CN201744350U - Inorganic substance hydrothermal method synthesizer - Google Patents
Inorganic substance hydrothermal method synthesizer Download PDFInfo
- Publication number
- CN201744350U CN201744350U CN2010202285775U CN201020228577U CN201744350U CN 201744350 U CN201744350 U CN 201744350U CN 2010202285775 U CN2010202285775 U CN 2010202285775U CN 201020228577 U CN201020228577 U CN 201020228577U CN 201744350 U CN201744350 U CN 201744350U
- Authority
- CN
- China
- Prior art keywords
- reactor
- hydrothermal method
- inorganic matter
- synthesizing inorganic
- heating
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Expired - Fee Related
Links
Abstract
The utility model relates to an inorganic substance hydrothermal method synthesizer, comprising a reactor; the reactor is internally provided with stirring devices and a heating temperature-control device, the top of the outer surface of the reactor is provided with a material inlet and a water inlet, and the bottom of the reactor is provided with a water outlet. The inorganic substance hydrothermal method synthesizer adopts two stirring devices to lead the stirring to be more uniform, adopts the heating temperature-control device to lead the heating or cooling to be more uniform, is simple and convenient in processing and installing, is safe in use, can synthesize large amount of homogeneous nano inorganic particles, is more convenient and efficient for separation and purification operation, can be widely applied in practical production of chemical products such as organic substances, inorganic substances, medicines, biochemistry and the like and has good market prospect.
Description
Technical field
The utility model relates to a kind of nm inorganic compound synthetic technology, especially relates to a kind of device for synthesizing inorganic matter by hydrothermal method.
Background technology
Hydro-thermal method is geologist's simulating nature circle mineralization and beginning one's study in the middle of the 19th century.Post-science men had set up the hydro-thermal blending theory in 1900, began to turn to the research of functional material later on again, had prepared over one hundred kind of crystal with hydro-thermal method at present.In the crystal study on the synthesis, adopt high-temperature and high-pressure conditions to carry out usually.At present this method has been widely used in the nano inorganic material technical process, carrying out nano inorganic material requirement condition gentleness when synthetic, need not high-temperature and high-pressure conditions.
Hydro-thermal method as the preparation powder body material in the prior art has been used to synthesizing superfine and different in nature powder, for example materials such as new ceramics, crystal, composite oxides.For the global design of high-temperature high-pressure anti-corrosive erosion hydrothermal reactor, mainly consider the sticking wall of powder granule in the viscosity of mode of heating, thermal conductivity factor, slurries and the slurries etc.Primary structure form as the liquid phase water thermal reactor.Less demanding for reaction condition, but to the demanding powder body material preparation of grain fineness, heat-transfer rate, the hot homogeneity of course of reaction is exactly one of major requirement of reactor.
More about the reactor design of HTHP hydro-thermal method at present, for example, a kind of tubular type high-temperature high pressure water thermic devices, carried out the hydro-thermal reaction of alkali magnesium sulfate crystal whisker greatly with it, temperature in the pipe can be controlled at 180～200 ℃, 6 hours hydro-thermal time, obtain the high-quality alkali magnesium sulfate crystal whisker of needle-like pattern.This kind structure of reactor complexity, the cost of manufacture height is fit to the high-temperature high pressure water thermal process, is fit to the preparation of inorganic material crystal, is not suitable for the synthetic production of nano particle.Also have a kind of novel reaction kettle, adopted double-deck heater and heat-transfer pipe, material heating or cooling are not more had hand over rapid, but do not design the separator of synthetic product, make end of synthesis afterproduct purifying and separation difficulty.
Summary of the invention
Technical problem to be solved in the utility model provides a kind of device for synthesizing inorganic matter by hydrothermal method, and this apparatus structure is simple, is suitable for the synthetic production of nano particle, and homogeneous heating makes things convenient for the purifying and the separation of product.
The technical scheme in the invention for solving the technical problem is: a kind of device for synthesizing inorganic matter by hydrothermal method, comprise reactor, be provided with agitating device and heating and temperature controlling device at inside reactor, the outer surface top of reactor is provided with charging aperture and water inlet, and the bottom is provided with delivery port.
Clean for convenience and maintenance, described reactor is dismountable two parts up and down, and its outer surface also is provided with the dismounting valve.
Described reactor is an elliposoidal, and its inner major diameter than length to height ratio is: 1.618: 1.The top volume of described reactor accounts for 85%～95% of cumulative volume.
For raw material can fully be mixed, described agitating device has two and horizontal positioned, and two agitating devices can stir in the same way also and can oppositely stir.
For the better controlled temperature, described temperature control heating device is between two horizontal agitating devices.
