CN203593712U - Chlorophyll metal salt preparation equipment - Google Patents

Chlorophyll metal salt preparation equipment Download PDF

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Publication number
CN203593712U
CN203593712U CN201320804210.7U CN201320804210U CN203593712U CN 203593712 U CN203593712 U CN 203593712U CN 201320804210 U CN201320804210 U CN 201320804210U CN 203593712 U CN203593712 U CN 203593712U
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China
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tank
lass lining
chlorophyll
reaction tank
pipeline
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CN201320804210.7U
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张云健
王大鹏
张世果
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WEIFANG HANXING CHLOROPHYLL Co Ltd
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WEIFANG HANXING CHLOROPHYLL Co Ltd
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Abstract

The utility model belongs to the technical field of chlorophyll metal salt production equipment and discloses chlorophyll metal salt preparation equipment. The equipment comprises a silkworm feces softening device, a silkworm feces soaking device, a silkworm feces soaking solution concentrating device, a chlorophyll liquid concentrating device, a chlorophyll dissolving and gelatinizing device, a chlorophyll saponification device, a chlorophyll metalizing device, a chlorophyll acidulating device, a chlorophyll salifying device and a chlorophyll metal salt drying device, which are sequentially arranged. During the process of extracting chlorophyll by using the silkworm feces, acetone and water are respectively recovered in the vacuum environment, the concentration time is shortened and the concentration efficiency is improved; the process of using the extracted chlorophyll to prepare chlorophyll metal salt comprises the steps of dissolving and gelatinizing, saponification, metalizing, acidification, salifying and the like, a step of removing purities via repeated separation is provided, and the obtained chlorophyll metal salt contains fewer purities.

Description

Chlorophyll metal-salt Preparation equipment
Technical field
The utility model belongs to chlorophyll metal-salt production unit technical field, relates in particular to a kind of chlorophyll metal-salt Preparation equipment.
Background technology
Chlorophyll metal sodium salt is the natural pigment forming through retrofit take chlorophyll as substrate, is a kind of natural food colour that Food and Argriculture OrganizationFAO, the World Health Organization and the approval of foodstuff additive standard committee of China are used.Chlorophyll is extensively present in all green plantss, chlorophyll metal sodium salt is compared tone, the strong coloring force not only with natural green plant with chlorophyll, and its stability is better, in addition, chlorophyll metal sodium salt is with the nutritive element that in itself distinctive constructional feature and derivative, institute huge legendary turtle is closed, painted to needs and improve or keep natural green food color, improve in the use value of food own and there is advantageous advantage.Moreover, chlorophyll metal sodium salt has become the popular medicine of anti-gene poison class in the world, is widely used in pharmaceutical industries, and leaf green metal sodium salt is also used to the daily-use chemical industry such as toothpaste and makeup industry and carries out painted.
The existing comparison in equipment that is used for processing chlorophyll metal-salt is simple and crude, and labor strength is large, extracts that concentrated speed is slow, the time is long, efficiency is low, and chlorophyll metal-salt foreign matter content that it makes is high, product yield is low.
Utility model content
Technical problem to be solved in the utility model is: a kind of chlorophyll metal-salt Preparation equipment is provided, so that solution is slow by the concentrated speed of existing installation processing chlorophyll metal-salt extraction, the time is long, efficiency is low, the high technical problem of chlorophyll metal-salt foreign matter content making.
