CN201524442U - High-efficient scraping wall type hollow sheet bar cooling continuous crystallizer - Google Patents
High-efficient scraping wall type hollow sheet bar cooling continuous crystallizer Download PDFInfo
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- CN201524442U CN201524442U CN2009202105799U CN200920210579U CN201524442U CN 201524442 U CN201524442 U CN 201524442U CN 2009202105799 U CN2009202105799 U CN 2009202105799U CN 200920210579 U CN200920210579 U CN 200920210579U CN 201524442 U CN201524442 U CN 201524442U
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Abstract
The utility model discloses a high-efficient scraping wall type hollow sheet bar cooling continuous crystallizer, which comprises a U-shaped horizontal elongated slot shaped container. A plurality of hollow cooling sheet bars are combined and arrayed inside the U-shaped horizontal elongated slot shaped container, a rotating shaft penetrates through all the cooling sheet bars, a separating circular disc is arranged between each two cooling sheet bars, adjustable scraping wall type blenders are mounted on the separating circular discs and the rotating shaft , and all the separating circular discs and all the scraping wall type blenders are arranged on the rotating shaft and driven by an electromotor and a speed reducer to rotationally blend. The scraping wall type blenders have functions of cleaning walls, rapidly scrap crystals on the surfaces of the cooling sheet bars, not only are large in cooling area, but also lead heat transmission and cooling efficiencies to be increased greatly. The crystallizer can be used for leading materials such as chemicals, fine chemicals, medicines, food and the like to be in mass continuous crystallization and intermittent batch crystallization. The crystallizer can replace few even dozens of kettle-type crystallizers with the same volume, is fast in crystallizing speed and high in efficiency, and can be operated continuously and closely.
Description
Technical field
The utility model relates to a kind of being used for the continuous crystallisation in enormous quantities of materials such as chemical and fine chemicals, medicine, food or the crystallizer of gap batch crystallization, is specifically related to a kind of hollow plate cooling of wall type continuous crystallisation machine of efficiently scraping.
Background technology
As everyone knows, the crystallisation by cooling of material is a medicine, and the crucial unit operations of industries such as chemical industry, food, directly influences the output and the quality of product at the quality of crystallization.
At present with the most use is the kettle type crystallization device, this equipment is to add cooling jacket at the kettle that a band stirs to come material is carried out crystallisation by cooling, or, in still, add cooling coil etc. again material is carried out crystallisation by cooling except adding at kettle cooling jacket cools off.Though this legacy equipment can solve common crystallisation problems, also has many shortcomings:
1. owing to adopt the chuck cooling, crystallization makes crystalline thing at first tie at the still wall at first from the still wall, can form thick crystalline thing on the still wall when serious, influences heat transfer efficiency greatly; Though can reduce the problem of crystallization on the still wall by the method that improves speed of agitator, but crystallization also is subjected to the restriction of speed of agitator under many circumstances, speed of agitator is too fast, the particle diameter of crystal grain is reduced greatly, influence next step filtration washing drying process, and obtain the occasion of crystal grain greatly for hope, improper especially.Still formula stirred crystallization in addition, paddle generally are difficult to accomplish to scrape wall and stir, and so just the crystal grain of tying on the still wall can not be scraped, thereby influence heat-transfer effect.
2. common crystallization kettle is often better at the crystallization effect near external refrigeration still wall, and very slow in the material crystallization near the still center, causes that crystal grain is inhomogeneous, and whole crystallization rate is slower.
3. in still, adding the crystallization kettle of cooling coil,,, outside static coil pipe, form crystallization earlier, have a strong impact on heat-transfer effect because cooling coil is static though can improve film-cooled heat greatly.Add the mixing effect that can influence crystallization kettle behind the coil pipe greatly in addition, scrape wall and stir and to accomplish that especially after forming more crystalline thing on the still wall and on the coil pipe, heat-transfer effect is poorer, and slurry can not successfully be discharged fully.
4. the bottom owing to crystallization kettle often is a standard elliptical head, thereby higher for material concentration, the crystallization kettle that crystalline solid is more, and often discharge is not thorough, and the partially crystallizable solid can remain in the interior row of still and not go out, and influences output and energy consumption.
