CN208726784U - A kind of hollow disk bar cooling continuous crystallizer of high effective - Google Patents
A kind of hollow disk bar cooling continuous crystallizer of high effective Download PDFInfo
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- CN208726784U CN208726784U CN201821307804.6U CN201821307804U CN208726784U CN 208726784 U CN208726784 U CN 208726784U CN 201821307804 U CN201821307804 U CN 201821307804U CN 208726784 U CN208726784 U CN 208726784U
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- cylinder
- hollow disk
- cone
- agitating device
- stirring shaft
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/005—Selection of auxiliary, e.g. for control of crystallisation nuclei, of crystal growth, of adherence to walls; Arrangements for introduction thereof
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- B—PERFORMING OPERATIONS; TRANSPORTING
- B01—PHYSICAL OR CHEMICAL PROCESSES OR APPARATUS IN GENERAL
- B01D—SEPARATION
- B01D9/00—Crystallisation
- B01D9/0004—Crystallisation cooling by heat exchange
- B01D9/0013—Crystallisation cooling by heat exchange by indirect heat exchange
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- Crystallography & Structural Chemistry (AREA)
- Chemical Kinetics & Catalysis (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Organic Low-Molecular-Weight Compounds And Preparation Thereof (AREA)
Abstract
The utility model discloses a kind of hollow disk bar cooling continuous crystallizers of high effective, and the central stirring shaft of the cylinder is protruded into including vertical cylinder and from the center vertical of the cylinder top surface；The coaxially connected cone in the bottom of the cylinder, is equipped with base bearing bracket between the cylinder and the cone, the central stirring shaft runs through the base bearing bracket, protrudes into the cone；It is arranged alternately from top to bottom in the cylinder and scrapes wall agitating device and the interior hollow disk for having refrigerant, the wall agitating device of scraping is fixed with the central stirring shaft, the inner periphery of the hollow disk and the cylinder is fixed, in the cylinder, the wall agitating device of scraping is N+1 grades total, and the hollow disk is N grades total；Vertical material flow channels are equipped on the hollow disk；Between material flow channels on the hollow disk of arbitrary neighborhood two-stage, it is greater than 0 degree around central stirring shaft deflection, is less than or equal to 180 degree.
Description
Technical field
The utility model relates to a kind of hollow disk bar cooling continuous crystallizers of high effective of field of chemical equipment.
Background technique
It is well known that the crystallisation by cooling of material is medicine, the highly important unit operation of the industries such as chemical industry, food, crystallization
Quality, directly affect the yield and quality of product.
With the most use at present is kettle type crystallization device, and this equipment is to add cooling jacket outside an autoclave body with stirring
Crystallisation by cooling is carried out to material, it is cooling outer in addition to adding cooling jacket to carry out other than autoclave body, then cooling coil etc. pair is added in kettle
Material carries out crystallisation by cooling.Though this traditional equipment can solve common crystallisation problems, there is also shortcomings:
First, due to cooling using collet, crystallization is first since kettle wall, so that crystalline object is tied in kettle wall, seriously first
When thick crystalline object can be formed on kettle wall, largely effect on heat transfer efficiency；Although can by improve speed of agitator method come
It reduces the problem of being crystallized on kettle wall, but crystallizes the also limitation by speed of agitator in many cases, speed of agitator is too fast, meeting
Making the partial size of crystal grain greatly reduces, and influences the filtration washing drying process of next step, and for wishing to obtain compared with big crystal grain
Occasion is even more improper.In addition autoclave stirred crystallization, agitating paddle, which is generally difficult to, scrapes wall stirring, can not will thus tie
Crystal grain on kettle wall scrapes, to influence heat-transfer effect.
Second, common crystallization kettle is often preferable in the crystallization effect close to external cooling reactor wall, and close to kettle center
Material crystallization is very slow, causes crystal grain uneven, whole crystallization rate is slower.
Third, for the crystallization kettle of cooling coil is added in kettle, though it is greatly improved film-cooled heat, due to cooler pan
Pipe be it is static, first crystallization is formed outside static coil pipe, seriously affect heat-transfer effect.It can be largely effected on after additionally incorporating coil pipe
The mixing effect of crystallization kettle, scraping wall stirring is even more that can not accomplish, after forming more crystalline object on kettle wall and on coil pipe, is passed
Thermal effect is worse, prevents slurry from being successfully completely exhausted out.
4th, since the bottom of crystallization kettle is often standard elliptical head, thus, crystalline solid higher for material concentration
More crystallization kettle, often discharge is not thorough, and partially crystallizable solid, which can remain in kettle, can not arrange, and influences yield and energy consumption.
