CN201586400U - Continuous crystallizer - Google Patents

Continuous crystallizer Download PDF

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Publication number
CN201586400U
CN201586400U CN2010200043589U CN201020004358U CN201586400U CN 201586400 U CN201586400 U CN 201586400U CN 2010200043589 U CN2010200043589 U CN 2010200043589U CN 201020004358 U CN201020004358 U CN 201020004358U CN 201586400 U CN201586400 U CN 201586400U
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CN
China
Prior art keywords
cone
cylinder
crystallizer
barrel
lower cone
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Expired - Fee Related
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CN2010200043589U
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Chinese (zh)
Inventor
陆国民
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JIANGYIN FENGLI BIOENGINEERING EQUIPMENT CO Ltd
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JIANGYIN FENGLI BIOENGINEERING EQUIPMENT CO Ltd
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Priority to CN2010200043589U priority Critical patent/CN201586400U/en
Application granted granted Critical
Publication of CN201586400U publication Critical patent/CN201586400U/en
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Expired - Fee Related legal-status Critical Current

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Abstract

The utility model relates to a continuous crystallizer, which is mainly used for the concentrated crystallization process of producing monosodium glutamate in the food industry. The continuous crystallizer is composed of an upper sealing head (14), an upper cylindrical body (12), an upper cone (9), a middle cylindrical body (7), a lower cone (3) and a bottom sealing head (1), which are in head-tail connection from top to bottom in sequence; a crystal magma circulation port (11) and an inoculation port (17) are connected to the cylinder wall of the upper cylindrical body (12); an inner cone (10) and an inner cylinder body (8) are arranged in the upper cone (9) and the middle cylindrical body (7) respectively; guide flow cylinders (4) are arranged in the inner cone (10), the inner cylinder body (8) and the lower cone (3); a circulation discharge port (18) is formed on the cylinder wall of the middle cylindrical body (7); a circulating reflux port (2) and a crystal magma outlet (20) are formed on the cylinder wall of the lower cone (3); an internal circulation pump (21) is arranged at the bottom end of the crystallizer; a collector (15) is arranged at the top of the upper sealing head (14); and a secondary steam outlet (16) is formed beside the collector (15). The utility model has the characteristics of low steam consumption of equipment, high equipment productivity, high degree of automation and the like.

