CN206392065U - A kind of Titanium series catalyst preparation facilities - Google Patents

A kind of Titanium series catalyst preparation facilities Download PDF

Info

Publication number
CN206392065U
CN206392065U CN201720039614.XU CN201720039614U CN206392065U CN 206392065 U CN206392065 U CN 206392065U CN 201720039614 U CN201720039614 U CN 201720039614U CN 206392065 U CN206392065 U CN 206392065U
Authority
CN
China
Prior art keywords
tank
tank body
solid
liquid separator
drier
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CN201720039614.XU
Other languages
Chinese (zh)
Inventor
顾晓华
龚子龙
龚晓光
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Shandong Dongte Environmental Technology Co Ltd
Original Assignee
Shandong Dongte Environmental Technology Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Shandong Dongte Environmental Technology Co Ltd filed Critical Shandong Dongte Environmental Technology Co Ltd
Priority to CN201720039614.XU priority Critical patent/CN206392065U/en
Application granted granted Critical
Publication of CN206392065U publication Critical patent/CN206392065U/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Abstract

The utility model discloses a kind of Titanium series catalyst preparation facilities, including titanium tetrachloride tank, ammonia water tank, deionization water pot, reactor, solid-liquid separator and drier;The reactor includes tank body, the tank body is externally provided with an incubation cavity and the hot air apparatus connected with incubation cavity, the tank body top is connected with titanium tetrachloride tank, ammonia water tank, deionization water pot respectively by pipeline, the bottom of the tank body is provided with agitating device, bottom in tank body is provided with the diversion seat of a taper, and the bottom of the tank body is provided with discharging opening;The discharging opening connects the import of solid-liquid separator, and the solid outlet connection drier of the solid-liquid separator, the liquid outlet of solid-liquid separator connects a disposing mother liquor tank.The utility model realizes the quick adjustment of reaction temperature;Unique stirring structure makes material be sufficiently mixed rapidly, improves the reaction rate of material, and product stability;Production procedure is pollution-free, and raw material availability is high.

