CN203241343U - Photoelectric direct reading spectrometer - Google Patents

Photoelectric direct reading spectrometer Download PDF

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Publication number
CN203241343U
CN203241343U CN 201320127588 CN201320127588U CN203241343U CN 203241343 U CN203241343 U CN 203241343U CN 201320127588 CN201320127588 CN 201320127588 CN 201320127588 U CN201320127588 U CN 201320127588U CN 203241343 U CN203241343 U CN 203241343U
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CN
China
Prior art keywords
control plate
beam splitting
constant temperature
frequency
photomultiplier
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Expired - Fee Related
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CN 201320127588
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Chinese (zh)
Inventor
夏赞贵
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NANJING NONGBO ANALYTICAL INSTRUMENT Co Ltd
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NANJING NONGBO ANALYTICAL INSTRUMENT Co Ltd
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Priority to CN 201320127588 priority Critical patent/CN203241343U/en
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Publication of CN203241343U publication Critical patent/CN203241343U/en
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  • Investigating, Analyzing Materials By Fluorescence Or Luminescence (AREA)

Abstract

The utility model discloses a photoelectric direct reading spectrometer. The photoelectric direct reading spectrometer comprises a constant temperature system, a beam splitting system, a vacuumizing system, a gas supply system, a measurement and control system, a stimulating system and photomultiplier tube, wherein the constant temperature system is used for ensuring that the beam splitting system is at the constant temperature; the vacuumizing system is used for vacuumizing the beam splitting system; the gas supply system is used for supplying gas to the beam splitting system; the stimulating system is used for generating high voltage with fixed frequency to stimulate a sample and ensuring that all stimulated elements of the sample pass through the beam splitting system and enter corresponding photomultiplier tubes; the measurement and control system is used for acquiring signals of the photomultiplier tubes and analyzing the acquired signals; the stimulating system comprises a stable voltage power supply, a rectifying module, a main control plate, a light source control plate, a frequency control plate, a high voltage plate and a stimulating device; 220V alternating current passes through the stable voltage power supply and the rectifying module and is input into the main control plate; the light source control plate and the frequency control plate are connected with the main control plate; adjustable frequency reference voltage output by the main control plate rises by virtue of the high voltage plate and is input into the stimulating device.

Description

Photo-electric direct reading spectrometer
Technical field
The utility model relates to a kind of photo-electric direct reading spectrometer.
Background technology
In order to improve the quality of products, the chemical composition of every profession and trade testing product generally adopts spectral analysis and wet chemistry analysis, adopts the traditional wet chemical analysis method to detect, and exists detection speed slow, and the shortcomings such as the easy contaminated environment of chemical reagent;
Spectroanalysis instrument is to utilize the physical method analysis, utilizes the electric spark excited sample, the photoelectric tube sampling, and quick and convenient, detection elements is many, but high to conditional requests such as analysis environments;
At present China's casting and detection industry use photo-electric direct reading spectrometer as quality control method, have progressively replaced traditional wet chemistry analytic approach, have developed into so far medium-sized and small enterprises and have also progressively adopted spectroscopic methodology to do the detection of on-the-spot sample analysis and finished product.
Summary of the invention
The purpose of this utility model is to provide a kind of photo-electric direct reading spectrometer, and this spectrometer excitation source segmental stability is better, so the spectrometer test is more accurate.
In order to realize above purpose, the technical scheme that the utility model adopts is:
Photo-electric direct reading spectrometer comprises constant temperature system, beam splitting system, pumped vacuum systems, air supply system, TT﹠C system, activating system and photomultiplier; Constant temperature system guarantees that beam splitting system is in constant temperature; Pumped vacuum systems is used for beam splitting system and vacuumizes processing; Air supply system is the beam splitting system air feed; Thereby activating system produces the high pressure excited sample of fixed frequency, then all elements that sample is inspired enters corresponding photomultiplier by beam splitting system, TT﹠C system is carried out signals collecting to photomultiplier, then the signal that gathers is carried out analyzing and processing, thereby obtain the percentage composition of each element in the material; It is characterized in that, described activating system comprises stabilized voltage supply, rectification module, master control borad, light source control plate, frequency control plate, hardboard and excitation apparatus; 220V exchanges through inputting master control borad after stabilized voltage supply and the rectification module, and the light source control plate links to each other with master control borad with the frequency control plate, and the frequency adjustable reference voltage of master control borad stable output inputs to excitation apparatus after boosting by hardboard.
Compared with prior art, the utility model has the advantage of: this spectrometer excitation source segmental stability is better, so the spectrometer test is more accurate.
Description of drawings
Fig. 1 is the photo-electric direct reading spectrometer block diagram;
Fig. 2 is activating system block diagram in the utility model photo-electric direct reading spectrometer.
Embodiment
Below in conjunction with accompanying drawing the utility model is described further.
Photo-electric direct reading spectrometer comprises constant temperature system, beam splitting system, pumped vacuum systems, air supply system, TT﹠C system, activating system and photomultiplier; Constant temperature system guarantees that beam splitting system is in constant temperature; Pumped vacuum systems is used for beam splitting system and vacuumizes processing; Air supply system is the beam splitting system air feed; Thereby activating system produces the high pressure excited sample of fixed frequency, then all elements that sample is inspired enters corresponding photomultiplier by beam splitting system, TT﹠C system is carried out signals collecting to photomultiplier, then the signal that gathers is carried out analyzing and processing, thereby obtain the percentage composition of each element in the material; It is characterized in that, described activating system comprises stabilized voltage supply, rectification module, master control borad, light source control plate, frequency control plate, hardboard and excitation apparatus; 220V exchanges through inputting master control borad after stabilized voltage supply and the rectification module, and the light source control plate links to each other with master control borad with the frequency control plate, and the frequency adjustable reference voltage of master control borad stable output inputs to excitation apparatus after boosting by hardboard.
In order to guarantee to analyze stability and precision, except reduce the interference of matrix element with software, collection signal has been carried out filtering, analytic signal carries out curve fitting etc., the method that also adopts stepper motor to carry out trace is adjusted automatically, reduce because the spectral line drift that the impact of the variation of temperature and other factor causes improves precision.
And the stability of raising activating system, it is the key factor that improves the spectrometer performance, in order to reach the stability Design purpose that improves activating system, at first adopt high stable magnetic saturation power conditioner to exciting the unit power supply, the power supply of high stable is provided, also the interference shielding that excites can be fallen, disturb the collection that seals in the line influence signal in case excite, then the rectification that exchanges, DC voltage reaches 400V after the rectification, then under the control of frequency control plate, produce the voltage of frequency stabilization, under computer software control, master control board can be carried out frequency and magnitude of voltage is adjusted to this voltage, generate stable frequency adjustable reference voltage, through high pressure generator voltage is risen to stable high voltage 15KV, by excitation bench, in fixing distance sample is excited, reach a stable excited state, thereby effectively guaranteed the stability of analyzing.
The principle of photo-electric direct reading spectrometer is that the high temperature with spark makes each element in the sample from solid-state direct gasification and is excited and launches the characteristic wavelength of each element, behind grating beam splitting, become " spectrum " arranged by wavelength, the characteristic light spectral line of these elements passes through exit slit, inject photomultiplier separately, light signal becomes electric signal, through the control survey system of instrument with the electric signal integration and carry out mould/number conversion, then by Computer Processing, and print the percentage composition of each element.