Description

Continuous crystalizer
(1) background technology
The utility model relates to a kind of continuous crystalizer.Be mainly used in the condensing crystallizing of food service industry glutamate production.The condensing crystallizing that also can be used for other industry.
(2) background technology
At present, the monosodium glutamate crystallization processes adopts gap single-action concentration and crystallization process mode basically.All there be not big breakthrough aspect the production capacity of equipment, the production serialization.The major defect of traditional gap crystallization processes is:
1, integrated steam using is poor, and consumption vapour quota is high.
According to related data, 4 tons of/ton monosodium glutamates of the consumption vapour of glutamate production quota average out to.
2, crystalliser volume is little, and equipment capacity is low.
At present, the crystalliser volume generally used of monosodium glutamate industry is 12m 3, 15m 3More, maximum also is no more than 50m 3
3, automaticity is low, the technology instability, and the ability of resisting the raw material quality fluctuation is also poor, thereby impurity content is higher in the monosodium glutamate finished product, the production cost height.
(3) utility model content
The purpose of this utility model is to overcome above-mentioned deficiency, and a kind of continuous crystalizer that steam is low, equipment capacity is high and automaticity is high that consumes is provided.
The purpose of this utility model is achieved in that a kind of continuous crystalizer, from top to bottom successively by upper cover, go up cylinder, upper cone, middle cylinder, lower cone and bottom (head) is end to end forms, described going up in the cylinder is horizontally arranged with a shower, be connected with a magma circulation port and inoculation mouthful on below the described shower on the cylinder barrel, in described upper cone and middle cylinder, be respectively arranged with an inner cone and an inner barrel, inner cone is inverted cone shape and is connected in the inner barrel top, is provided with a guide shell in described inner cone, inner barrel and lower cone; The cylinder barrel is provided with a circulation discharging opening in described, described lower cone barrel is provided with one and loops back head piece and magma outlet, be provided with an internal circulation pump in the bottom of described crystallizer, the import of this internal circulation pump and the intracavity inter-connection of crystallizer, the outlet of this internal circulation pump is arranged in the described guide shell, be provided with trap at described upper cover top, this trap has umbrella-shaped baffle, is provided with indirect steam outlet at the trap side.
The beneficial effects of the utility model are:
1, crystallizer equipment enlarging, production capacity increases.
The volume of crystallizer has been broken through the conventional size of gap single-action condensing crystallizing device, can reach 80m 3More than.And general gap crystallizer has only 20m 3About, amplify doubly a lot of.Not only equipment capacity is greatly improved, but also has saved the table of equipment number, has reduced investment cost.It is reported, build identical production-scale monosodium glutamate device.The investment of continuous crystalizer technology will be saved more than 30%.
2, continuous crystalizer operation serialization, production cost descends.
Continuous crystalizer technology has been improved the recurrent state of crystallization solution, has reduced degree of supersaturation, and is very favourable to the growth of the formation of nucleus and crystal.Thereby crystallization temperature has descended, and percent crystallization in massecuite is enhanced, and magma can be from extraction continuously in the crystallizer.Realized the operation serialization, required operating personnel reduce significantly, and labor productivity is enhanced.
3, continuous crystalizer can be realized automation control, and quality further improves.Show that mainly impurity is few, the appearance luster light, long crystal formation crystallization is evenly neat.
The gap crystallizer is in order to obtain higher percent crystallization in massecuite, have to rely on the means that improve degree of supersaturation to realize, but degree of supersaturation is high more, the viscosity of magma also sharply raises, viscosity raises and is unfavorable for crystallization, must improve crystallization temperature again as reducing viscosity, chromogenesis and pyroglutamic acid influence product quality and crystalline rate so inevitably.Continuous crystalizer has been implemented the key process parameter feedback controls, and inside and outside internal circulating load and advance jar steam and rationally set has been optimized technology greatly, and impurity obviously reduces in the product, and quality is greatly improved.
Comprehensively above-mentioned, continuous crystalizer of the present utility model has production capacity height, characteristic of low energy consumption.
(4) description of drawings
Fig. 1 is a mold structure schematic diagram of the present utility model.
Fig. 2 is the vertical view of Fig. 1.
Among the figure:
Bottom (head) 1, loop back head piece 2, lower cone 3, guide shell 4, gusset I 5, gusset II 6, middle cylinder 7, inner barrel 8, upper cone 9, inner cone 10, magma circulation port 11, go up cylinder 12, shower 13, upper cover 14, trap 15, indirect steam outlet 16, inoculation mouthfuls 17, circulation discharging opening 18, gripper shoe 19, magma outlet 20, internal circulation pump 21.
(5) specific embodiment
Referring to Fig. 1~2, Fig. 1 is a continuous crystalizer structural representation of the present utility model.Fig. 2 is the vertical view of Fig. 1.By Fig. 1 and Fig. 2 as can be seen, crystallizer of the present utility model, from top to bottom successively by upper cover 14, go up cylinder 12, upper cone 9, middle cylinder 7, lower cone 3 and bottom (head) 1 end to end forming.Described going up in the cylinder 12 is horizontally arranged with a shower 13, be connected with a magma circulation port 11 and inoculation mouthfuls 17 on below the described shower 13 on cylinder 12 barrels, in order to prevent crystallization deposition and poor circulation, in described upper cone 9 and middle cylinder 7, be respectively arranged with an inner cone 10 and an inner barrel 8, inner cone 10 is inverted cone shape and is connected in inner barrel 8 tops, described inner barrel 8 outer rims link to each other with the inwall of described lower cone 3 by gusset I 5, at described inner cone 10, be provided with a guide shell 4 in inner barrel 8 and the lower cone 3, guide shell 4 outer rim tops link to each other with the inwall of inner barrel 8 by gusset II6, and guide shell 4 outer rim bottoms link to each other with the inwall of described lower cone 3 by gripper shoe 19; Cylinder 7 barrels are provided with a circulation discharging opening 18 in described, and described lower cone 3 barrels are provided with one and loop back head piece 2 and magma outlet 20, and this magma outlet 20 adopts crystal to eluriate the structure of leg; Be provided with an internal circulation pump 21 in the bottom of described crystallizer, the import of this internal circulation pump 21 and the intracavity inter-connection of crystallizer, the outlet of this internal circulation pump 21 is arranged in the described guide shell 4; Be provided with trap 15 at described upper cover 14 tops, this trap 15 has umbrella-shaped baffle, to preventing to escape liquid, reducing the loss of operation entrainment and played fine effect.Be provided with indirect steam outlet 16 at trap 15 sides.
In the design of crystallizer structural dimensions, also taken into full account high through than, generally be no more than 2, can cause boiling point to rise after excessive, influence evaporation rate; The highest liquid level of umbrella shape plate washer distance should keep more than the 1m.The magma loss is little like this.
All parts of crystallizer all adopt stainless steel, and stainless steel surfaces also will carry out acid wash passivation processing, inner surface polishing.
Crystallizer drops into quadruplet technological parameter feedback controls instrument, sets three flow values, has realized the crystallizer operation automation.
Quadruplet technological parameter feedback controls instrument is respectively:
1, solid-to-liquid ratio parameter feedback controls inlet amount adopts the rotating speed (frequency control) of double flanges differential pressure transmitter output signal feedback regulation feed pump to realize automatic control.
2, liquid level parameter feedback controls load in the crystallizer.Adopt two flange differential pressure device transmitters to carry signal feedback to regulate discharging revolution speed (frequency control) and realize automatic control.
3, heater condensation water pot liquid level parameter feedback controls is taken out the condensate pump flow, adopts control valve control.
4, surface cooler temperature parameter feedback controls cooling water flow adopts control valve control.
Three flow values are set and are respectively: advance circular flow and outer circulation flow in heater steam flow, the crystallizer.

