CN203183721U - Decompression distillation device for muscone production - Google Patents
Decompression distillation device for muscone production Download PDFInfo
- Publication number
- CN203183721U CN203183721U CN 201320155347 CN201320155347U CN203183721U CN 203183721 U CN203183721 U CN 203183721U CN 201320155347 CN201320155347 CN 201320155347 CN 201320155347 U CN201320155347 U CN 201320155347U CN 203183721 U CN203183721 U CN 203183721U
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- Prior art keywords
- distillation tower
- vacuum distillation
- decompression distillation
- liquid
- phase outlet
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Abstract
Te utility model discloses a decompression distillation device for muscone production. The decompression distillation device comprises three decompression distillation towers, wherein decompression valves and pressure meters are arranged on the three decompression distillation towers, gas-phase outlets and liquid-phase outlets are formed in the tops and the bottoms of the three decompression distillation towers, and material inlets are formed the side walls of all the three decompression distillation towers; the three gas-phase outlets are commonly connected with a vacuum pump, the vacuum pump is connected with a liquid waste cooler, and the liquid waste cooler is connected with a liquid waste collection tank and is arranged at the top of the liquid waste collection tank; the liquid-phase outlet of a first decompression distillation tower is connected with the material inlet of a second decompression distillation tower, the liquid-phase outlet of the second decompression distillation tower is connected with the material inlet of a third decompression distillation tower, the liquid-phase outlet of the third decompression distillation tower is connected with a product collection tank, and a sampler is arranged at the liquid-phase outlet of the third decompression distillation tower. According to the decompression distillation device, the process device is simplified, the production flow is shortened, the input cost of the device is lowered, and the purity of the muscone is greatly improved by carrying out continuous decompression distillation.
Description
Technical field
The utility model relates to muskone production equipment technical field, especially relates to a kind of muskone production vacuum distillation apparatus.
Background technology
Muskone is that the dry secretion Moschus from animal in deer family woods musk deer or the ripe male body note capsule of former musk deer extracts one of active component that obtains through distillation, formal name used at school is 3-methyl cyclopentadecanone, it is the main flavor component of Moschus, muskone is oily liquids, peat-reek is arranged, have resuscitation with aromatics, clearing and activating the channels and collaterals, swelling and pain relieving effect, low dose of have excitation to nervous centralis, and heavy dose then has inhibitory action.To isolated frog heart is dirty excitation is arranged, and the effect of male sex hormone sample and antiinflammatory action are arranged.Be used for coronary disease and angina pectoris, vascular headache, sciatica, leucoderma etc. clinically, have the effect of coronary artery dilator and increase CF, angina pectoris is had certain curative effect.Generally take effect in back 5 minutes in medication (sublingual administration, aerosol suck), the effect of allevating angina pectoris is slightly close with monobel.The pharmacological action of artificial composite after tested, similar to natural musk ketone through test, all need to distill this step of purifying in the artificial synthetic muskone production process, and distillation generally is to carry out in distillation still, but, obtain the higher muskone of purity, then need various other components are separated after by decompression distillation, separated device of the prior art generally is the separator of collecting each component after separating respectively, so just need a plurality of coolers and separator collecting tank, so the production technology production procedure complexity of prior art, equipment investment is big, the production cost height.
The utility model content
Technical problem to be solved in the utility model is: a kind of muskone production vacuum distillation apparatus is provided, the equal separated of waste liquid that produces is to same waste collection jar, simplified process equipment, shortened production procedure, reduction equipment input cost, in addition, through continuous decompression distillation, improved the purity of muskone greatly.
For solving the problems of the technologies described above, the technical solution of the utility model is: muskone production vacuum distillation apparatus, comprise first vacuum distillation tower, second vacuum distillation tower and the 3rd vacuum distillation tower, described first vacuum distillation tower, be equipped with relief valve and Pressure gauge on second vacuum distillation tower and the 3rd vacuum distillation tower, described first vacuum distillation tower, the top of second vacuum distillation tower and the 3rd vacuum distillation tower is equipped with gaseous phase outlet, described first vacuum distillation tower, the bottom of second vacuum distillation tower and the 3rd vacuum distillation tower is equipped with the liquid phase outlet, described first vacuum distillation tower, the sidewall of second vacuum distillation tower and the 3rd vacuum distillation tower is equipped with material inlet, three described gaseous phase outlets are connected with a vavuum pump jointly, described vavuum pump is connected with liquid waste cooler, described liquid waste cooler is connected with the waste collection jar, described liquid waste cooler is arranged at the top of described waste collection jar, the liquid phase outlet of described first vacuum distillation tower connects the material inlet of described second vacuum distillation tower, the liquid phase outlet of described second vacuum distillation tower connects the material inlet of described the 3rd vacuum distillation tower, the liquid phase outlet of described the 3rd vacuum distillation tower is connected with the product collecting tank, and the liquid phase exit of described the 3rd vacuum distillation tower is provided with sampler.
Preferably, the liquid phase exit of described first vacuum distillation tower and second vacuum distillation tower also is provided with sampler.
Adopted technique scheme, the beneficial effects of the utility model are: because muskone production first vacuum distillation tower of vacuum distillation apparatus, the gaseous phase outlet of second vacuum distillation tower and the 3rd vacuum distillation tower is connected with a liquid waste cooler jointly, liquid waste cooler is connected with the waste collection jar, all common separated of other component separators except muskone are to same waste collection jar, simplified process equipment, shortened production procedure, reduction equipment input cost, in addition, the liquid phase outlet of first vacuum distillation tower connects the material inlet of second vacuum distillation tower, the liquid phase outlet of second vacuum distillation tower connects the material inlet of the 3rd vacuum distillation tower, the material inlet of the 3rd vacuum distillation tower is connected with the product collecting tank, through continuous decompression distillation, improved the purity of muskone greatly.