For solving the problems of the technologies described above, the technical solution of the utility model is:
Chlorophyll metal-salt Preparation equipment, comprise the silkworm excrement softening installation, silkworm excrement infuser device, silkworm excrement soak solution concentrating unit, chlorophyl liquid concentrating unit, the molten paste device of chlorophyll, chlorophyll device for saponifying, chlorophyll metal device, chlorophyllin gasifying device, chlorophyll salify device and the chlorophyll metal-salt drying installation that set gradually
Described silkworm excrement softening installation comprises the first conveying belt being driven by power set, one end of described the first conveying belt is provided with hopper, described the first conveying belt is provided with vibratory screening apparatus away from one end of described hopper, described vibratory screening apparatus is provided with stirrer away from one end of described the first conveying belt, on described stirrer, be also provided with inlet channel, the bottom of described vibratory screening apparatus is provided with dust receiving tank, and described dust receiving tank connects induced draft fan;
Described silkworm excrement infuser device comprises the lift that is arranged on stirrer downstream, described lift is arranged on one end of feed pipe, on described feed pipe, be set up in parallel several steeping tanks, in all described steeping tanks, be provided with first heater, the top of described steeping tank is provided with acetone pipeline and material inlet valve, described feed pipe is positioned at the top of described material inlet valve, described material inlet valve is by reinforced hose connection feed pipe, described reinforced flexible pipe one end is fixedly mounted on described feed pipe, the opening for feed of the other end and described material inlet valve is suitable, the bottom of described steeping tank is provided with vent valves, below one side position of described vent valves is provided with the second conveying belt being driven by power set, all described vent valves are all towards described the second conveying belt, the end of described the second conveying belt is provided with waste residue storage pool,
Described silkworm excrement soak solution concentrating unit comprises and the temporary tank of the tank connected soak solution of described immersion, the temporary tank of described soak solution connects lass lining recover acetone retort, described lass lining recover acetone retort connects separating tank, the top of described lass lining recover acetone retort connects the first spiral-plate heat exchanger, described the first spiral-plate heat exchanger connects the temporary tank of acetone, on the top of described lass lining recover acetone retort, be also provided with the first vacuum pump, in described lass lining recover acetone retort, be provided with secondary heating mechanism;
Described chlorophyl liquid concentrating unit comprises thickening filtration pond and lass lining concentration response tank, described thickening filtration pond is positioned at the below of described separating tank, described thickening filtration is provided with filtering layer in pond, the top of described lass lining concentration response tank is provided with suction pipeline, the end of described suction pipeline is positioned at described thickening filtration pond and is positioned at the top of described filtering layer, the top of described lass lining concentration response tank connects secondary spiral lamina interchanger, described secondary spiral lamina interchanger connects the temporary tank of yellow water, the top of described lass lining concentration response tank is also provided with the second vacuum pump, in described lass lining concentration response tank, be provided with the 3rd heating unit,
The molten paste device of described chlorophyll comprises and the molten paste retort of the tank connected lass lining of described lass lining concentration response, the molten paste retort of described lass lining connects molten paste separating tank, the top of the molten paste retort of described lass lining is provided with alcohol pipeline, the top of the molten paste retort of described lass lining is also connected with the 3rd vacuum pump, the inside of the molten paste retort of described lass lining is provided with the 4th heating unit, in the molten paste retort of described lass lining, is also provided with the first whipping appts;
Described chlorophyll device for saponifying comprises and separates tank connected lass lining saponification reaction tank with described molten paste, described lass lining saponification reaction tank connects saponification liquor separating tank, described saponification liquor separating tank connects the temporary tank of saponification liquor, between described molten paste separating tank and lass lining saponification reaction tank, be provided with first branch that is used for separating alcohol, described the first branch comprises that alcohol keeps in tank, between the temporary tank of described saponification liquor separating tank and saponification liquor, be provided with second branch that is used for separating gasoline, described the second branch comprises that gasoline keeps in tank, the top of described lass lining saponification reaction tank is provided with liquid caustic soda pipeline, gasoline pipeline and alcohol pipeline, the inside of described lass lining saponification reaction tank is provided with the 5th heating unit, on described lass lining saponification reaction tank, be also provided with the second whipping appts,
Described chlorophyll metal device comprises that keeping in tank with described saponification liquor is connected lass lining metallization reaction tank, described lass lining metallization reaction tank connection metal separating tank, the top of described lass lining metallization reaction tank is provided with metal-salt pipeline, in described lass lining metallization reaction tank, be provided with the 6th heating unit, on described lass lining metallization reaction tank, be also provided with the 3rd whipping appts;
Described chlorophyllin gasifying device comprises and separates tank connected lass lining acidification reaction tank with described metallization, between described metallization separating tank and lass lining acidification reaction tank, be provided with the 3rd branch that is used for separating impurity, described the 3rd branch comprises that impurity keeps in tank, the top of described lass lining acidification reaction tank is provided with acid adding pipeline, the inside of described lass lining acidification reaction tank is provided with the 7th heating unit, on described lass lining acidification reaction tank, is also provided with the 4th whipping appts;
Described chlorophyll salify device comprises and the tank connected lass lining salt-forming reaction of described lass lining acidification reaction tank, described lass lining salt-forming reaction tank is provided with liquid caustic soda pipeline, the inside of described lass lining salt-forming reaction tank is provided with the 8th heating unit, on described lass lining salt-forming reaction tank, is also provided with the 5th whipping appts;
Described chlorophyll metal-salt drying installation comprises and the tank connected Highspeedcentrifugingandsprayingdrier of described lass lining salt-forming reaction.
