CN202044809U - Plant active ingredient multistage continuation automatic percolation extraction system - Google Patents
Plant active ingredient multistage continuation automatic percolation extraction system Download PDFInfo
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- CN202044809U CN202044809U CN2011201078541U CN201120107854U CN202044809U CN 202044809 U CN202044809 U CN 202044809U CN 2011201078541 U CN2011201078541 U CN 2011201078541U CN 201120107854 U CN201120107854 U CN 201120107854U CN 202044809 U CN202044809 U CN 202044809U
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Abstract
The utility model relates to a plant active ingredient multistage continuation automatic percolation extraction system comprising an automatic control system, at least three groups of percolation tank components, a heat exchanger, a storage tank, an oil-water separator, a cooler and a condenser. Each percolation tank component comprises a percolation tank for containing plants. In each percolation tank component, a hot water inlet of the middle lower part of the percolation tank is connected with a hot water inlet pipe, a hot water outlet of the middle upper part of the percolation tank is connected with a hot water return pipe, a menstruum inlet of the upper end part of the percolation tank is sequentially connected with a first timing linkage control valve, a delivery pump, a timing adjusting valve and a menstruum outlet of the heat exchanger, an outlet of the delivery pump is also connected with an extraction liquid discharge pipe through a second timing linkage control valve, a liquid discharge port of the bottom of the percolation tank is connected with a steam pipe through a third timing control valve, the outlet of the bottom of the percolation tank is also connected with an inlet of the delivery pump in another percolation tank component through a liquid level control valve, and a steam outlet of the top part of the percolation tank is connected with the inlet of the condenser.
Description
Technical field
The utility model relates to the multistage continuously automatic diacolation extraction system of a kind of effective ingredients in plant.
Background technology
Existing effective ingredients in plant extraction system, solvent load is more, energy consumption was higher when extract concentrated.Therefore how to provide that a kind of solvent load is less, the lower effective ingredients in plant extraction system of energy consumption when extract concentrates, be the technical problem that this area will solve.
The utility model content
The technical problems to be solved in the utility model provide a kind of simple in structure, solvent load is less and the multistage diacolation extraction system automatically continuously of the extract effective ingredients in plant that energy consumption is lower when concentrating.
In order to solve the problems of the technologies described above, the utility model provides a kind of effective ingredients in plant multistage continuously automatically diacolation extraction system, comprising: on automatic control system, at least three group diacolation canister assemblies, the heat exchanger that is used to heat solvent, the basin that is used to store solvent that links to each other with the solvent inlet of heat exchanger, the solvent of being located at the basin top enter the mouth be used for solvent and moisture from oil water separator, be located at cooler on the entry to mixed solution on oil water separator top, be located at the condenser on the entry to mixed solution on cooler top.
Each diacolation canister assembly comprises the diacolation jar that is used to hold plant, in each diacolation canister assembly: the hot water inlet of the middle and lower part of diacolation jar links to each other with the hot water inlet pipe, the hot water outlet of the middle and upper part of diacolation jar links to each other with the hot water return pipe, the solvent inlet of the upper end of diacolation jar links to each other with the solvent outlet of heat exchanger through the chain control valve of first timing, delivery pump, valve timing regulation successively, and this carries delivery side of pump also to link to each other with the extract discharge pipe through the chain control valve of second timing; The leakage fluid dram of diacolation pot bottom links to each other with steam pipe through the 3rd timing control valve, and the outlet of the diacolation pot bottom also inlet of the delivery pump in fluid level control valve and another diacolation canister assembly links to each other; The steam (vapor) outlet of diacolation tank top links to each other with the inlet of described condenser.
The extracting system that described extract discharge pipe and is used for separating plant active ingredient and solvent links to each other; Regularly chain control valve, the chain control valve of second timing, the 3rd timing control valve, valve timing regulation, fluid level control valve link to each other with delivery pump described automatic control system with described first.
The cooling water inlet of described condenser and cooler links to each other with the cooling water inlet pipe, and the coolant outlet of condenser and cooler links to each other with the cooling water return pipe.
Described solvent is generally gasoline, alcohol etc.Hot water temperature in the hot water inlet pipe according to different effective ingredients in plant in corresponding solvent solubility and the relation of temperature decide.When adopting alcohol as solvent, this diacolation extraction system need not to adopt oil water separator, and cooler directly links to each other with basin.