Description

A kind of Titanium series catalyst preparation facilities
Technical field
The utility model is related to a kind of Titanium series catalyst preparation facilities.
Background technology
In recent years, Titanium series catalyst especially nano titanium oxide (abbreviation nano-titanium) is due to its remarkable physics and chemistry One of property, study hotspot as Material Field.Nano-titanium has excellent photocatalysis performance, is current most application prospect One of catalysis material, and entered practical application in many fields, such as automatic cleaning coating, light catalytic purifying, anti- Bacterium coating, super-hydrophilic coating etc..In the prior art, the preparation method of nano-titanium mainly has:Sol-gel process, hydro-thermal method, chemistry The precipitation method, solvent-thermal method etc..Wherein sol-gel process because synthesis technique it is simple, reaction condition is gentle and the advantages of being easily controlled, And as the most frequently used synthetic method for preparing nano-titanium.In sol gel reaction, there is metatitanic acid alkoxide very strong reaction to live Property, with condensation reaction rapidly, therefore, during to reaction the control of temperature and mixing speed is the key of production for hydrolysis, is used at present Process units there is certain defect in temperature control and agitating function.
Utility model content
The purpose of this utility model be for overcome above-mentioned the deficiencies in the prior art there is provided.
To achieve the above object, the utility model uses following technical proposals:A kind of Titanium series catalyst preparation facilities, including Titanium tetrachloride tank, ammonia water tank, deionization water pot, reactor, solid-liquid separator and drier;The reactor includes tank body, institute State tank body and be externally provided with an incubation cavity and the hot air apparatus connected with incubation cavity, the tank body top by pipeline respectively with four chlorinations Titanium tank, ammonia water tank, the connection of deionization water pot, the bottom of the tank body are provided with agitating device, and the agitating device includes being located at tank Stirrer paddle is provided with four internal mozzles, mozzle, the water conservancy diversion inside pipe wall, which is provided with, to be used for leading that material is heated Bottom in deep fat pipe, tank body is provided with the diversion seat of a taper, and the bottom of the tank body is provided with discharging opening;The discharging opening connection The import of solid-liquid separator, the solid outlet connection drier of the solid-liquid separator, the liquid outlet connection of solid-liquid separator One disposing mother liquor tank.
The drier is connected with deionization water pot, and the deionized water of evaporation is recovered into deionization water pot.
In use, the raw material in titanium tetrachloride tank, ammonia water tank, deionization water pot enters in reactor, reactor by leading Deep fat pipe and hot air apparatus are heated and are incubated, and four stirrer paddles rotate downward discharge in reactor, and slurry passes through water conservancy diversion Pipe reach tank body inner bottom part, four strands slurry stream collisional mixings, after the upward reflux in centre through diversion seat water conservancy diversion from four mozzles, Mozzle is finally reentered, whole process forms acutely quickly mixing circulation liquid stream;Material is through discharging opening after completion of the reaction Into solid-liquid separator, the mother liquor after separation enters disposing mother liquor tank, and the solid of separation is dried into drier, drier The moisture of interior evaporation is reclaimed into deionization water pot.
The beneficial effects of the utility model are:The utility model can be by hot air apparatus and heat-conducting oil pipes to reaction temperature Double control is carried out, the quick adjustment of reaction temperature is realized;Unique stirring structure makes material be sufficiently mixed rapidly, improves thing The reaction rate of material, and product stability;The present apparatus can realize that reacted mother liquor and deionized water are reclaimed, production Flow is pollution-free, and raw material availability is high.
Brief description of the drawings
, below will be to embodiment in order to illustrate more clearly of the utility model embodiment or technical scheme of the prior art Or the accompanying drawing used required in description of the prior art is briefly described, it should be apparent that, drawings in the following description are only It is some embodiments of the present utility model, for those of ordinary skill in the art, before creative labor is not paid Put, other accompanying drawings can also be obtained according to these accompanying drawings.
Fig. 1 is structural representation of the present utility model;
Fig. 2 is the structural representation of agitating device.
Shown in figure:1st, titanium tetrachloride tank, 2, ammonia water tank, 3, deionization water pot, 4, solid-liquid separator, 5, reactor, 6, Drier, 7, tank body, 8, incubation cavity, 9, hot air apparatus, 10, mozzle, 11, stirrer paddle, 12, heat-conducting oil pipes, 13, water conservancy diversion Seat, 14, disposing mother liquor tank.
Embodiment
Below in conjunction with the accompanying drawing in the utility model embodiment, the technical scheme in the utility model embodiment is carried out Clearly and completely describe, it is clear that described embodiment is only a part of embodiment of the utility model, rather than whole Embodiment.Based on the embodiment in the utility model, those of ordinary skill in the art are not under the premise of creative work is made The every other embodiment obtained, belongs to the scope of the utility model protection.
A kind of Titanium series catalyst preparation facilities as depicted in figs. 1 and 2, including titanium tetrachloride tank 1, ammonia water tank 2, deionization Water pot 3, reactor 5, solid-liquid separator 4 and drier 6;The reactor 5 includes tank body 7, and the tank body 7 is externally provided with an insulation Chamber 8 and the hot air apparatus 9 connected with incubation cavity 8, the top of tank body 7 by pipeline respectively with titanium tetrachloride tank 1, ammonia water tank 2, Deionization water pot 3 is connected, and the bottom of the tank body 7 is provided with agitating device, and the agitating device includes four in tank body 7 Stirrer paddle 11 is provided with mozzle 10, mozzle 10, the inwall of mozzle 10 is provided with the heat conduction for being used for heating to material Bottom in oil pipe 12, tank body 7 is provided with the diversion seat 13 of a taper, and the bottom of the tank body 7 is provided with discharging opening;The discharging opening Connect the import of solid-liquid separator 4, the solid outlet connection drier 6 of the solid-liquid separator 4, the liquid of solid-liquid separator 4 One disposing mother liquor tank 14 of outlet connection.
The drier 6 is connected with deionization water pot 3, and the deionized water of evaporation is recovered into deionization water pot 3.
Preferred embodiment of the present utility model is the foregoing is only, it is all at this not to limit the utility model Within the spirit and principle of utility model, any modification, equivalent substitution and improvements made etc. should be included in the utility model Protection domain within.

