CN203336898U - 一种空分液空进氩塔汽提装置 - Google Patents

一种空分液空进氩塔汽提装置 Download PDF

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CN203336898U
CN203336898U CN201320326572XU CN201320326572U CN203336898U CN 203336898 U CN203336898 U CN 203336898U CN 201320326572X U CN201320326572X U CN 201320326572XU CN 201320326572 U CN201320326572 U CN 201320326572U CN 203336898 U CN203336898 U CN 203336898U
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air
connecting pipeline
pipeline
liquid
liquid air
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汤爱平
顾栋磊
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SHANGHAI BAOMIN INDUSTRIAL GASES Co Ltd
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SHANGHAI BAOMIN INDUSTRIAL GASES Co Ltd
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    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642Recovering noble gases from air
    • F25J3/04648Recovering noble gases from air argon
    • F25J3/04721Producing pure argon, e.g. recovered from a crude argon column
    • F25J3/04727Producing pure argon, e.g. recovered from a crude argon column using an auxiliary pure argon column for nitrogen rejection
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04642Recovering noble gases from air
    • F25J3/04648Recovering noble gases from air argon
    • F25J3/04654Producing crude argon in a crude argon column
    • F25J3/04666Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system
    • F25J3/04672Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser
    • F25J3/04678Producing crude argon in a crude argon column as a parallel working rectification column of the low pressure column in a dual pressure main column system having a top condenser cooled by oxygen enriched liquid from high pressure column bottoms
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04793Rectification, e.g. columns; Reboiler-condenser
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04793Rectification, e.g. columns; Reboiler-condenser
    • F25J3/048Argon recovery
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J3/00Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification
    • F25J3/02Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream
    • F25J3/04Processes or apparatus for separating the constituents of gaseous or liquefied gaseous mixtures involving the use of liquefaction or solidification by rectification, i.e. by continuous interchange of heat and material between a vapour stream and a liquid stream for air
    • F25J3/04763Start-up or control of the process; Details of the apparatus used
    • F25J3/04769Operation, control and regulation of the process; Instrumentation within the process
    • F25J3/04793Rectification, e.g. columns; Reboiler-condenser
    • F25J3/048Argon recovery
    • F25J3/04806High purity argon purification
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2210/00Processes characterised by the type or other details of the feed stream
    • F25J2210/40Air or oxygen enriched air, i.e. generally less than 30mol% of O2
    • FMECHANICAL ENGINEERING; LIGHTING; HEATING; WEAPONS; BLASTING
    • F25REFRIGERATION OR COOLING; COMBINED HEATING AND REFRIGERATION SYSTEMS; HEAT PUMP SYSTEMS; MANUFACTURE OR STORAGE OF ICE; LIQUEFACTION SOLIDIFICATION OF GASES
    • F25JLIQUEFACTION, SOLIDIFICATION OR SEPARATION OF GASES OR GASEOUS OR LIQUEFIED GASEOUS MIXTURES BY PRESSURE AND COLD TREATMENT OR BY BRINGING THEM INTO THE SUPERCRITICAL STATE
    • F25J2235/00Processes or apparatus involving steps for increasing the pressure or for conveying of liquid process streams
    • F25J2235/06Lifting of liquids by gas lift, e.g. "Mammutpumpe"

Abstract

一种空分液空进氩塔汽提装置,安装于空分冷箱;包括,两个液空节流阀,安装于空分冷箱,并通过管路分别连接于粗氩塔、精氩塔;第一、第二连接管路,分别对应连接于所述两个液空阀,该第一、第二连接管路上分别设有截止阀、压力表、单向阀;进气管路,其进口端连接压缩空气,出口端分别连接第一、第二连接管路;该进气管路中设控制阀。本实用新型在空分装置正常运行阶段使用压缩空气作为冷箱液空的汽提气,实现了低成本生产,克服原液空输送上的缺陷;保证了制氩系统的稳定运行。