The method of work of the multistage continuously automatic diacolation extraction system of above-mentioned effective ingredients in plant comprises: exist first, second two groups of diacolation canister assemblies to constitute series connection at least, and carry out diacolation and extract; There is the 3rd a diacolation canister assembly that is in closed condition simultaneously, is used to replace standby; When the concentration that records the active ingredient in the extract of the first diacolation canister assembly by ultraviolet detector when automatic control system is lower than preset value, close the described first diacolation canister assembly, open the 3rd diacolation canister assembly; At this moment, second, third two groups of diacolation canister assemblies constitute series connection, and carry out diacolation and extract; Simultaneously, the quantitative vapours of input in the diacolation jar of the first diacolation canister assembly so that solvent in the diacolation jar and water evaporation, and escapes and enter a condenser from the steam (vapor) outlet of diacolation tank top; In the diacolation jar of the first diacolation canister assembly, add new plant material then; When the concentration of the active ingredient in the extract that records the described second diacolation canister assembly is lower than preset value, close the second diacolation canister assembly, open the first diacolation canister assembly, in the diacolation jar of the second diacolation canister assembly, import quantitative vapours simultaneously, so that solvent in the diacolation jar and water evaporation, and escape and enter described condenser from the steam (vapor) outlet of diacolation tank top, in the diacolation jar of the second diacolation canister assembly, add new plant material then; When the concentration of the active ingredient in the extract that records described the 3rd diacolation canister assembly is lower than preset value, close the 3rd diacolation canister assembly, open the second diacolation canister assembly, in the diacolation jar of the 3rd diacolation canister assembly, import quantitative vapours simultaneously, so that solvent in the diacolation jar and water evaporation, and escape and enter described condenser from the steam (vapor) outlet of diacolation tank top, in the diacolation jar of the 3rd diacolation canister assembly, add new plant material then; So repeatedly.
Wherein, the condensate liquid of described condenser output is sent into the basin that is used to store solvent successively behind cooler, oil water separator, and basin only provides the thermosol matchmaker to each the diacolation canister assembly that is in series connection through heat exchanger.
Technique scheme of the present utility model has the following advantages compared to existing technology: in the multistage continuously automatic diacolation extraction system of (1) effective ingredients in plant of the present utility model, adopt multistage diacolation to dispose pump and flow control mode respectively, avoid the hypertonia of single pump; (2) position of the liquid level detector on the diafiltration jar is associated with flow-control; (3) course of work of native system, have that diacolation extracts thoroughly, automaticity is higher, solvent load is less and extract when concentrating energy consumption lower characteristics.Simultaneously, can fully reclaim solvent, to save cost.
Description of drawings
For the easier quilt of content of the present utility model is clearly understood, below the specific embodiment and in conjunction with the accompanying drawings of basis, the utility model is described in further detail, wherein
Fig. 1 is the structural representation of the multistage continuously automatic diacolation extraction system of effective ingredients in plant of the present utility model.
The specific embodiment
See Fig. 1, the multistage continuously automatically diacolation extraction system of the effective ingredients in plant of present embodiment comprises: on automatic control system, at least three group diacolation canister assemblies, the heat exchanger 1 that is used to heat solvent, the basin 2 that is used to store solvent that links to each other with the solvent inlet of heat exchanger 1, the solvent of being located at basin 2 tops enter the mouth be used for solvent and moisture from oil water separator 3, be located at cooler 4 on the entry to mixed solution on oil water separator 3 tops, be located at the condenser 5 on the entry to mixed solution on cooler 4 tops.
Each diacolation canister assembly comprises the diacolation jar S that is used to hold plant, in each diacolation canister assembly: the hot water inlet of the middle and lower part of diacolation jar S links to each other with the hot water inlet pipe, the hot water outlet of the middle and upper part of diacolation jar S links to each other with the hot water return pipe, the solvent inlet of the upper end of diacolation jar S links to each other with the solvent outlet of heat exchanger 1 through first timing chain control valve F1, the delivery pump M1, valve timing regulation F4 successively, and the outlet of this delivery pump M1 also links to each other with the extract discharge pipe through the chain control valve F2 of second timing; The leakage fluid dram of diacolation jar S bottom links to each other with steam pipe through the 3rd timing control valve F3, and the outlet of the diacolation pot bottom also inlet of the delivery pump in fluid level control valve F5 and another diacolation canister assembly links to each other; The steam (vapor) outlet at diacolation jar S top links to each other with the inlet of described condenser 5.