Shortcoming at above-mentioned common kettle type crystallization machine existence, research institution had once developed horizontal interior disk crystallisation by cooling machine, horizontal interior commentaries on classics comb crystallisation by cooling machine, horizontal interior commentaries on classics ribbon crystallisation by cooling machine, the pusher continuous crystallisation by cooling machine of horizontal cored screw, vertical interior commentaries on classics comb crystallisation by cooling machine, the vertical interior ribbon crystallisation by cooling machine etc. that changes of changeing in the industry, crystalline rate is increased, saved energy consumption and reduced crystallization time.
Above-mentioned crystallizer is compared with common kettle type crystallization machine, though efficient increases, but in the process of crystallization, the cooling surface of rotating moving part still has crystal to bear, in case cooling surface has crystal to form, even the thinlyyest also can influence cooling effect, occasion to gap operating, this phenomenon is also very not outstanding, because the crystallized stock of next group heat adds fashionable meeting this layer crystalline solid dissolved, but to the situation of continuous crystallisation, above-mentioned this situation will be very outstanding, because the crystalline solid of cooling surface is can be long-pending more thick more and can't remove and have a strong impact on cooling effect.For this reason, demand urgently developing and a kind ofly can cooling surface be remained totally, thereby improve the crystallizer of crystalline rate.
Summary of the invention
The purpose of this utility model is in order to overcome the deficiencies in the prior art, a kind of hollow plate cooling of wall type continuous crystallisation machine of efficiently scraping is provided, it can all can carry out wall clearly to cooling surface in any process of crystallization, it is smooth clean that cooling surface is remained, thereby improve the Cooling Heat Transfer effect greatly, crystalline rate is improved greatly.
A kind of technical scheme that realizes above-mentioned purpose is: a kind of hollow plate cooling of wall type continuous crystallisation machine of efficiently scraping, comprise frame and sealed housing, wherein,
Described housing is made of horizontal U-shaped elongated slot, left end cap, right end cap and top cover; The bottom of housing is provided with a discharging hole, and end is offered an overflow outlet and a charge door respectively about housing;
In the described U-shaped elongated slot to be spaced and to have fixedly mounted the hollow cooling plate of polylith with the perpendicular mode of U-shaped elongated slot, an elongated slot is offered in bottoms of these cooling plates for the U-shaped structure that is complementary with the U-shaped elongated slot and at the center, seal around the every cooling plate, and the top or the side direction of every cooling plate are respectively equipped with a refrigerant import and a refrigerant exit; The refrigerant exit of every cooling plate is communicated with the refrigerant import of a back cooling plate from left to right by refrigerant communicating pipe respectively, connect a refrigerant inlet tube and a refrigerant exit pipe that leads to outside the described housing respectively in refrigerant import that is positioned at first on U-shaped elongated slot left side cooling plate and the refrigerant exit that is positioned on first cooling in the U-shaped elongated slot the right plate, to form one group of refrigerant turnover loop, or in the U-shaped elongated slot, connect a refrigerant inlet tube that leads to outside the described housing in the refrigerant import of some of other position cooling plates, and on the refrigerant exits of the corresponding some cooling refrigerant exits of plates or some other cooling plates, connect a refrigerant exit pipe that leads to described housing outside respectively, pass in and out loops to form many group refrigerants;
The center of described U-shaped elongated slot is provided with one and passes left end cap, all cooling plate and the rotating shaft of right end cap, and this rotating shaft is by being located at outer left bearing device of housing and the supporting of right bearing device, and by motor, reductor and shaft coupling driven rotary;
In the rotating shaft between first cooling in the described left end cap and the left side plate one or more left ends are installed and are stirred scraper, in the rotating shaft between per two cooling plates, install one and intercept disk, on the right side of every cooling plate with intercept and to install between the disk and to intercept one or more right sides that disk is connected and stir the propelling scrapers, in the left side of every cooling plate with intercept and to install between the disk and to intercept one or more left sides that disk is connected and stir and advance scrapers, the one or more right-hand members stirring of installation scrapers in the rotating shaft between first cooling in right end cap and the right plate;
Described left end stirs scraper, the right side stirring advances scraper, obstruct disk, left side stirring to advance scraper and right-hand member stirring scraper all can rotate with rotating shaft.