Improve as one, on arbitrary described steeping tank, be equipped with self-circulation pipeline.
Improve as one, described in two, between steeping tank, be provided with circulation line.
Improve as one, described the second conveying belt is positioned at flatly below plane, between described vent valves and the second conveying belt, is provided with material slide carriage.
Improve as one, the cross-sectional shape of described material slide carriage is flute profile.
Improve as one, the connecting tube that described saponification liquor separating tank and described saponification liquor are kept between tank, the temporary tank of gasoline is provided with pipeline viewing mirror.
Improve as one, described pipeline viewing mirror comprises the Glass tubing being arranged between the first flange and the second flange, and described the first flange tightens together described the first flange, the second flange and Glass tubing by threaded stud with the second flange.
Adopted after technique scheme, the beneficial effects of the utility model are:
Because chlorophyll metal-salt Preparation equipment comprises the silkworm excrement softening installation setting gradually, silkworm excrement infuser device, silkworm excrement soak solution concentrating unit, chlorophyl liquid concentrating unit, the molten paste device of chlorophyll, chlorophyll device for saponifying, chlorophyll metal device, chlorophyllin gasifying device, chlorophyll salify device and chlorophyll metal-salt drying installation, extract chlorophyllous process from silkworm excrement, under vacuum environment, reclaim respectively acetone and water, shorten concentration time, improve thickening efficiency, utilize the chlorophyll extracting to prepare in the process of chlorophyll metal-salt, through molten paste, saponification, metallization, acidifying, the steps such as salify, remove impurity comprising separating for several times, in the chlorophyll metal-salt obtaining, foreign matter content is few.
Owing to being equipped with self-circulation pipeline on arbitrary steeping tank, self-circulation pipeline can make the acetone in steeping tank flow, and the flow circuit of acetone can accelerate to extract chlorophyllous speed, shortens extraction time, raises the efficiency.
Owing to being provided with circulation line between two steeping tanks, circulation line can make two acetone in steeping tank occur to flow, and further can accelerate to extract chlorophyllous speed, shortens extraction time, raises the efficiency.
Because the second conveying belt is positioned at flatly below plane, between vent valves and the second conveying belt, be provided with material slide carriage, the second conveying belt is located at flatly plane and does not take up space below, between vent valves and the second conveying belt, be provided with material slide carriage, can make silkworm excrement better be discharged to the second conveying belt from steeping tank.
Because the cross-sectional shape of material slide carriage is flute profile, can prevent that silkworm excrement from tumbling from the second conveying belt.
Because the connecting tube between the temporary tank of saponification liquor separating tank and gasoline, the temporary tank of saponification liquor is provided with pipeline viewing mirror, can observe the mobility status of liquid by pipeline viewing mirror, accurately control saponification liquor and waste vapour oil separating, minimizing foreign matter content.