Draining for convenience, water inlet and reinforced, water inlet links to each other with the hollow pipe that has shower nozzle in the inside of reactor.Described delivery port is positioned at reactor bottom 5～15cm place.
The utility model has the advantages that: adopt two agitating devices, stirring more even adopts heating and temperature controlling device, make heating or cooling more even, the processing simple installation, safe in utilization, can synthesize homogeneous nano inorganic particle in a large number, the separation and purification operation is more convenient efficient.Can be widely used in organicly, inorganic, medicine during the practice of chemical products such as biochemistry is produced, has good market prospects.
Description of drawings
Fig. 1 is a profilograph of the present utility model.
1, reactor 2, agitating device 3, heating and temperature controlling device 4, charging aperture 5, water inlet 6, delivery port 7, dismounting valve
The specific embodiment
As shown in Figure 1, the utility model device mainly by reactor 1 (providing reaction synthetic place), is the ellipsoid shape, helps stirring, and is unfavorable for that synthetic product attached in the reactor, can improve efficiency of pcr product; Heating and temperature controlling device 3 (the reaction heating is provided), this device is preferably straight tube, the convenient installation, and minimizing takies space in the tank body; Agitating device 2 (providing heating heat decentralized system and reaction low thing mixing parts), be divided into two mixing parts up and down, as Fig. 1 profile, be positioned on the same cross section, can stir in the same way, form eddy current but preferably oppositely stir, so not only help the reaction substrate contact, and can make uniform heat distribution, make sufficient reacting, the product homogeneous; Be used to add the charging aperture 4 of each reaction substrate, this type of mouthful can make one to several according to reaction type and reaction substrate kind, and for convenience of application of sample, charging aperture all is arranged at the top; Be used to react and wash the water inlet 5 of usefulness, this mouth is positioned at reactor 1 top, preferably injects in the sprinkling irrigation mode, helps the product washing so evenly; Delivery port 6 is used for reaction waste and product washing wastewater outlet, is positioned at 5-15cm place, tank body bottom, and this helps reaction waste and washes the discharging of waste water and do not drive the flow losses of product.For better separation and purification, this reactor 1 design is divided into two parts up and down, and detachable the separation, help product like this and separate, avoid sticking in the jar.
Provide a kind of embodiment that uses this device to produce trivalent silver iron below:
For this contrive equipment synthesis capability is described, carried out the synthetic trivalent silver iron compound (silver sesquioxide) of this device of following application, take by weighing 2400g potassium peroxydisulfate and 48g NaOH, add in the reactor 1 by charging aperture 4, add water 10L by water inlet 5 again, start heating and temperature controlling device 3 and agitating device 2, be warming up to 85 ℃, add the 140g Tetrasilver tetroxides mixing that rolls by charging aperture 4,85 ℃ of insulation 30min, and with pure water rinsing four times, discharge by delivery port 6,, obtain trivalent silver iron product (silver sesquioxide) 132.3 grams to remove potassium sulfate (sodium) and potassium nitrate (sodium) and other impurity, synthetic yield is 88.8%, and trivalent silver granular size is about 50nm.
Claims (8)
1. device for synthesizing inorganic matter by hydrothermal method, it is characterized in that: comprise reactor (1), be provided with agitating device (2) and heating and temperature controlling device (3) in reactor (1) inside, the outer surface top of reactor (1) is provided with charging aperture (4) and water inlet (5), and the bottom is provided with delivery port (6).
2. device for synthesizing inorganic matter by hydrothermal method according to claim 1 is characterized in that: described reactor (1) is dismountable two parts up and down, and its outer surface also is provided with dismounting valve (7).
3. device for synthesizing inorganic matter by hydrothermal method according to claim 1 is characterized in that: described reactor (1) is an elliposoidal, and its inner major diameter than length to height ratio is: 1.618: 1.
4. device for synthesizing inorganic matter by hydrothermal method according to claim 2 is characterized in that: the top volume of described reactor (1) accounts for 85%～95% of cumulative volume.
5. device for synthesizing inorganic matter by hydrothermal method according to claim 1 is characterized in that: described agitating device (2) has two and horizontal positioned.
6. device for synthesizing inorganic matter by hydrothermal method according to claim 1 is characterized in that: described temperature control heating device (3) is positioned between the two horizontal agitating devices (2).
7. device for synthesizing inorganic matter by hydrothermal method according to claim 1 is characterized in that: described water inlet (5) links to each other with the hollow pipe that has shower nozzle in the inside of reactor (1).