The extracting system that described extract discharge pipe and is used for separating plant active ingredient and solvent links to each other; Regularly chain control valve F1, the chain control valve F2 of second timing, the 3rd timing control valve F3, valve timing regulation F4, fluid level control valve F5's described automatic control system link to each other with delivery pump M1 with described first.
The cooling water inlet of described condenser 5 and cooler 4 links to each other with the cooling water inlet pipe, and the coolant outlet of condenser 5 and cooler 4 links to each other with the cooling water return pipe.
During work, under the effect of automatic control system, open described first, second diacolation canister assembly, close the 3rd diacolation canister assembly simultaneously, that is: in the first diacolation canister assembly: the chain control valve F2 of described second timing closes, valve timing regulation F4 opens, the solvent of heat exchanger 1 is sent into diacolation jar S through valve timing regulation F4, delivery pump M1 and the chain control valve F1 of first timing successively, open the 3rd timing control valve F3 simultaneously so that the solvent among the diacolation jar S is heated to design temperature, the liquid level among the fluid level control valve F5 control diacolation jar S is to preset height; In the second diacolation canister assembly: valve timing regulation and second regularly chain control valve is closed, delivery pump will be sent into the diacolation jar through the chain control valve of first timing from the mixed liquor of the first diacolation canister assembly, open the 3rd timing control valve F3 simultaneously so that the solvent among the diacolation jar S is heated to design temperature, the liquid level among the fluid level control valve F5 control diacolation jar S is to preset height; In the 3rd diacolation canister assembly: the described second regularly chain control valve F2 opens, and valve timing regulation F4 closes, and delivery pump will be sent into the extract discharge pipe through the chain control valve of second timing from the mixed liquor of the second diacolation canister assembly.
During work, exist first, second two groups of diacolation canister assemblies to constitute series connection at least, extract to carry out diacolation; Exist one to replace the 3rd diacolation canister assembly of usefulness simultaneously.When the concentration that records the active ingredient in the extract of the first diacolation canister assembly by ultraviolet detector when automatic control system is lower than preset value, close the described first diacolation canister assembly, open the 3rd diacolation canister assembly; At this moment, second, third two groups of diacolation canister assemblies constitute series connection, in the diacolation jar of the first diacolation canister assembly, import quantitative vapours simultaneously, so that solvent in the diacolation jar and water evaporation, and escape and enter described condenser from the steam (vapor) outlet of diacolation tank top, in the diacolation jar of the first diacolation canister assembly, add new plant material then; When the concentration of the active ingredient in the extract that records the second diacolation canister assembly is lower than preset value, close the described second diacolation canister assembly, open the first diacolation canister assembly, in the diacolation jar of the second diacolation canister assembly, import quantitative vapours simultaneously, so that solvent in the diacolation jar and water evaporation, and escape and enter described condenser from the steam (vapor) outlet of diacolation tank top, in the diacolation jar of the second diacolation canister assembly, add new plant material then; When the concentration of the active ingredient in the extract that records the 3rd diacolation canister assembly is lower than preset value, close described the 3rd diacolation canister assembly, open the second diacolation canister assembly, in the diacolation jar of the 3rd diacolation canister assembly, import quantitative vapours simultaneously, so that solvent in the diacolation jar and water evaporation, and escape and enter described condenser from the steam (vapor) outlet of diacolation tank top, in the diacolation jar of the 3rd diacolation canister assembly, add new plant material then; So repeatedly.
This process has the thorough and higher characteristics of automaticity that diacolation extracts.Simultaneously, can fully reclaim solvent, to save cost.
Obviously, the foregoing description only is for the utility model example clearly is described, and is not to be qualification to embodiment of the present utility model.For those of ordinary skill in the field, can also make other changes in different forms on the basis of the above description.Here need not also can't give exhaustive to all embodiments.And these belong to conspicuous variation or the change that spirit of the present utility model extended out and still are among the protection domain of the present utility model.