Accompanying drawing explanation
Fig. 1 is structural representation of the present utility model;
In figure: 1, the first conveying belt, 2, hopper, 3, vibratory screening apparatus, 4, vibration screen, 5, stirrer, 6, inlet channel, 7, dust receiving tank, 8, induced draft fan, 9, lift, 10, feed pipe, 11, steeping tank, 12, first heater, 13, acetone pipeline, 14, material inlet valve, 15, reinforced flexible pipe, 16, vent valves, 17, the second conveying belt, 18, waste residue storage pool, 19, soak solution is kept in tank, 20, lass lining recover acetone retort, 21, separating tank, 22, the first spiral-plate heat exchanger, 23, acetone is kept in tank, 24, the first vacuum pump, 25, secondary heating mechanism, 26, thickening filtration pond, 261, filtering layer, 27, lass lining concentration response tank, 28, suction pipeline, 29, secondary spiral lamina interchanger, 30, yellow water is kept in tank, 31, the second vacuum pump, 32, the 3rd heating unit, 33, the molten paste retort of lass lining, 34, molten paste separating tank, 35, alcohol pipeline, 36, the 3rd vacuum pump, 37, the 4th heating unit, 38, the first whipping appts, 39, lass lining saponification reaction tank, 40, saponification separating tank, 41, saponification liquor is kept in tank, 42, alcohol is kept in tank, 43, gasoline is kept in tank, 44, liquid caustic soda pipeline, 45, gasoline pipeline, 46, alcohol pipeline, 47, the 5th heating unit, 48, the second whipping appts, 49, lass lining metallization reaction tank, 50, metallization separating tank, 51, metal-salt pipeline, 52, the 6th heating unit, 53, the 3rd whipping appts, 54, lass lining acidification reaction tank, 55, impurity is kept in tank, 56, acid adding pipeline, 57, the 7th heating unit, 58, the 4th whipping appts, 59, lass lining salt-forming reaction tank, 60, liquid caustic soda pipeline, 61, the 8th heating unit, 62, the 5th whipping appts, 63, Highspeedcentrifugingandsprayingdrier, 64, self-circulation pipeline, 65, circulation line, 66, material slide carriage, 67, pipeline viewing mirror, 671, the first flange, 672, the second flange, 673, Glass tubing.
Embodiment
In order to make the purpose of this utility model, technical scheme and advantage clearer, below in conjunction with drawings and Examples, the utility model is further elaborated.Should be appreciated that specific embodiment described herein is only in order to explain the utility model, and be not used in restriction the utility model.
Fig. 1 is the structural representation of the chlorophyll metal-salt Preparation equipment that provides of the utility model, for convenience of explanation, has only provided the part relevant to the utility model in figure.
The chlorophyll metal-salt Preparation equipment that the utility model provides, comprise the silkworm excrement softening installation, silkworm excrement infuser device, silkworm excrement soak solution concentrating unit, chlorophyl liquid concentrating unit, the molten paste device of chlorophyll, chlorophyll device for saponifying, chlorophyll metal device, chlorophyllin gasifying device, chlorophyll salify device and the chlorophyll metal-salt drying installation that set gradually
Silkworm excrement softening installation comprises the first conveying belt 1 being driven by power set, one end of the first conveying belt 1 is provided with hopper 2, the first conveying belt 1 is provided with vibratory screening apparatus 3 away from one end of hopper 2, in vibratory screening apparatus, be provided with the vibration screen 4 being obliquely installed, vibratory screening apparatus 3 is provided with stirrer 5 away from one end of the first conveying belt 1, on stirrer 5, be also provided with inlet channel 6, the bottom of vibratory screening apparatus 3 is provided with dust receiving tank 7, dust receiving tank 7 connects induced draft fan 8, silkworm excrement mixes more even with water, bating effect is good, also greatly alleviated workman's labour intensity, the dust containing in silkworm excrement can be collected in dust receiving tank 7, drain by induced draft fan 8, prevent that dust from flying upward in air, protection workman's is healthy,
Silkworm excrement infuser device comprises the lift 9 that is arranged on stirrer 5 downstreams, lift 9 is arranged on one end of feed pipe 10, on feed pipe 10, be set up in parallel several steeping tanks 11, in all steeping tanks 11, be provided with first heater 12, the top of steeping tank 11 is provided with acetone pipeline 13 and material inlet valve 14, feed pipe 10 is positioned at the top of material inlet valve 14, material inlet valve 14 connects feed pipe 10 by reinforced flexible pipe 15, reinforced flexible pipe 15 one end are fixedly mounted on feed pipe 10, the opening for feed of the other end and material inlet valve 14 is suitable, the bottom of steeping tank 11 is provided with vent valves 16, below one side position of vent valves 16 is provided with the second conveying belt 17 being driven by power set, all vent valves 16 are all towards the second conveying belt 17, the end of the second conveying belt 17 is provided with waste residue storage pool 18, charging and discharge automatization, greatly alleviate workman's labour intensity,