The above-mentioned hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping, wherein, the outside of described U-shaped elongated slot also can be provided with a chuck, also be provided with a refrigerant import and a refrigerant exit on this chuck, described motor, reductor, left bearing device, right bearing device, U-shaped elongated slot and chuck all are supported on the frame.
The above-mentioned hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping, wherein, the inside of described every cooling plate is provided with some water conservancy diversion gussets.
The above-mentioned hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping, wherein, described rotating shaft and left end cap reach and right end cap between seal by gland seal device respectively.
Above-mentioned any one efficiently scraped the hollow plate cooling of wall type continuous crystallisation machine, wherein, described continuous crystallisation machine is when being used for the gap batch crystallization, remove a described charge door, one overflow outlet, all choked flow disks and all refrigerant communicating pipes, and stirring scratch boards one or more and that rotating shaft is rotated together are installed between the plates respectively in per two coolings, and a plurality of charging apertures are installed on the top of housing, described discharging hole is as drain hole, the refrigerant import of all cooling plates is connected in an inlet tube, connect one or more refrigerant inflow pipe on this inlet tube, the refrigerant exit of all cooling plates all is connected in a fairlead, connects one or more refrigerant effuser on this fairlead.
Technical scheme of efficiently scraping the hollow plate cooling of wall type continuous crystallisation machine of the present utility model, by assembled arrangement in the horizontal long trough container of a U-shaped a plurality of hollow cooling plates, one rotating shaft from all cooling plates pass through by, between per two cooling plates, the obstruct disk is installed, the adjustable wall type agitating device of scraping is installed intercepting in disk and the rotating shaft, all obstruct disks and scrape the wall type agitating device and be installed in the rotating shaft, stir by motor and reductor driven rotary, this scrapes the wall type agitating device all can carry out wall clearly to cooling surface in any process of crystallization, it is smooth clean that cooling surface is remained, thereby improve the Cooling Heat Transfer effect greatly, crystalline rate is improved greatly.The kettle type crystallization machine of scraping alternative several even tens the same volumes of the hollow plate of wall type cooling continuous crystallisation machine of one playscript with stage directions utility model, crystallization rate is fast, efficient height, and closed-loop operation continuously.
Description of drawings
Fig. 1 is the structure cutaway view of efficiently scraping the hollow plate cooling of wall type continuous crystallisation machine of the present utility model;
Fig. 2 is the side view of Fig. 1;
Fig. 3 is the structure cutaway view of the hollow plate cooling continuous crystallisation machine of wall type when being used for the gap batch operation of efficiently scraping of the present utility model;
Fig. 4 is the side view of Fig. 3.