Claims (3)

1. continuous crystalizer, it is characterized in that described continuous crystalizer, from top to bottom successively by upper cover (14), last cylinder (12), upper cone (9), middle cylinder (7), lower cone (3) and end to end the forming of bottom (head) (1), described going up in the cylinder (12) is horizontally arranged with a shower (13), on last cylinder (12) barrel of described shower (13) below, be connected with a magma circulation port (11) and inoculation mouthful (17), in described upper cone (9) and middle cylinder (7), be respectively arranged with an inner cone (10) and an inner barrel (8), inner cone (10) is inverted cone shape and is connected in inner barrel (8) top, in described inner cone (10), be provided with a guide shell (4) in inner barrel (8) and the lower cone (3); Cylinder (7) barrel is provided with a circulation discharging opening (18) in described, described lower cone (3) barrel is provided with one and loops back head piece (2) and magma outlet (20), be provided with an internal circulation pump (21) in the bottom of described crystallizer, the import of this internal circulation pump (21) and the intracavity inter-connection of crystallizer, the outlet of this internal circulation pump (21) are arranged in the described guide shell (4); Be provided with trap (15) at described upper cover (14) top, this trap (15) has umbrella-shaped baffle, is provided with indirect steam outlet (16) at trap (15) side.
2. a kind of continuous crystalizer according to claim 1, it is characterized in that described inner barrel (8) outer rim links to each other with the inwall of described lower cone (3) by gusset I (5), guide shell (4) outer rim top links to each other with the inwall of inner barrel (8) by gusset II (6), and guide shell (4) outer rim bottom links to each other with the inwall of described lower cone (3) by gripper shoe (19).
3. a kind of continuous crystalizer according to claim 1 and 2 is characterized in that described magma exports (20) and adopts crystal to eluriate the structure of leg.
CN2010200043589U 2010-01-16 2010-01-16 Continuous crystallizer Expired - Fee Related CN201586400U (en)

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Application Number Priority Date Filing Date Title
CN2010200043589U CN201586400U (en) 2010-01-16 2010-01-16 Continuous crystallizer

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Application Number Priority Date Filing Date Title
CN2010200043589U CN201586400U (en) 2010-01-16 2010-01-16 Continuous crystallizer

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CN201586400U true CN201586400U (en) 2010-09-22

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102294135A (en) * 2011-07-21 2011-12-28 无锡荣丰生物工程有限公司 Crystal-magma separator device
CN104014155A (en) * 2014-05-21 2014-09-03 江苏嘉泰蒸发结晶设备有限公司 Continuous discharge device of evaporation and crystallization equipment

Cited By (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102294135A (en) * 2011-07-21 2011-12-28 无锡荣丰生物工程有限公司 Crystal-magma separator device
CN102294135B (en) * 2011-07-21 2013-06-19 无锡荣丰生物工程有限公司 Crystal-magma separator device
CN104014155A (en) * 2014-05-21 2014-09-03 江苏嘉泰蒸发结晶设备有限公司 Continuous discharge device of evaporation and crystallization equipment

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C14 Grant of patent or utility model
GR01 Patent grant
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20100922

Termination date: 20150116

EXPY Termination of patent right or utility model