CN202951403U - Production device for decoloring crude product of vitamin B6 - Google Patents

Production device for decoloring crude product of vitamin B6 Download PDF

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Publication number
CN202951403U
CN202951403U CN 201220651896 CN201220651896U CN202951403U CN 202951403 U CN202951403 U CN 202951403U CN 201220651896 CN201220651896 CN 201220651896 CN 201220651896 U CN201220651896 U CN 201220651896U CN 202951403 U CN202951403 U CN 202951403U
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CN
China
Prior art keywords
crude product
cobastab
tubular membrane
filtration system
membrane filtration
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Lifetime
Application number
CN 201220651896
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Chinese (zh)
Inventor
王勇
李新宇
付林
徐勇
王英
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HUAZHONG PHARMACEUTICAL CO Ltd
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HUAZHONG PHARMACEUTICAL CO Ltd
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Priority to CN 201220651896 priority Critical patent/CN202951403U/en
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Abstract

The utility model provides a production device for decoloring a crude product of vitamin B6. The production device is characterized by comprising a tubular membrane filtering system, wherein the tubular membrane filtering system comprises an ultrafiltration membrane core arranged inside the tubular membrane filtering system, a decoloring stock solution feed port formed in one end of the ultrafiltration membrane core, a concentrated solution discharge port formed in the other end of the ultrafiltration membrane core, and a decoloring solution discharge port formed in the outer layer of the tubular membrane filtering system. By using the production device, the decoloring efficiency is improved, the production cycle is shortened, the stability of the product quality is good, the labor intensity is reduced, and the utilization rate of equipment is high.

Description

A kind of for Cobastab 6The process units of crude product decolouring
Technical field
The utility model relates to the vitamin production technical field, particularly a kind of for Cobastab 6The process units of crude product decolouring.
Background technology
Cobastab 6(Vitamin B 6) claim again pyridoxine, be a kind of water soluble vitamin, be white crystal, soluble in water and ethanol, stable in acid solution, meet light or alkali destructible, non-refractory.Cobastab 6In saccharomycete, liver, grain, meat, fish, egg, beans and peanut, content is more, is the constituent of some coenzyme in human body, participates in multiple metabolic response, especially with amino acid metabolism, substantial connection is arranged.Apply clinically Cobastab 6The preparation control vomiting of pregnancy and radiation sickness vomiting.
At present, industrial common employing chemical synthesis is produced Cobastab 6, the process route of realizing suitability for industrialized production has two kinds of pyridone method and oxazole methods." pyridone method " is that early stage industry adopts, and because of defects such as step are long, yield is low, equipment corrosion is serious, is leveraged to the sixties in 20th century afterwards, by " oxazole method ", replaced gradually.
Because the reaction temperature of oxazole operation is higher, cause producing the more impurity such as tar, the Cobastab of production 6The crude product color is darker, needs could remove through 2-3 activated carbon decolorizing, and traditional handicraft is carried out in reactor, Cobastab 6Add appropriate active carbon in crude product solution, after the mechanical agitation certain hour, blowing is through the centrifuge decarburization, and filtrate is so repeatedly decoloured and repeatedly just can be reached requirement again.
Yet, the mode of production like this, be difficult to ensure colored foreign and reach fully and remove at short notice, thus under this kind of mode of production 2-3 time even repeatedly repetitive operation be unavoidable, there is long, the shortcoming such as utilization rate of equipment and installations is low of cycle, and increased Cobastab 6The risk that crude product is rotten.Make like this competitiveness of product in market descend.
Summary of the invention
The technical problem that the utility model solves is to provide a kind of for Cobastab 6The process units of crude product decolouring, improve decolorizing efficiency, shortens the production cycle, and constant product quality is good.
It is a kind of for Cobastab that the utility model provides 6The process units of crude product decolouring, it comprises: the tubular membrane filtration system, described tubular membrane filtration system comprises:
Be arranged on the milipore filter core of described tubular membrane filtration system inside; And
Be arranged on the decolouring stoste charging aperture of described milipore filter core one end;
Be arranged on the concentrate discharging opening of the described milipore filter core other end;
Be arranged on the outer field destainer discharging opening of described tubular membrane filtration system.
Further, described a kind of for Cobastab 6The process units of crude product decolouring also comprises:
Reactor for activated carbon decolorizing;
And pass through channel attached centrifuge between described reactor; And
Pass through respectively channel attached circulating pump with described centrifuge, tubular membrane filtration system.
Further, described a kind of for Cobastab 6The process units of crude product decolouring, also comprise: the transfer tank of depositing concentrate;
Further, between described transfer tank and circulating pump, by passage, be connected;
Further, described transfer tank comprises purified water inlet.
The utility model is a kind of for Cobastab 6The process units of crude product decolouring, by the milipore filter core of tubular membrane filtration system, the Cobastab in the stoste of once decolouring 6, water etc. sees through milipore filter, the large molecule such as foreign pigment is retained in concentrate, has improved decolorizing efficiency, shortens the production cycle, constant product quality is good, and has reduced labour intensity, utilization rate of equipment and installations is higher.
The accompanying drawing explanation
Fig. 1 is that the utility model is a kind of for Cobastab 6One preferred embodiment schematic diagram of the process units of crude product decolouring.
The specific embodiment
Below in conjunction with drawings and Examples, the utility model is elaborated.
Refer to Fig. 1, it is that the utility model is a kind of for Cobastab 6One preferred embodiment schematic diagram of the process units of crude product decolouring.
It is a kind of for Cobastab that the utility model provides 6The process units of crude product decolouring, it comprises: tubular membrane filtration system 4, described tubular membrane filtration system 4 comprises:
Be arranged on the milipore filter core 43 of described tubular membrane filtration system 4 inside; And
Be arranged on the decolouring stoste charging aperture 41 of described milipore filter core 43 1 ends;
Be arranged on the concentrate discharging opening 42 of described milipore filter core 43 other ends;
Be arranged on the outer field destainer discharging opening 44 of described tubular membrane filtration system 4.
Further, described a kind of for Cobastab 6The process units of crude product decolouring also comprises:
Reactor 1 for activated carbon decolorizing;
And pass through channel attached centrifuge 2 between described reactor; And
Pass through respectively channel attached circulating pump 3 with described centrifuge 2, tubular membrane filtration system 4.
Further, described a kind of for Cobastab 6The process units of crude product decolouring, also comprise: the transfer tank 5 of depositing concentrate;
Further, between described transfer tank 5 and circulating pump 3, by passage, be connected;
Further, described transfer tank comprises purified water inlet 51.
The utility model is a kind of for Cobastab 6The workflow of the process units of crude product decolouring is as described below:
By the Cobastab measured 6Crude product solution, active carbon are placed in decoloring reaction still 1, and after the mechanical agitation certain hour, blowing is through centrifuge 2 decarburizations, and filtrate enters the decolouring stoste entrance 41 of tubular membrane filtration system 4, the Cobastab in stoste through circulating pump 3 6, most water can see through milipore filter core 43 and discharge by the outer field destainer outlet 44 of tubular membrane filtration system 4, enter subsequent handling and obtain Cobastab 6Finished product.The concentrate do not seen through enters transfer tank 5 through concentrated solution outlet 42, after adding appropriate pure water dilution by purified water inlet 51, then enters the decolouring stoste entrance 41 of tubular membrane filtration system 4 through circulating pump 3, and circulating filtration to destainer exports the sampling of 44 places and surveys Cobastab 6Content during lower than certain value till.
In the above-described embodiments, only the utility model has been carried out to exemplary description, but those skilled in the art carry out various modifications in the situation that can or else break away from spirit and scope of the present utility model after reading present patent application to the utility model.