The specific embodiment
Below by embodiment particularly and in conjunction with the accompanying drawings the technical solution of the utility model is described:
See also Fig. 1 and Fig. 2, the hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping of the present utility model comprises frame 24 and sealed housing, wherein,
Housing is made of horizontal U-shaped elongated slot 13, left end cap 4, right end cap 17 and top cover 14; The bottom of housing is provided with one or more discharging holes 12, end is offered overflow outlet 2 and one charge door 18 respectively about housing, be that overflow outlet 2 is opened on the left end or left end cap 4 of U-shaped elongated slot 13, charge door 18 is opened on the right-hand member or right end cap 17 of U-shaped elongated slot 13;
In the U-shaped elongated slot 13 to be spaced and to have fixedly mounted the hollow cooling plate 7 of polylith with the perpendicular mode of U-shaped elongated slot 13, an elongated slot 28 is offered in bottoms of these cooling plates 7 for the U-shaped structure that is complementary with U-shaped elongated slot 13 and at the center, seal around the every cooling plate 7, and the top or the side direction of every cooling plate 7 are respectively equipped with a refrigerant import 27 and a refrigerant exit 30; Be provided with some water conservancy diversion gussets 29 in the every cooling plate 7, can carry out water conservancy diversion, do not make it walk short circuit to cooling 7 booster actions of plate and to refrigerant; In the refrigerant import 27 that is positioned at first cooling in U-shaped elongated slot 13 left sides plate 7, connect a refrigerant inlet tube 5 that leads to outside the sealed housing, the refrigerant exit 30 of every cooling plate 7 is communicated with the refrigerant import 27 of a back cooling plate 7 from left to right by refrigerant communicating pipe 8 respectively, connects a refrigerant exit pipe 16 that leads to outside the sealed housing on the refrigerant exit 30 that is positioned at first cooling in U-shaped elongated slot 13 the right plate 7; Form one group of refrigerant turnover loop by that analogy, refrigerant is finally discharged through the refrigerant exit 16 that is communicated with it from refrigerant exit pipe 30; Or in U-shaped elongated slot 13, connect a refrigerant inlet tube 5 that leads to outside the described housing in the refrigerant import 27 of some of other position cooling plates 7, and on the refrigerant exits 30 of the corresponding some cooling refrigerant exits 30 of plates 7 or some other cooling plates 7, connect a refrigerant exit pipe 16 that leads to outside the described housing respectively, to form many group refrigerant turnover loop, to satisfy different process for cooling needs;
The outside of U-shaped elongated slot 13 also can be provided with a chuck 26, and this chuck 26 is provided with a refrigerant import 32 and a refrigerant exit 31; Because the film-cooled heat of cooling plate 7 is enough big, U-shaped elongated slot 13 outer chucks 26 can be accepted or rejected according to actual needs;
The center of U-shaped elongated slot 13 is provided with one and passes left end cap 4, all cooling plate 7 and the rotating shaft 20 of right end cap 17, this rotating shaft 20 is supported by the left bearing device 1 and the right bearing device 21 that are located at outside the housing, and by motor 25, reductor 23 and shaft coupling 22 driven rotary; Rotating shaft 20 and left shrouding 4 and with right shrouding 17 between seal by gland seal device 3,19 respectively;
In the rotating shaft 20 between first cooling in the left end cap 4 and the left side plate 7 one or more left ends are installed and are stirred scraper 6, in the rotating shaft 20 between per two cooling plates 7, install one and intercept disk 10, cool off the right side of plate 7 and intercept the one or more right sides stirring propelling scrapers 9 that are connected with obstruct disk 10 of installation between the disk 10 at every, cool off the left side of plate 7 and intercept the one or more left sides stirring propelling scrapers 11 that are connected with obstruct disk 10 of installation between the disk 10, the one or more right-hand members stirring of installation scrapers 15 in the rotating shaft 20 between first cooling of right end cap 17 and the right plate 7 at every;
Left end stirring scraper 6, right side stirring advance scraper 9, obstruct disk 10, left side to stir propelling scraper 11 and right-hand member stirring scraper 15 all can be with rotating shaft 20 rotations;
The hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping of the present utility model is when being used for continuous crystallisation, earlier in refrigerant inlet tube 5, feed refrigerant, refrigerant enters cooling plate 7 by the refrigerant import 27 on first cooling in the left side plate 7, and refrigerant exit 30 outflows of cooling off plate 7 from this piece, the refrigerant inlet tube 27 that flows on the hollow cooling plate 7 of next piece through communicating pipe 8, so by that analogy, refrigerant is finally discharged through the refrigerant exit pipe 16 that is communicated with it from refrigerant exit 30, and refrigerant also can be divided into one or more groups connection and cool off.Simultaneously feed refrigerant in the external jacket 26 of U-shaped elongated slot 13, refrigerant enters from the refrigerant import 32 on the chuck 26, and the refrigerant exit 31 from chuck 26 flows out.Starter motor 25, drive reductor 23 rotates, and passes through shaft coupling 22 drive rotating shafts 20, left end stirring scraper 6, right side stirring propelling scraper 9, obstruct disk 10, left side stirring propelling scraper 11 and right-hand member stirring scraper 15 and rotate together.