Claims (2)

1. a kind of Titanium series catalyst preparation facilities, it is characterised in that:Including titanium tetrachloride tank, ammonia water tank, deionization water pot, reaction Kettle, solid-liquid separator and drier;The reactor includes tank body, and the tank body is externally provided with an incubation cavity and connected with incubation cavity Hot air apparatus, the tank body top is connected with titanium tetrachloride tank, ammonia water tank, deionization water pot respectively by pipeline, the tank The bottom of body is provided with agitating device, and the agitating device is included in four mozzles in tank body, mozzle provided with stirring Blade, the bottom that the water conservancy diversion inside pipe wall is provided with the heat-conducting oil pipes for being used for heating to material, tank body leading provided with a taper Seat is flowed, the bottom of the tank body is provided with discharging opening;The discharging opening connects the import of solid-liquid separator, the solid-liquid separator Solid outlet connects drier, and the liquid outlet of solid-liquid separator connects a disposing mother liquor tank.
2. Titanium series catalyst preparation facilities according to claim 1, it is characterised in that:The drier and deionization water pot Connection, deionization water pot is recovered into by the deionized water of evaporation.
CN201720039614.XU 2017-01-13 2017-01-13 A kind of Titanium series catalyst preparation facilities Expired - Fee Related CN206392065U (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN201720039614.XU CN206392065U (en) 2017-01-13 2017-01-13 A kind of Titanium series catalyst preparation facilities

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN201720039614.XU CN206392065U (en) 2017-01-13 2017-01-13 A kind of Titanium series catalyst preparation facilities

Publications (1)

Publication Number Publication Date
CN206392065U true CN206392065U (en) 2017-08-11

Family

ID=59513660

Family Applications (1)

Application Number Title Priority Date Filing Date
CN201720039614.XU Expired - Fee Related CN206392065U (en) 2017-01-13 2017-01-13 A kind of Titanium series catalyst preparation facilities

Country Status (1)

Country Link
CN (1) CN206392065U (en)

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107519893A (en) * 2017-10-20 2017-12-29 德清四海化工有限公司 A kind of Raney's nickel process units
CN113842854A (en) * 2021-08-24 2021-12-28 深圳市银宝山新科技股份有限公司 Reaction device

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN107519893A (en) * 2017-10-20 2017-12-29 德清四海化工有限公司 A kind of Raney's nickel process units
CN113842854A (en) * 2021-08-24 2021-12-28 深圳市银宝山新科技股份有限公司 Reaction device

Similar Documents

Publication Publication Date Title
CN206392065U (en) A kind of Titanium series catalyst preparation facilities
CN105623861B (en) A kind of glycerine esterification reaction unit
CN207713419U (en) A kind of device preparing boehmite
CN211586169U (en) Heating agitator tank
CN205925531U (en) Heat recovery type water -reducing agent stirring reation kettle that stirring effect is good
CN205241251U (en) Ludox closed loop reation kettle
CN203018087U (en) Reaction kettle
CN109900089A (en) A kind of novel stoving process method preparing super absorbent resin
CN210656627U (en) Homogeneous acidification pyrolysis device and system for treating various mixed organic wastes
CN210993892U (en) A agitating unit for instant agar production
CN205045998U (en) Device for producing large -volumetric cement water reducing agent
CN206965737U (en) A kind of aluminium ash prepares flocculant poly aluminium chloride device
CN205659668U (en) Novel polypropylene reation kettle
CN207933406U (en) A kind of fully-automatic production system of refined cooking wine
CN102764624A (en) Precipitation reactor for producing silica
CN102512843A (en) Vacuum sublimation device
CN206295938U (en) A kind of hydrolysis reaction device of benzophenone
CN206424951U (en) A kind of reactor produced for titanium series polyester catalyst
CN206157063U (en) Naphthalene is high efficiency water reducing agent production system
CN206325517U (en) The cooling body of agitator tank
CN214861208U (en) Dewatering device is used in production of diethylene glycol methyl ethyl ether
CN205062030U (en) Crude oil of oil chaff granule leaches device
CN211659964U (en) Stirring-free mixing circulating device
CN202845017U (en) Reaction kettle capable of quick cooling
CN206751420U (en) A kind of feed arrangement for preparing lithium titanate or modified lithium titanate presoma

Legal Events

Date Code Title Description
GR01 Patent grant
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20170811

Termination date: 20180113

CF01 Termination of patent right due to non-payment of annual fee