Silkworm excrement soak solution concentrating unit comprises the temporary tank 19 of the soak solution being connected with steeping tank 11, the temporary tank 19 of soak solution connects lass lining recover acetone reaction 20, lass lining recover acetone reaction 20 connects separating tank 21, the top of lass lining recover acetone reaction 20 connects the first spiral-plate heat exchanger 22, the first spiral-plate heat exchanger 22 connects the temporary tank 23 of acetone, on the top of lass lining recover acetone reaction 20, be also provided with the first vacuum pump 24, in lass lining recover acetone reaction 20, be provided with secondary heating mechanism 25, the first vacuum pump 24 can reduce the pressure in lass lining recover acetone reaction 20, reduce the boiling point of acetone, accelerating the evaporation of acetone reclaims, shorten the concentration time of soak solution, improve thickening efficiency, connect steeping tank 11 and be provided with filtering net with the pipeline of the temporary tank 19 of soak solution near one end of steeping tank 11, can prevent that silkworm excrement from entering in the temporary tank 19 of soak solution with soak solution,
Chlorophyl liquid concentrating unit comprises thickening filtration pond 26 and lass lining concentration response tank 27, thickening filtration pond 26 is positioned at the below of separating tank 21, in thickening filtration pond 26, be provided with filtering layer 261, the top of lass lining concentration response tank 27 is provided with suction pipeline 28, the end of suction pipeline 28 is positioned at thickening filtration pond 26 and is positioned at the top of filtering layer 261, the top of lass lining concentration response tank 27 connects secondary spiral lamina interchanger 29, secondary spiral lamina interchanger 29 connects the temporary tank 30 of yellow water, the top of lass lining concentration response tank 27 is also provided with the second vacuum pump 31, in lass lining concentration response tank 27, be provided with the 3rd heating unit 32, the a part of water in chlorophyl liquid can be first removed in thickening filtration pond 26, shorten the concentration time of chlorophyl liquid, the second vacuum pump 31 can reduce the pressure in lass lining concentration response tank 27, reduce the boiling point of water, accelerating evaporation of water reclaims, further shorten the concentration time of chlorophyl liquid, improve thickening efficiency,
The molten paste device of chlorophyll comprises the molten paste retort 33 of the lass lining being connected with lass lining concentration response tank 27, the molten paste retort 33 of lass lining connects molten paste separating tank 34, the top of the molten paste retort 33 of lass lining is provided with alcohol pipeline 35, the top of the molten paste retort 33 of lass lining is also connected with the 3rd vacuum pump 36, the inside of the molten paste retort 33 of lass lining is provided with the 4th heating unit 37, in the molten paste retort 33 of lass lining, be also provided with the first whipping appts 38, the 3rd vacuum pump 36 is conducive to pasty state chlorophyll by being evacuated in molten lass lining paste retort 33 enters, the chlorophyll of pasty state is dissolved in alcohol in the molten paste retort 33 of lass lining, enter the interior stratification of molten paste separating tank 34, the alcohol that contains impurity is on upper strata, chlorophyll is in lower floor,
Chlorophyll device for saponifying comprises the lass lining saponification reaction tank 39 being connected with molten paste separating tank 34, lass lining saponification reaction tank 39 connects saponification separating tank 40, saponification separating tank 40 connects the temporary tank 41 of saponification liquor, between molten paste separating tank 34 and lass lining saponification reaction tank 39, be provided with first branch that is used for separating alcohol, the first branch comprises that alcohol keeps in tank 42, between the temporary tank 41 of saponification separating tank 40 and saponification liquor, be provided with second branch that is used for separating gasoline, the second branch comprises that gasoline keeps in tank 43, the top of lass lining saponification reaction tank 39 is provided with liquid caustic soda pipeline 44, gasoline pipeline 45 and alcohol pipeline 46, the inside of lass lining saponification reaction tank 39 is provided with the 5th heating unit 47, on lass lining saponification reaction tank 39, be also provided with the second whipping appts 48, in lass lining saponification reaction tank 39 inner chlorophylls and liquid caustic soda saponification reaction, enter the interior stratification of saponification separating tank 40, the gasoline that contains impurity is on upper strata, chlorophyll is in lower floor,
