CN206392065U - A kind of Titanium series catalyst preparation facilities - Google Patents
A kind of Titanium series catalyst preparation facilities Download PDFInfo
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- CN206392065U CN206392065U CN201720039614.XU CN201720039614U CN206392065U CN 206392065 U CN206392065 U CN 206392065U CN 201720039614 U CN201720039614 U CN 201720039614U CN 206392065 U CN206392065 U CN 206392065U
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- tank
- tank body
- solid
- liquid separator
- drier
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Abstract
The utility model discloses a kind of Titanium series catalyst preparation facilities, including titanium tetrachloride tank, ammonia water tank, deionization water pot, reactor, solid-liquid separator and drier；The reactor includes tank body, the tank body is externally provided with an incubation cavity and the hot air apparatus connected with incubation cavity, the tank body top is connected with titanium tetrachloride tank, ammonia water tank, deionization water pot respectively by pipeline, the bottom of the tank body is provided with agitating device, bottom in tank body is provided with the diversion seat of a taper, and the bottom of the tank body is provided with discharging opening；The discharging opening connects the import of solid-liquid separator, and the solid outlet connection drier of the solid-liquid separator, the liquid outlet of solid-liquid separator connects a disposing mother liquor tank.The utility model realizes the quick adjustment of reaction temperature；Unique stirring structure makes material be sufficiently mixed rapidly, improves the reaction rate of material, and product stability；Production procedure is pollution-free, and raw material availability is high.
Description
Technical field
The utility model is related to a kind of Titanium series catalyst preparation facilities.
Background technology
In recent years, Titanium series catalyst especially nano titanium oxide (abbreviation nano-titanium) is due to its remarkable physics and chemistry
One of property, study hotspot as Material Field.Nano-titanium has excellent photocatalysis performance, is current most application prospect
One of catalysis material, and entered practical application in many fields, such as automatic cleaning coating, light catalytic purifying, anti-
Bacterium coating, super-hydrophilic coating etc..In the prior art, the preparation method of nano-titanium mainly has：Sol-gel process, hydro-thermal method, chemistry
The precipitation method, solvent-thermal method etc..Wherein sol-gel process because synthesis technique it is simple, reaction condition is gentle and the advantages of being easily controlled,
And as the most frequently used synthetic method for preparing nano-titanium.In sol gel reaction, there is metatitanic acid alkoxide very strong reaction to live
Property, with condensation reaction rapidly, therefore, during to reaction the control of temperature and mixing speed is the key of production for hydrolysis, is used at present
Process units there is certain defect in temperature control and agitating function.
Utility model content
The purpose of this utility model be for overcome above-mentioned the deficiencies in the prior art there is provided.
To achieve the above object, the utility model uses following technical proposals：A kind of Titanium series catalyst preparation facilities, including
Titanium tetrachloride tank, ammonia water tank, deionization water pot, reactor, solid-liquid separator and drier；The reactor includes tank body, institute
State tank body and be externally provided with an incubation cavity and the hot air apparatus connected with incubation cavity, the tank body top by pipeline respectively with four chlorinations
Titanium tank, ammonia water tank, the connection of deionization water pot, the bottom of the tank body are provided with agitating device, and the agitating device includes being located at tank
Stirrer paddle is provided with four internal mozzles, mozzle, the water conservancy diversion inside pipe wall, which is provided with, to be used for leading that material is heated
Bottom in deep fat pipe, tank body is provided with the diversion seat of a taper, and the bottom of the tank body is provided with discharging opening；The discharging opening connection
The import of solid-liquid separator, the solid outlet connection drier of the solid-liquid separator, the liquid outlet connection of solid-liquid separator
One disposing mother liquor tank.
The drier is connected with deionization water pot, and the deionized water of evaporation is recovered into deionization water pot.
In use, the raw material in titanium tetrachloride tank, ammonia water tank, deionization water pot enters in reactor, reactor by leading
Deep fat pipe and hot air apparatus are heated and are incubated, and four stirrer paddles rotate downward discharge in reactor, and slurry passes through water conservancy diversion
Pipe reach tank body inner bottom part, four strands slurry stream collisional mixings, after the upward reflux in centre through diversion seat water conservancy diversion from four mozzles,
Mozzle is finally reentered, whole process forms acutely quickly mixing circulation liquid stream；Material is through discharging opening after completion of the reaction
Into solid-liquid separator, the mother liquor after separation enters disposing mother liquor tank, and the solid of separation is dried into drier, drier
The moisture of interior evaporation is reclaimed into deionization water pot.
The beneficial effects of the utility model are：The utility model can be by hot air apparatus and heat-conducting oil pipes to reaction temperature
Double control is carried out, the quick adjustment of reaction temperature is realized；Unique stirring structure makes material be sufficiently mixed rapidly, improves thing
The reaction rate of material, and product stability；The present apparatus can realize that reacted mother liquor and deionized water are reclaimed, production
Flow is pollution-free, and raw material availability is high.