Claims (5)

1. one kind for Cobastab 6The process units of crude product decolouring, is characterized in that comprising tubular membrane filtration system (4), and described tubular membrane filtration system (4) comprising:
Be arranged on the inner milipore filter core (43) of described tubular membrane filtration system (4); And
Be arranged on the decolouring stoste charging aperture (41) of described milipore filter core (43) one ends;
Be arranged on the concentrate discharging opening (42) of described milipore filter core (43) other end;
Be arranged on the outer field destainer discharging opening of described tubular membrane filtration system (4) (44).
2. according to claim 1 a kind of for Cobastab 6The process units of crude product decolouring, is characterized in that: also comprise the reactor (1) for activated carbon decolorizing;
And pass through channel attached centrifuge (2) between described reactor; And
Pass through respectively channel attached circulating pump (3) with described centrifuge (2), tubular membrane filtration system (4).
3. according to claim 1 and 2 a kind of for Cobastab 6The process units of crude product decolouring, is characterized in that: also comprise the transfer tank (5) of depositing concentrate.
4. according to claim 3 a kind of for Cobastab 6The process units of crude product decolouring is characterized in that: between described transfer tank (5) and circulating pump (3), by passage, be connected.
5. described a kind of for Cobastab according to claim 3 or 4 6The process units of crude product decolouring, it is characterized in that: described transfer tank (5) comprises purified water inlet (51).
CN 201220651896 2012-12-03 2012-12-03 Production device for decoloring crude product of vitamin B6 Expired - Lifetime CN202951403U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN 201220651896 CN202951403U (en) 2012-12-03 2012-12-03 Production device for decoloring crude product of vitamin B6

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 201220651896 CN202951403U (en) 2012-12-03 2012-12-03 Production device for decoloring crude product of vitamin B6

Publications (1)

Publication Number Publication Date
CN202951403U true CN202951403U (en) 2013-05-29

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN 201220651896 Expired - Lifetime CN202951403U (en) 2012-12-03 2012-12-03 Production device for decoloring crude product of vitamin B6

Country Status (1)

Country Link
CN (1) CN202951403U (en)

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Granted publication date: 20130529

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