Chlorophyll metal device comprises that keeping in tank 41 with saponification liquor is connected lass lining metallization reaction tank 49, lass lining metallization reaction tank 49 connection metal separating tanks 50, the top of lass lining metallization reaction tank 49 is provided with metal-salt pipeline 51, in lass lining metallization reaction tank 49, be provided with the 6th heating unit 52, on lass lining metallization reaction tank 49, be also provided with the 3rd whipping appts 53, generate chlorophyll metal liquid at lass lining metallization reaction tank 49 inner chlorophyll saponification liquors and reacting metal salt;
Chlorophyllin gasifying device comprises the lass lining acidification reaction tank 54 being connected with metallization separating tank 50, between metallization separating tank 50 and lass lining acidification reaction tank 54, be provided with the 3rd branch that is used for separating impurity, the 3rd branch comprises that impurity keeps in tank 55, the top of lass lining acidification reaction tank 54 is provided with acid adding pipeline 56, the inside of lass lining acidification reaction tank 54 is provided with the 7th heating unit 57, on lass lining acidification reaction tank 54, be also provided with the 4th whipping appts 58, generate chlorophyll metal acid at lass lining acidification reaction tank 54 inner chlorophyll metallization liquid and acid-respons;
Chlorophyll salify device comprises the lass lining salt-forming reaction tank 59 being connected with lass lining acidification reaction tank 54, lass lining salt-forming reaction tank 59 is provided with liquid caustic soda pipeline 60, the inside of lass lining salt-forming reaction tank 59 is provided with the 8th heating unit 61, on lass lining salt-forming reaction tank 59, be also provided with the 5th whipping appts 62, in lass lining acidification reaction tank 54, chlorophyll metal acid is reacted with liquid caustic soda and is generated chlorophyll metal-salt;
Chlorophyll metal-salt drying installation comprises the Highspeedcentrifugingandsprayingdrier 63 being connected with lass lining salt-forming reaction tank 59.
On arbitrary steeping tank 11, be equipped with self-circulation pipeline 64, self-circulation pipeline 64 can make the acetone in steeping tank 11 flow, the flow circuit of acetone can accelerate to extract chlorophyllous speed, shorten extraction time, raise the efficiency, the two ends of self-circulation pipeline 64 are equipped with filtering net, can prevent that silkworm excrement from flowing and stopping up self-circulation pipeline 64 with acetone.
Between two steeping tanks, be provided with circulation line 65, circulation line 65 can make two acetone in steeping tank occur to flow, further can accelerate to extract chlorophyllous speed, shorten extraction time, raise the efficiency, the two ends of circulation line 65 are also equipped with filtering net, can prevent that silkworm excrement from flowing and stopping up circulation line 65 with acetone.
The second conveying belt 17 is positioned at flatly below plane, between vent valves 16 and the second conveying belt 17, be provided with material slide carriage 66, the second conveying belt 17 is located at flatly plane and does not take up space below, material slide carriage 66 can make silkworm excrement better be discharged to the second conveying belt 17 from steeping tank 11, the cross-sectional shape of material slide carriage 66 is flute profile, can prevent that silkworm excrement from tumbling from the second conveying belt 17.
The connecting tube that saponification liquor separating tank 40 and saponification liquor are kept between tank 41, the temporary tank 43 of gasoline is provided with pipeline viewing mirror 67, pipeline viewing mirror 67 comprises the Glass tubing 673 being arranged between the first flange 671 and the second flange 672, the first flange 671 tightens together the first flange 671, the second flange 672 and Glass tubing 673 by threaded stud with the second flange 672, can observe the mobility status of liquid by pipeline viewing mirror 67, accurately control saponification liquor and waste vapour oil separating, reduce foreign matter content.
First heater 12, secondary heating mechanism 25, the 3rd heating unit 32, the 4th heating unit 37, the 5th heating unit the 47, the 64 heating unit 52, the 7th heating unit 57 and the 8th heating unit 61 include the coil pipe being arranged in retort, coil pipe connects steam-pipe, the heating of employing coil pipe, is heated in retort more even.