8. device for synthesizing inorganic matter by hydrothermal method according to claim 1 is characterized in that: described delivery port (5) is positioned at 5～15cm place, reactor (1) bottom.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010202285775U CN201744350U (en) | 2010-06-18 | 2010-06-18 | Inorganic substance hydrothermal method synthesizer |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN2010202285775U CN201744350U (en) | 2010-06-18 | 2010-06-18 | Inorganic substance hydrothermal method synthesizer |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN201744350U true CN201744350U (en) | 2011-02-16 |
Family
ID=43579023
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN2010202285775U Expired - Fee Related CN201744350U (en) | 2010-06-18 | 2010-06-18 | Inorganic substance hydrothermal method synthesizer |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN201744350U (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101844066A (en) * | 2010-06-18 | 2010-09-29 | 苏州邦安新材料科技有限公司 | Device for synthesizing inorganic matter by hydrothermal method and using method thereof |
-
2010
- 2010-06-18 CN CN2010202285775U patent/CN201744350U/en not_active Expired - Fee Related
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101844066A (en) * | 2010-06-18 | 2010-09-29 | 苏州邦安新材料科技有限公司 | Device for synthesizing inorganic matter by hydrothermal method and using method thereof |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN103935962B (en) | A kind of supercritical water thermal synthesis preparation system of nano-metal-oxide | |
| CN106807317A (en) | A kind of reaction unit for disperseing to mix battery material | |
| CN204122112U (en) | A kind of hydro-thermal method prepares the reactor of superhigh intensity αsemiwatergypsum fast | |
| CN201744350U (en) | Inorganic substance hydrothermal method synthesizer | |
| CN204816416U (en) | Acryl resin preparation facilities with adjustable | |
| CN101333268A (en) | Reactor for EPS | |
| CN206810267U (en) | A kind of scattered reaction unit for mixing battery material | |
| CN206500147U (en) | A kind of reactor fast cooling device of Hydrothermal Synthesiss titanium dioxide nano material | |
| CN101844066A (en) | Device for synthesizing inorganic matter by hydrothermal method and using method thereof | |
| CN200958082Y (en) | Continuous producer of alpha-half-hydrate gypsum | |
| CN102897823B (en) | Preparation device and process of CeO2 powder by supercritical water system oxidation | |
| CN206392065U (en) | A kind of Titanium series catalyst preparation facilities | |
| CN206935357U (en) | A kind of chemical reaction kettle | |
| CN110841585A (en) | Benzyl cyanide production device and use method thereof | |
| CN206981312U (en) | A kind of high-efficiency quartz sand cleaning device | |
| CN205084682U (en) | Preparation oil gas field anti -corrosion paint's reaction unit | |
| CN201729786U (en) | Expandable polystyrene reaction kettle | |
| CN109264759B (en) | Reaction furnace | |
| CN202951474U (en) | Conical bottom surface stirring reaction kettle | |
| CN211471264U (en) | Benzyl cyanide apparatus for producing | |
| CN201276514Y (en) | Reactor for expansible polystyrene | |
| CN207641446U (en) | A kind of synthetic system | |
| CN207659508U (en) | A kind of level tandem short route refining bismuth device | |
| CN205761059U (en) | A kind of isomerization reaction device continuously | |
| CN106622030B (en) | A kind of vertical decompression cycles chemical reaction equipment |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: SUZHOU TNY SANJIA NANOMETER TECHNOLOGY CO., LTD. Free format text: FORMER OWNER: JIANGSU BANG'AN NEW MATERIALS TECHNOLOGY CO., LTD. Effective date: 20130402 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 215122 SUZHOU, JIANGSU PROVINCE TO: 215121 SUZHOU, JIANGSU PROVINCE |
|
| TR01 | Transfer of patent right |
Effective date of registration: 20130402 Address after: 215121, Jiangsu Industrial Park, Suzhou province only Town, only 9 new road, only Pavilion industry square B2 blocks Patentee after: SUZHOU TAILI SANJIA NANO TECHNOLOGY CO., LTD. Address before: Double road Suzhou Industrial Park Suzhou city Jiangsu province 215122 No. 2 Patentee before: Jiangsu Bang'an New Materials Technology Co., Ltd. |
|
| DD01 | Delivery of document by public notice | ||
| DD01 | Delivery of document by public notice |
Addressee: SUZHOU TAILI SANJIA NANO TECHNOLOGY CO., LTD. Document name: Notification to Pay the Fees |
|
| DD01 | Delivery of document by public notice | ||
| DD01 | Delivery of document by public notice |
Addressee: SUZHOU TAILI SANJIA NANO TECHNOLOGY CO., LTD. Document name: Notification of Termination of Patent Right |
|
| CF01 | Termination of patent right due to non-payment of annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20110216 Termination date: 20180618 |