Want the material of crystallization to enter in the housing of crystallizer from charge door 18 by measuring continuously, after stirring scraper 15 and scrape wall and stir by right-hand member, flow in the space on its left side and first obstruct disk 10 right side along central slot 28 from the right side of first cooling plate 7, stir the stirring that advances scraper 11 by the left side, make and climbed over first by crystallized stock and intercept disk 10 and enter into its left side, again by intercepting disk 10 left sides and second stirring that propelling scraper 9 is stirred on the right side of cooling off between the plate 7, the central slot 28 of cooling off plate 7 of flowing through second flows in the space on its left side and second obstruct disk 10 right side, like this and the like, export near 2 up to flow to overflow by crystallized stock, after stirring scraper 6 stirrings by pusher left end at last, discharge outside the housings from overflow outlet 2.
Flow into from the process that overflow outlet 2 is flowed out from charge door 18 by crystallized stock, passed through full of twists and turns distance many times, and contact cooling with the cooling surface of the smooth cooling plate 7 of constantly scraping wall and chuck 26, make by the continuous crystallisation by cooling of crystallized stock, finally flow out from overflow outlet 2, obtain the material of advantages of good crystallization continuously, realize real continuous crystallisation.
See also Fig. 3 and Fig. 4 again, the hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping of the present utility model is when being used for the gap batch crystallization, remove charge door 18, one overflow outlet 2, all choked flow disks 10 and all refrigerant communicating pipes 8, and stirring scratch boards 33 one or more and that rotating shaft 20 is rotated together are installed between the plates 7 respectively in per two coolings, and a plurality of charging apertures 34 are installed on the top of housing, and with the drain hole of discharging hole (12) as the good material of batch crystallization, refrigerant import 27 at all cooling plates 7 all is connected in an inlet tube 35, connect one or more refrigerant inflow pipe 36 on this inlet tube 35, the refrigerant exit 30 of all cooling plates 7 all is connected in a fairlead 37, connects one or more refrigerant effuser 38 on this fairlead 37.
The hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping of the present utility model is when being used for the gap batch crystallization, feed refrigerant by one or more refrigerant inflow pipe 36 earlier, make refrigerant enter inlet tube 35, the even distribution of refrigerant entered every refrigerant import 27 on the cooling plate 7, refrigerant flows out from the refrigerant exit 30 on the every cooling plate 7 through the back of flowing through in every cooling plate 7, enter fairlead 37 outside one or more refrigerant effuser 38 discharge machines, refrigerant is turnover or circulation constantly, every cooling plate 7 obtains cooling, simultaneously in the external jacket 26 of U-shaped elongated slot 13, feed refrigerant, refrigerant enters from the refrigerant import 32 of chuck 26, flow out from the refrigerant exit 31 of chuck 26, also to being cooled off by crystallized stock.
Add by crystallized stock to suitable volume from one or more charging apertures 34, starter motor 25, drive reductor 23 rotations, and drive axle 20, left end by shaft coupling 22 and stir scraper 6, right-hand member and stir scraper 15 and stirring scratch board 33 and rotate together with to being stirred crystallisation by cooling by crystallized stock.All stir scraper and all the wall type stirring are scraped on all cooling plate 7 surfaces in the crystallization process, make the surface of cooling plate 7 keep smooth, and then make cooling effect very good.
One batch materials crystallization finishes, and opens bottom drain hole 12, outside the material discharge machine of advantages of good crystallization.
Sometimes in order to obtain big crystal grain, adopt the mode of static crystallization, at this moment agitating device can not leave, and starts agitating device again behind to be crystallized the finishing, and crystallized stock making beating back is discharged from drain hole 12.
The kettle type crystallization machine of efficiently scraping alternative several even tens the same volumes of the hollow plate of wall type cooling continuous crystallisation machine of one playscript with stage directions utility model, crystallization rate is fast, efficient height, and closed-loop operation continuously.
Those of ordinary skill in the art will be appreciated that, above embodiment is used for illustrating the utility model, and be not to be used as qualification of the present utility model, as long as in connotation scope of the present utility model, all will drop in claims scope of the present utility model variation, the modification of the above embodiment.