The first whipping appts 38, the second whipping appts 48, the 3rd whipping appts 53, the 4th whipping appts 58 and the 5th whipping appts 62 include the agitator motor being arranged on outside retort, agitator motor drives stir shaft to rotate, some agitating vanes are installed on stir shaft, in the axial direction of stir shaft, some agitating vanes are installed in the shape of a spiral along the circumference of stir shaft, and stir shaft rotates more steady, and mixing effect is better, whipping appts can be accelerated the speed of response in retort, enhances productivity.
These are only preferred embodiment of the present utility model, not in order to limit the utility model, all any modifications of doing within spirit of the present utility model and principle, be equal to and replace and improvement etc., within all should being included in protection domain of the present utility model.

Claims (7)

1. chlorophyll metal-salt Preparation equipment, it is characterized in that, comprise the silkworm excrement softening installation, silkworm excrement infuser device, silkworm excrement soak solution concentrating unit, chlorophyl liquid concentrating unit, the molten paste device of chlorophyll, chlorophyll device for saponifying, chlorophyll metal device, chlorophyllin gasifying device, chlorophyll salify device and the chlorophyll metal-salt drying installation that set gradually
Described silkworm excrement softening installation comprises the first conveying belt being driven by power set, one end of described the first conveying belt is provided with hopper, described the first conveying belt is provided with vibratory screening apparatus away from one end of described hopper, described vibratory screening apparatus is provided with stirrer away from one end of described the first conveying belt, on described stirrer, be also provided with inlet channel, the bottom of described vibratory screening apparatus is provided with dust receiving tank, and described dust receiving tank connects induced draft fan;
Described silkworm excrement infuser device comprises the lift that is arranged on stirrer downstream, described lift is arranged on one end of feed pipe, on described feed pipe, be set up in parallel several steeping tanks, in all described steeping tanks, be provided with first heater, the top of described steeping tank is provided with acetone pipeline and material inlet valve, described feed pipe is positioned at the top of described material inlet valve, described material inlet valve is by reinforced hose connection feed pipe, described reinforced flexible pipe one end is fixedly mounted on described feed pipe, the opening for feed of the other end and described material inlet valve is suitable, the bottom of described steeping tank is provided with vent valves, below one side position of described vent valves is provided with the second conveying belt being driven by power set, all described vent valves are all towards described the second conveying belt, the end of described the second conveying belt is provided with waste residue storage pool,
Described silkworm excrement soak solution concentrating unit comprises and the temporary tank of the tank connected soak solution of described immersion, the temporary tank of described soak solution connects lass lining recover acetone retort, described lass lining recover acetone retort connects separating tank, the top of described lass lining recover acetone retort connects the first spiral-plate heat exchanger, described the first spiral-plate heat exchanger connects the temporary tank of acetone, on the top of described lass lining recover acetone retort, be also provided with the first vacuum pump, in described lass lining recover acetone retort, be provided with secondary heating mechanism;
Described chlorophyl liquid concentrating unit comprises thickening filtration pond and lass lining concentration response tank, described thickening filtration pond is positioned at the below of described separating tank, described thickening filtration is provided with filtering layer in pond, the top of described lass lining concentration response tank is provided with suction pipeline, the end of described suction pipeline is positioned at described thickening filtration pond and is positioned at the top of described filtering layer, the top of described lass lining concentration response tank connects secondary spiral lamina interchanger, described secondary spiral lamina interchanger connects the temporary tank of yellow water, the top of described lass lining concentration response tank is also provided with the second vacuum pump, in described lass lining concentration response tank, be provided with the 3rd heating unit,
The molten paste device of described chlorophyll comprises and the molten paste retort of the tank connected lass lining of described lass lining concentration response, the molten paste retort of described lass lining connects molten paste separating tank, the top of the molten paste retort of described lass lining is provided with alcohol pipeline, the top of the molten paste retort of described lass lining is also connected with the 3rd vacuum pump, the inside of the molten paste retort of described lass lining is provided with the 4th heating unit, in the molten paste retort of described lass lining, is also provided with the first whipping appts;