Claims (2)
1. the multistage diacolation extraction system automatically continuously of an effective ingredients in plant is characterized in that comprising: on automatic control system, at least three group diacolation canister assemblies, the heat exchanger (1) that is used to heat solvent, the basin that is used to store solvent (2) that links to each other with the solvent inlet of heat exchanger (1), the solvent of being located at basin (2) top enter the mouth be used for solvent and moisture from oil water separator (3), be located at cooler (4) on the entry to mixed solution on oil water separator (3) top, be located at the condenser (5) on the entry to mixed solution on cooler (4) top;
Each diacolation canister assembly comprises the diacolation jar (S) that is used to hold plant, in each diacolation canister assembly: the hot water inlet of the middle and lower part of diacolation jar (S) links to each other with the hot water inlet pipe, the hot water outlet of the middle and upper part of diacolation jar (S) links to each other with the hot water return pipe, the solvent inlet of the upper end of diacolation jar (S) links to each other with the solvent outlet of heat exchanger (1) through the first timing chain control valve (F1), delivery pump (M1), valve timing regulation (F4) successively, and the outlet of this delivery pump (M1) also links to each other with the extract discharge pipe through the second chain control valve of timing (F2); The leakage fluid dram of diacolation jar (S) bottom links to each other with steam pipe through the 3rd timing control valve (F3), and the outlet of the diacolation pot bottom also inlet of the delivery pump in fluid level control valve (F5) and another diacolation canister assembly links to each other; The steam (vapor) outlet at diacolation jar (S) top links to each other with the inlet of described condenser (5);
The extracting system that described extract discharge pipe and is used for separating plant active ingredient and solvent links to each other;
Regularly chain control valve (F1), the second timing chain control valve (F2), the 3rd timing control valve (F3), valve timing regulation (F4), fluid level control valve (F5) link to each other with delivery pump (M1) described automatic control system with described first.
2. the multistage continuously automatic diacolation extraction system of effective ingredients in plant according to claim 1, it is characterized in that: the cooling water inlet of described condenser (5) and cooler (4) links to each other with the cooling water inlet pipe, and the coolant outlet of condenser (5) and cooler (4) links to each other with the cooling water return pipe.
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CN2011201078541U CN202044809U (en) | 2011-04-13 | 2011-04-13 | Plant active ingredient multistage continuation automatic percolation extraction system |
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CN2011201078541U CN202044809U (en) | 2011-04-13 | 2011-04-13 | Plant active ingredient multistage continuation automatic percolation extraction system |
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Cited By (3)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102205185A (en) * | 2011-04-13 | 2011-10-05 | 陆文光 | Multistage continuous automatic percolation extraction system for effective ingredients of plants and working method thereof |
CN104186709A (en) * | 2014-06-16 | 2014-12-10 | 无穷食品有限公司 | Preparation device and preparation method of edible seasoning oil |
CN110270128A (en) * | 2019-07-29 | 2019-09-24 | 湖南正清制药集团股份有限公司 | Extract the heavy diacolation tele-control system and method for cucoline |
-
2011
- 2011-04-13 CN CN2011201078541U patent/CN202044809U/en not_active Expired - Lifetime
Cited By (5)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN102205185A (en) * | 2011-04-13 | 2011-10-05 | 陆文光 | Multistage continuous automatic percolation extraction system for effective ingredients of plants and working method thereof |
CN102205185B (en) * | 2011-04-13 | 2013-01-09 | 陆文光 | Multistage continuous automatic percolation extraction system for effective ingredients of plants and working method thereof |
CN104186709A (en) * | 2014-06-16 | 2014-12-10 | 无穷食品有限公司 | Preparation device and preparation method of edible seasoning oil |
CN110270128A (en) * | 2019-07-29 | 2019-09-24 | 湖南正清制药集团股份有限公司 | Extract the heavy diacolation tele-control system and method for cucoline |
CN110270128B (en) * | 2019-07-29 | 2022-03-18 | 湖南正清制药集团股份有限公司 | Percolation remote control system and method for extracting sinomenine |
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C14 | Grant of patent or utility model | ||
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AV01 | Patent right actively abandoned |
Granted publication date: 20111123 Effective date of abandoning: 20130306 |
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RGAV | Abandon patent right to avoid regrant |