Brief description of the drawings
, below will be to embodiment in order to illustrate more clearly of the utility model embodiment or technical scheme of the prior art
Or the accompanying drawing used required in description of the prior art is briefly described, it should be apparent that, drawings in the following description are only
It is some embodiments of the present utility model, for those of ordinary skill in the art, before creative labor is not paid
Put, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is structural representation of the present utility model；
Fig. 2 is the structural representation of agitating device.
Shown in figure：1st, titanium tetrachloride tank, 2, ammonia water tank, 3, deionization water pot, 4, solid-liquid separator, 5, reactor, 6,
Drier, 7, tank body, 8, incubation cavity, 9, hot air apparatus, 10, mozzle, 11, stirrer paddle, 12, heat-conducting oil pipes, 13, water conservancy diversion
Seat, 14, disposing mother liquor tank.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the utility model embodiment is carried out
Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the utility model, rather than whole
Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made
The every other embodiment obtained, belongs to the scope of the utility model protection.
A kind of Titanium series catalyst preparation facilities as depicted in figs. 1 and 2, including titanium tetrachloride tank 1, ammonia water tank 2, deionization
Water pot 3, reactor 5, solid-liquid separator 4 and drier 6；The reactor 5 includes tank body 7, and the tank body 7 is externally provided with an insulation
Chamber 8 and the hot air apparatus 9 connected with incubation cavity 8, the top of tank body 7 by pipeline respectively with titanium tetrachloride tank 1, ammonia water tank 2,
Deionization water pot 3 is connected, and the bottom of the tank body 7 is provided with agitating device, and the agitating device includes four in tank body 7
Stirrer paddle 11 is provided with mozzle 10, mozzle 10, the inwall of mozzle 10 is provided with the heat conduction for being used for heating to material
Bottom in oil pipe 12, tank body 7 is provided with the diversion seat 13 of a taper, and the bottom of the tank body 7 is provided with discharging opening；The discharging opening
Connect the import of solid-liquid separator 4, the solid outlet connection drier 6 of the solid-liquid separator 4, the liquid of solid-liquid separator 4
One disposing mother liquor tank 14 of outlet connection.
The drier 6 is connected with deionization water pot 3, and the deionized water of evaporation is recovered into deionization water pot 3.
Preferred embodiment of the present utility model is the foregoing is only, it is all at this not to limit the utility model
Within the spirit and principle of utility model, any modification, equivalent substitution and improvements made etc. should be included in the utility model
Protection domain within.
Claims (2)
1. a kind of Titanium series catalyst preparation facilities, it is characterised in that：Including titanium tetrachloride tank, ammonia water tank, deionization water pot, reaction
Kettle, solid-liquid separator and drier；The reactor includes tank body, and the tank body is externally provided with an incubation cavity and connected with incubation cavity
Hot air apparatus, the tank body top is connected with titanium tetrachloride tank, ammonia water tank, deionization water pot respectively by pipeline, the tank
The bottom of body is provided with agitating device, and the agitating device is included in four mozzles in tank body, mozzle provided with stirring
Blade, the bottom that the water conservancy diversion inside pipe wall is provided with the heat-conducting oil pipes for being used for heating to material, tank body leading provided with a taper
Seat is flowed, the bottom of the tank body is provided with discharging opening；The discharging opening connects the import of solid-liquid separator, the solid-liquid separator
Solid outlet connects drier, and the liquid outlet of solid-liquid separator connects a disposing mother liquor tank.
2. Titanium series catalyst preparation facilities according to claim 1, it is characterised in that：The drier and deionization water pot
Connection, deionization water pot is recovered into by the deionized water of evaporation.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720039614.XU CN206392065U (en) | 2017-01-13 | 2017-01-13 | A kind of Titanium series catalyst preparation facilities |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201720039614.XU CN206392065U (en) | 2017-01-13 | 2017-01-13 | A kind of Titanium series catalyst preparation facilities |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN206392065U true CN206392065U (en) | 2017-08-11 |
Family
ID=59513660
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN201720039614.XU Expired - Fee Related CN206392065U (en) | 2017-01-13 | 2017-01-13 | A kind of Titanium series catalyst preparation facilities |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN206392065U (en) |
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519893A (en) * | 2017-10-20 | 2017-12-29 | 德清四海化工有限公司 | A kind of Raney's nickel process units |
| CN113842854A (en) * | 2021-08-24 | 2021-12-28 | 深圳市银宝山新科技股份有限公司 | Reaction device |
-
2017
- 2017-01-13 CN CN201720039614.XU patent/CN206392065U/en not_active Expired - Fee Related
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN107519893A (en) * | 2017-10-20 | 2017-12-29 | 德清四海化工有限公司 | A kind of Raney's nickel process units |
| CN113842854A (en) * | 2021-08-24 | 2021-12-28 | 深圳市银宝山新科技股份有限公司 | Reaction device |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| GR01 | Patent grant | ||
| GR01 | Patent grant | ||
| CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20170811 Termination date: 20180113 |
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| CF01 | Termination of patent right due to non-payment of annual fee |