Described chlorophyll device for saponifying comprises and separates tank connected lass lining saponification reaction tank with described molten paste, described lass lining saponification reaction tank connects saponification liquor separating tank, described saponification liquor separating tank connects the temporary tank of saponification liquor, between described molten paste separating tank and lass lining saponification reaction tank, be provided with first branch that is used for separating alcohol, described the first branch comprises that alcohol keeps in tank, between the temporary tank of described saponification liquor separating tank and saponification liquor, be provided with second branch that is used for separating gasoline, described the second branch comprises that gasoline keeps in tank, the top of described lass lining saponification reaction tank is provided with liquid caustic soda pipeline, gasoline pipeline and alcohol pipeline, the inside of described lass lining saponification reaction tank is provided with the 5th heating unit, on described lass lining saponification reaction tank, be also provided with the second whipping appts,
Described chlorophyll metal device comprises that keeping in tank with described saponification liquor is connected lass lining metallization reaction tank, described lass lining metallization reaction tank connection metal separating tank, the top of described lass lining metallization reaction tank is provided with metal-salt pipeline, in described lass lining metallization reaction tank, be provided with the 6th heating unit, on described lass lining metallization reaction tank, be also provided with the 3rd whipping appts;
Described chlorophyllin gasifying device comprises and separates tank connected lass lining acidification reaction tank with described metallization, between described metallization separating tank and lass lining acidification reaction tank, be provided with the 3rd branch that is used for separating impurity, described the 3rd branch comprises that impurity keeps in tank, the top of described lass lining acidification reaction tank is provided with acid adding pipeline, the inside of described lass lining acidification reaction tank is provided with the 7th heating unit, on described lass lining acidification reaction tank, is also provided with the 4th whipping appts;
Described chlorophyll salify device comprises and the tank connected lass lining salt-forming reaction of described lass lining acidification reaction tank, described lass lining salt-forming reaction tank is provided with liquid caustic soda pipeline, the inside of described lass lining salt-forming reaction tank is provided with the 8th heating unit, on described lass lining salt-forming reaction tank, is also provided with the 5th whipping appts;
Described chlorophyll metal-salt drying installation comprises and the tank connected Highspeedcentrifugingandsprayingdrier of described lass lining salt-forming reaction.
2. chlorophyll metal-salt Preparation equipment as claimed in claim 1, is characterized in that, on arbitrary described steeping tank, is equipped with self-circulation pipeline.
3. chlorophyll metal-salt Preparation equipment as claimed in claim 2, is characterized in that, is provided with circulation line described in two between steeping tank.
4. chlorophyll metal-salt Preparation equipment as claimed in claim 1, is characterized in that, described the second conveying belt is positioned at flatly below plane, between described vent valves and the second conveying belt, is provided with material slide carriage.
5. chlorophyll metal-salt Preparation equipment as claimed in claim 4, is characterized in that, the cross-sectional shape of described material slide carriage is flute profile.
6. chlorophyll metal-salt Preparation equipment as claimed in claim 1, is characterized in that, the connecting tube that described saponification liquor separating tank and described saponification liquor are kept between tank, the temporary tank of gasoline is provided with pipeline viewing mirror.
7. chlorophyll metal-salt Preparation equipment as claimed in claim 6, it is characterized in that, described pipeline viewing mirror comprises the Glass tubing being arranged between the first flange and the second flange, and described the first flange tightens together described the first flange, the second flange and Glass tubing by threaded stud with the second flange.
CN201320804210.7U 2013-12-06 2013-12-06 Chlorophyll metal salt preparation equipment Withdrawn - After Issue CN203593712U (en)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103626780A (en) * 2013-12-06 2014-03-12 潍坊瀚星叶绿素有限公司 Preparation equipment of chlorophyll metal salt

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103626780A (en) * 2013-12-06 2014-03-12 潍坊瀚星叶绿素有限公司 Preparation equipment of chlorophyll metal salt
CN103626780B (en) * 2013-12-06 2015-05-20 潍坊瀚星叶绿素有限公司 Preparation equipment of chlorophyll metal salt

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