Description of drawings
Fig. 1 is the structural representation of the utility model embodiment;
Wherein: 1, first vacuum distillation tower; 2, second vacuum distillation tower; 3, the 3rd vacuum distillation tower; 4, relief valve; 5, Pressure gauge; 6, liquid waste cooler; 7, waste collection jar; 8, the first vacuum distillation tower material inlet; 9, first vacuum distillation tower liquid phase outlet; 10, the second vacuum distillation tower material inlet; 11, second vacuum distillation tower liquid phase outlet; 12, the 3rd vacuum distillation tower material inlet; 13, the 3rd vacuum distillation tower liquid phase outlet; 14, product collecting tank; 15, sampler; 16, vavuum pump; 17, gaseous phase outlet.
The specific embodiment
Below in conjunction with drawings and Examples the utility model is further specified.
As shown in Figure 1, muskone production vacuum distillation apparatus, comprise first vacuum distillation tower 1, second vacuum distillation tower 2 and the 3rd vacuum distillation tower 3, first vacuum distillation tower 1, be equipped with relief valve 4 and Pressure gauge 5 on second vacuum distillation tower 2 and the 3rd vacuum distillation tower 3, first vacuum distillation tower 1, the top of second vacuum distillation tower 2 and the 3rd vacuum distillation tower 3 is equipped with gaseous phase outlet 17, first vacuum distillation tower 1, the bottom of second vacuum distillation tower 2 and the 3rd vacuum distillation tower 3 is equipped with the liquid phase outlet, first vacuum distillation tower 1, the sidewall of second vacuum distillation tower 2 and the 3rd vacuum distillation tower 3 is equipped with material inlet, three gaseous phase outlets 17 are connected with a vavuum pump 16 jointly, vavuum pump 16 is connected with liquid waste cooler 6, liquid waste cooler 6 is connected with waste collection jar 7, liquid waste cooler 6 is arranged at the top of waste collection jar 7, wherein, the low-purity muskone is entered by the first vacuum distillation tower material inlet 8, first vacuum distillation tower liquid phase outlet 9 connects the second vacuum distillation tower material inlet 10, second vacuum distillation tower liquid phase outlet 11 connects the 3rd vacuum distillation tower material inlet 12, the three vacuum distillation tower liquid phases outlet 13 and is connected with product collecting tank 14.Sampling for convenience, first vacuum distillation tower liquid phase outlet, 9, second vacuum distillation tower liquid phase outlet the 11 and the 3rd vacuum distillation tower liquid phase exports 13 places and is equipped with sampler 15.
All common separated of other component separators except muskone of the utility model are to same waste collection jar 7, simplified process equipment, shortened production procedure, reduction equipment input cost, in addition, through the continuous decompression distillation of first vacuum distillation tower 1, second vacuum distillation tower 2 and the 3rd vacuum distillation tower 3, improved the purity of muskone greatly.
The utility model is not limited to above-mentioned concrete embodiment, and those of ordinary skill in the art is from above-mentioned design, and without performing creative labour, all conversion of having done all drop within the protection domain of the present utility model.
Claims (2)
1. muskone production vacuum distillation apparatus, comprise first vacuum distillation tower, second vacuum distillation tower and the 3rd vacuum distillation tower, described first vacuum distillation tower, be equipped with relief valve and Pressure gauge on second vacuum distillation tower and the 3rd vacuum distillation tower, it is characterized in that, described first vacuum distillation tower, the top of second vacuum distillation tower and the 3rd vacuum distillation tower is equipped with gaseous phase outlet, described first vacuum distillation tower, the bottom of second vacuum distillation tower and the 3rd vacuum distillation tower is equipped with the liquid phase outlet, described first vacuum distillation tower, the sidewall of second vacuum distillation tower and the 3rd vacuum distillation tower is equipped with material inlet, three described gaseous phase outlets are connected with a vavuum pump jointly, described vavuum pump is connected with liquid waste cooler, described liquid waste cooler is connected with the waste collection jar, described liquid waste cooler is arranged at the top of described waste collection jar, the liquid phase outlet of described first vacuum distillation tower connects the material inlet of described second vacuum distillation tower, the liquid phase outlet of described second vacuum distillation tower connects the material inlet of described the 3rd vacuum distillation tower, the liquid phase outlet of described the 3rd vacuum distillation tower is connected with the product collecting tank, and the liquid phase exit of described the 3rd vacuum distillation tower is provided with sampler.
2. muskone production vacuum distillation apparatus as claimed in claim 1 is characterized in that, the liquid phase exit of described first vacuum distillation tower and second vacuum distillation tower also is provided with sampler.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320155347 CN203183721U (en) | 2013-03-29 | 2013-03-29 | Decompression distillation device for muscone production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 201320155347 CN203183721U (en) | 2013-03-29 | 2013-03-29 | Decompression distillation device for muscone production |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN203183721U true CN203183721U (en) | 2013-09-11 |
Family
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Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 201320155347 Expired - Fee Related CN203183721U (en) | 2013-03-29 | 2013-03-29 | Decompression distillation device for muscone production |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN203183721U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113144655A (en) * | 2021-04-28 | 2021-07-23 | 安徽金轩科技有限公司 | Jiale musk rectification unit and rectification process thereof |
-
2013
- 2013-03-29 CN CN 201320155347 patent/CN203183721U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN113144655A (en) * | 2021-04-28 | 2021-07-23 | 安徽金轩科技有限公司 | Jiale musk rectification unit and rectification process thereof |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20130911 Termination date: 20180329 |
|
| CF01 | Termination of patent right due to non-payment of annual fee |