Claims (5)
1. efficiently scrape the hollow plate cooling of wall type continuous crystallisation machine for one kind, comprise frame (24) and sealed housing, it is characterized in that,
Described housing is made of horizontal U-shaped elongated slot (13), left end cap (4), right end cap (17) and top cover (14); The bottom of housing is provided with one or more discharging holes (12), and end is offered overflow outlet (2) and a charge door (18) respectively about housing;
In the described U-shaped elongated slot (13) to be spaced and to have fixedly mounted the hollow cooling plate (7) of polylith with the perpendicular mode of U-shaped elongated slot (13), an elongated slot (28) is offered in bottoms of these cooling plates (7) for the U-shaped structure that is complementary with U-shaped elongated slot (13) and at the center, seal around the every cooling plate (7), and the top or the side direction of every cooling plate (7) are respectively equipped with a refrigerant import (27) and a refrigerant exit (30), the refrigerant exit (30) of every cooling plate (7) is communicated with the refrigerant import (27) of a back cooling plate (7) from left to right by refrigerant communicating pipe (8) respectively, connect a refrigerant inlet tube (5) and a refrigerant exit pipe (16) that leads to outside the described housing respectively in refrigerant import (27) that is positioned at first on U-shaped elongated slot (13) left side cooling plate (7) and the refrigerant exit (30) that is positioned on U-shaped elongated slot (13) the right first cooling plate (7), to form one group of refrigerant turnover loop, or refrigerant inlet tube (5) that leads to outside the described housing of connection is gone up in the refrigerant import (27) of the some cooling plates (7) of other position in U-shaped elongated slot (13), and on the refrigerant exits (30) of the refrigerant exit (30) of corresponding some cooling plates (7) or some other cooling plates (7), connect a refrigerant exit pipe (16) that leads to described housing outside respectively, pass in and out loops to form many group refrigerants;
The center of described U-shaped elongated slot (13) is provided with one and passes left end cap (4), all cooling plate (7) and the rotating shaft (20) of right end cap (17), this rotating shaft (20) is supported by being located at outer left bearing device (1) of housing and right bearing device (21), and by motor (25), reductor (23) and shaft coupling (22) driven rotary;
Rotating shaft (20) between the described left end cap (4) and the left side first cooling plate (7) is gone up one or more left ends stirring scrapers (6) is installed, rotating shaft (20) between per two cooling plates (7) is gone up an obstruct disk (10) is installed, on the right side of every cooling plate (7) with intercept and to install between the disk (10) and intercept one or more right sides stirring propelling scrapers (9) that disk (10) is connected, in the left side of every cooling plate (7) with intercept to install between the disk (10) with intercepting one or more left sides that disk (10) is connected and stir and advance scrapers (11), the rotating shaft (20) between right end cap (17) and the right first cooling plate (7) is the one or more right-hand members stirring of installation scrapers (15) upward;
Described left end stirs scraper (6), the right side stirring advances scraper (9), obstruct disk (10), left side stirring to advance scraper (11) and right-hand member stirring scraper (15) all can rotate with rotating shaft (20).
2. the hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping according to claim 1, it is characterized in that, the outside of described U-shaped elongated slot (13) also can be provided with a chuck (26), also be provided with a refrigerant import (32) and a refrigerant exit (31) on this chuck (26), described motor (25), reductor (23), left bearing device (1), right bearing device (21), U-shaped elongated slot (13) and chuck (26) all are supported on the frame (24).
3. the hollow plate cooling of the wall type continuous crystallisation machine of efficiently scraping according to claim 1 is characterized in that the inside of described every cooling plate (7) is provided with some water conservancy diversion gussets (29).
4. the hollow plate of the wall type cooling continuous crystallisation machine of efficiently scraping according to claim 1 is characterized in that, described rotating shaft (20) and left end cap (4) and with right end cap (17) between pass through gland seal device (3) respectively, (19) seal.
