressure and high-speed agitator |
| CN104741041A (en) * | 2014-07-10 | 2015-07-01 | 季永东 | High-pressure reactor |
| CN107446617A (en) * | 2016-10-27 | 2017-12-08 | 王延睿 | A kind of analogue experiment installation |
| CN107557056A (en) * | 2016-10-27 | 2018-01-09 | 王延睿 | A kind of analogue experiment installation |
| CN107557056B (en) * | 2016-10-27 | 2019-06-25 | 江苏华安科研仪器有限公司 | A kind of imitative experimental appliance |
| CN111715146A (en) * | 2020-03-31 | 2020-09-29 | 同济大学 | Solid-liquid dual-purpose high-temperature high-pressure carbonization reaction kettle capable of indicating carbonization degree |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20140625 Termination date: 20151231 |
|
| EXPY | Termination of patent right or utility model |