Description

一种空分液空进氩塔汽提装置
技术领域
本实用新型属于空气分离领域,具体涉及一种空分液空进氩塔汽提装置。
背景技术
空气分离在工业上最常用的方法就是低温分离法。空气中的氧、氮、氩等组分在低温下通过精馏被分离出来。其中氧、氮组分通过主塔精馏被分离出来,而粗氩塔及精氩塔分别分离氩、氧组分及氩氮组分,在精氩塔底部得到纯度为99.999%的液氩产品。
随着空分设计和制造工艺的不断变革,单套空分装置生产能力更大、更安全、更节能、产品提取率也更高,但伴随生产能力扩大而来的是精馏塔越来越高,各塔之间低温液体物料输送难度越来越大,为了缓解低温液体输送问题,低温液体汽提输送技术越来越多的被采用。该技术具有设备简单可靠、投资少、节能、便于操作等优点。
目前国内小空分低温液体输送大都靠节流阀节流后压力能转化成速度能,前后的管道管径变化,可以保证低温液体获得足够的动力,并控制低温液体流速。缺点是精馏塔的高度不能过高,以及下塔压力要求高,造成空压机出口压力也需相应提高,空分的运行成本偏高。
国外部分厂家使用的是汽提阀提供与低温液体的温度和组分相近的气体通入提升管。低温液体与汽提气在节流阀后的提升管内汽液混合“密度”降低。根据连通管原理,在上下塔压差不变的情况下,提升管内“低密度液体”将升的更高。这种方法的优点是对下塔的压力要求不高,精馏塔的设计高度也可适当放高,有利于精馏。缺点是所提供的气体必须与低温液体的温度和组分相近,汽提阀及汽提管路需安装在冷箱内,设计制造安装的成本都大幅提高。
发明内容
本实用新型的目的在于提供一种空分液空进氩塔汽提装置,获得低运行成本、高可靠性的汽提气。
为达到上述目的,本实用新型的技术方案是:
一种空分液空进氩塔汽提装置,安装于空分冷箱;包括,两个液空节流阀,安装于空分冷箱,并通过管路分别连接于粗氩塔、精氩塔;第一、第二连接管路,分别对应连接于所述两个液空阀,该第一、第二连接管路上分别设有截止阀、压力表、单向阀;进气管路,其进口端连接压缩空气,出口端分别连接第一、第二连接管路;该进气管路中设控制阀。
本实用新型的有益效果:
本实用新型在空分装置正常运行阶段使用压缩空气作为冷箱液空的的汽提气,实现了低成本生产,克服原液空输送上的缺陷;保证了制氩系统的稳定运行。
附图说明
图1为本实用新型一实施例的结构示意图。
具体实施方式
参见图1,本实用新型的一种空分液空进氩塔汽提装置,安装于空分冷箱100;包括,两个液空节流阀1、2,安装于空分冷箱100,并通过管路分别连接于粗氩塔A、精氩塔B;第一、第二连接管路3、4,分别对应连接于所述两个液空阀1、2,该第一、第二连接管路3、4上分别设有截止阀5、5’、压力表6、6’、单向阀7、7’;进气管路8,其进口端连接压缩空气,出口端分别连接第一、第二连接管路3、4;该进气管路中设控制阀9。空分冷箱100内还包括下塔C,空分冷箱100内还有珠光砂填充物。
本实用新型在空分装置正常运行阶段使用压缩空气作为冷箱液空的的汽提气,实现了低成本生产,克服原液空输送上的缺陷;保证了制氩系统的稳定运行。

Claims (1)

1.一种空分液空进氩塔汽提装置,安装于空分冷箱;其特征在于,包括,
两个液空节流阀,安装于空分冷箱,并通过管路分别连接于粗氩塔、精氩塔;
第一、第二连接管路,分别对应连接于所述两个液空阀,该第一、第二连接管路上分别设有截止阀、压力表、单向阀;
进气管路,其进口端连接压缩空气,出口端分别连接第一、第二连接管路;该进气管路中设控制阀。
CN201320326572XU 2013-06-06 2013-06-06 一种空分液空进氩塔汽提装置 Expired - Fee Related CN203336898U (zh)

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Cited By (1)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103968642A (zh) * 2014-05-15 2014-08-06 南通天源气体有限公司 一种塔式提高气体纯度的方法

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103968642A (zh) * 2014-05-15 2014-08-06 南通天源气体有限公司 一种塔式提高气体纯度的方法
CN103968642B (zh) * 2014-05-15 2016-05-18 南通天源气体有限公司 一种塔式提高气体纯度的方法

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Termination date: 20180606