Claims (1)

1. photo-electric direct reading spectrometer comprises constant temperature system, beam splitting system, pumped vacuum systems, air supply system, TT﹠C system, activating system and photomultiplier; Constant temperature system guarantees that beam splitting system is in constant temperature; Pumped vacuum systems is used for beam splitting system and vacuumizes processing; Air supply system is the beam splitting system air feed; Thereby activating system produces the high pressure excited sample of fixed frequency, then all elements that sample is inspired enters corresponding photomultiplier by beam splitting system, TT﹠C system is carried out signals collecting to photomultiplier, then the signal that gathers is carried out analyzing and processing, thereby obtain the percentage composition of each element in the material; It is characterized in that, described activating system comprises stabilized voltage supply, rectification module, master control borad, light source control plate, frequency control plate, hardboard and excitation apparatus; 220V exchanges through inputting master control borad after stabilized voltage supply and the rectification module, and the light source control plate links to each other with master control borad with the frequency control plate, and the frequency adjustable reference voltage of master control borad stable output inputs to excitation apparatus after boosting by hardboard.
CN 201320127588 2013-03-20 2013-03-20 Photoelectric direct reading spectrometer Expired - Fee Related CN203241343U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201320127588 CN203241343U (en) 2013-03-20 2013-03-20 Photoelectric direct reading spectrometer

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201320127588 CN203241343U (en) 2013-03-20 2013-03-20 Photoelectric direct reading spectrometer

Publications (1)

Publication Number Publication Date
CN203241343U true CN203241343U (en) 2013-10-16

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CN 201320127588 Expired - Fee Related CN203241343U (en) 2013-03-20 2013-03-20 Photoelectric direct reading spectrometer

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CN (1) CN203241343U (en)

Cited By (4)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103969245A (en) * 2014-05-20 2014-08-06 江苏鑫知源仪器有限公司 Vacuum photoelectric direct-reading spectrometer
CN105302009A (en) * 2014-06-09 2016-02-03 郎溪杰博电器科技有限公司 Measurement control system of fully-digital spectrum analyzer
CN106602886A (en) * 2016-12-30 2017-04-26 杭州谱育科技发展有限公司 Arc excitation circuit and method applied to direct-reading spectrometer
CN109425579A (en) * 2017-09-04 2019-03-05 南京麒麟科学仪器集团有限公司 A kind of photo-electric direct reading spectrometer

Cited By (6)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103969245A (en) * 2014-05-20 2014-08-06 江苏鑫知源仪器有限公司 Vacuum photoelectric direct-reading spectrometer
CN103969245B (en) * 2014-05-20 2016-03-23 江苏鑫知源仪器有限公司 A kind of vacuum photo-electric direct reading spectrometer
CN105302009A (en) * 2014-06-09 2016-02-03 郎溪杰博电器科技有限公司 Measurement control system of fully-digital spectrum analyzer
CN105302009B (en) * 2014-06-09 2019-02-22 郎溪杰博电器科技有限公司 A kind of full digital spectroanalysis instrument Measurement and Control System
CN106602886A (en) * 2016-12-30 2017-04-26 杭州谱育科技发展有限公司 Arc excitation circuit and method applied to direct-reading spectrometer
CN109425579A (en) * 2017-09-04 2019-03-05 南京麒麟科学仪器集团有限公司 A kind of photo-electric direct reading spectrometer

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CF01 Termination of patent right due to non-payment of annual fee
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Granted publication date: 20131016

Termination date: 20170320