5. efficiently scrape the hollow plate cooling of wall type continuous crystallisation machine according to described any one of claim 1 to 4, it is characterized in that, described continuous crystallisation machine is when being used for the gap batch crystallization, remove a described charge door (18), one overflow outlet (2), all choked flow disks (10) and all refrigerant communicating pipes (8), and between per two cooling plates (7), stirring scratch board (33) one or more and that rotating shaft (20) is rotated together is installed respectively, and one or more charging apertures (34) are installed on the top of housing, described one or more discharging hole (12) is as drain hole, the refrigerant import (27) of all cooling plates (7) all is connected in an inlet tube (35), this inlet tube (35) is gone up and is connected one or more refrigerant inflow pipe (36), the refrigerant exit (30) of all cooling plates (7) all is connected in a fairlead (37), and this fairlead (37) is gone up and connected one or more refrigerant effuser (38).
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CN105771305A (en) * | 2016-05-11 | 2016-07-20 | 南宁市夏阳化工科技有限责任公司 | Buffer crystallization equipment for producing adblue |
CN107847900A (en) * | 2015-07-29 | 2018-03-27 | 托尔斯滕·海特曼 | For continuously cultivating the crystal crystallizer that either continuous reaction guides or reactor and method |
CN108096872A (en) * | 2018-01-05 | 2018-06-01 | 浙江万享科技股份有限公司 | A kind of plate type crystallizer |
CN108726578A (en) * | 2018-06-27 | 2018-11-02 | 安徽帝瑟化工科技工程有限公司 | Ferrous sulfate continuous crystallisation technique in a kind of production of sulfate process titanium dioxide |
CN108786170A (en) * | 2018-05-30 | 2018-11-13 | 谢茗 | A kind of horizontal continuous crystallization tank using automatic cleaning brix instrument probe outside mechanical agitation and tank |
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CN112386942A (en) * | 2021-01-21 | 2021-02-23 | 潍坊惠米农业科技发展有限公司 | Crystallization kettle |
CN113975848A (en) * | 2021-11-01 | 2022-01-28 | 安徽相泉化工有限公司 | External continuous cooling crystallization system of cooler |
CN115105853A (en) * | 2022-06-24 | 2022-09-27 | 温州市康而达实业有限公司 | Vertical continuous cooling crystallizer |
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CN107847900A (en) * | 2015-07-29 | 2018-03-27 | 托尔斯滕·海特曼 | For continuously cultivating the crystal crystallizer that either continuous reaction guides or reactor and method |
CN105771305A (en) * | 2016-05-11 | 2016-07-20 | 南宁市夏阳化工科技有限责任公司 | Buffer crystallization equipment for producing adblue |
CN108096872A (en) * | 2018-01-05 | 2018-06-01 | 浙江万享科技股份有限公司 | A kind of plate type crystallizer |
CN108786170A (en) * | 2018-05-30 | 2018-11-13 | 谢茗 | A kind of horizontal continuous crystallization tank using automatic cleaning brix instrument probe outside mechanical agitation and tank |
CN108726578A (en) * | 2018-06-27 | 2018-11-02 | 安徽帝瑟化工科技工程有限公司 | Ferrous sulfate continuous crystallisation technique in a kind of production of sulfate process titanium dioxide |
CN108726578B (en) * | 2018-06-27 | 2020-10-13 | 安徽帝瑟化工科技工程有限公司 | Ferrous sulfate continuous crystallization process in sulfuric acid method titanium dioxide production |
CN111621346A (en) * | 2020-05-28 | 2020-09-04 | 开封泓盈化工发展有限公司 | Process for producing fatty acid type diesel antiwear agent |
CN112386942A (en) * | 2021-01-21 | 2021-02-23 | 潍坊惠米农业科技发展有限公司 | Crystallization kettle |
CN113975848A (en) * | 2021-11-01 | 2022-01-28 | 安徽相泉化工有限公司 | External continuous cooling crystallization system of cooler |
CN115105853A (en) * | 2022-06-24 | 2022-09-27 | 温州市康而达实业有限公司 | Vertical continuous cooling crystallizer |
CN115105853B (en) * | 2022-06-24 | 2024-05-24 | 温州市康而达实业有限公司 | Vertical continuous cooling crystallizer |
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