For above-mentioned common kettle type crystallization machine there are the shortcomings that, research institution once had developed in horizontal that turn disk cold in the industry
But crystallizer, it is horizontal in turn comb cooling crystallization machine, it is horizontal in turn ribbon cooling crystallization machine, Horizontal hollow screw-pushing type continuous
Cooling crystallization machine, it is vertical in turn comb cooling crystallization machine, it is vertical in turn ribbon cooling crystallization machine etc., mention crystalline rate
Height saves energy consumption and reduces crystallization time.
Above-mentioned crystallizer is compared with common kettle type crystallization machine, though efficiency increases, during crystallization, rotation fortune
The cooling surface of dynamic component still has crystal to bear, once cooling surface has Crystallization, even most thin also will affect cooling effect,
To the occasion of gap operating, this phenomenon is not also very prominent, because the crystallized stock of next group heat can be this layer knot when being added
Dissolution of crystals falls, but the case where to continuous crystallisation, the above situation will protrude very much, because of the crystalline solid meeting of cooling surface
It gets deeper and not can be removed and seriously affect cooling effect.Thus, it would be highly desirable to which cooling table can be made during crystallization by developing one kind
Face remains completely, to improve the crystallizer of crystalline rate.
Utility model content
The purpose of this utility model is to overcome the deficiencies in the prior art, and it is cold to provide a kind of hollow disk of high effective
But continuous crystallisation machine can make material sufficient crystallising in cylinder, and effectively prevent crystallization deposition in the inner periphery of cylinder
On.
Realizing a kind of technical solution of above-mentioned purpose is: a kind of hollow disk bar cooling continuous crystallizer of high effective, packet
It includes vertical cylinder and protrudes into the central stirring shaft of the cylinder from the center vertical of the cylinder top surface；
The coaxially connected cone in the bottom of the cylinder is equipped with base bearing bracket between the cylinder and the cone,
The central stirring shaft runs through the base bearing bracket, protrudes into the cone；
It is arranged alternately from top to bottom in the cylinder and scrapes wall agitating device and the interior hollow disk for having refrigerant, it is described to scrape wall
Agitating device is fixed with the central stirring shaft, and the inner periphery of the hollow disk and the cylinder is fixed, the cylinder
Interior, the wall agitating device of scraping is N+1 grades total, and the hollow disk is N grades total；
Vertical material flow channels are equipped on the hollow disk；Material on the hollow disk of arbitrary neighborhood two-stage
Between flow channels, it is greater than 0 degree around central stirring shaft deflection, is less than or equal to 180 degree.
Further, the refrigerant inlet for stretching out the cylinder horizontally outward is equipped on the excircle of the hollow disk
The refrigerant exit of the cylinder is stretched out horizontally outward.
Further, the radial outside of the cylinder is equipped with cylinder collet, and the bottom end of the cylinder collet is equipped with collet
It is imported and exported equipped with collet refrigerant on the top of refrigerant inlet, the cylinder collet.
Further, the radial outside of the cone is equipped with cone collet, and the bottom end of the cone collet is pressed from both sides equipped with cone
Refrigerant inlet is covered, the top of the cone collet is equipped with cone collet refrigerant exit.
Further, level-one scrape bottom surface that wall agitating device scrapes wall agitating device to N grades with the hollow disk of lower section
Top surface contact, the N+1 grades of bottom surfaces for scraping wall agitating device are contacted with the top surface of the base bearing bracket, and second level scrapes wall agitating device extremely
The N+1 grades of top surfaces for scraping wall agitating device are contacted with the bottom surface of the hollow disk in top, and level-one scrapes wall agitating device and scrapes wall to N+1 grades
The excircle of agitating device is contacted with the inner periphery of the cylinder.
Further, the top of the cylinder is equipped with feed inlet and exhaust outlet；The bottom of the cone is gone out by bottom
Between material flow channels on the hollow disk of material flange closure, the feed inlet and top, stirred around the center
Axis deflection is greater than 0 degree, is less than or equal to 180 degree.
Further, equipped with the K cone agitating device cone being connect with central stirring shaft stirrings in the cone
Device, the free end of the cone agitating device are equipped with scraper, the scraper along the cone inner circle circumference bus direction with
The inner circle contour of the cone contacts, K >=1.
Further, the cone agitating device be around the central stirring shaft peripheral helical it is uniformly distributed.
Further, base bearing is equipped between the central stirring shaft and the base bearing bracket.
Using a kind of technical solution of the hollow disk bar cooling continuous crystallizer of high effective of the utility model, including
Vertical cylinder and the central stirring shaft that the cylinder is protruded into from the center vertical of the cylinder top surface；The cylinder
The coaxially connected cone in bottom, base bearing bracket is equipped between the cylinder and the cone, the central stirring shaft runs through
The base bearing bracket, protrudes into the cone；Be arranged alternately from top to bottom in the cylinder scrape wall agitating device and it is interior have it is cold
The hollow disk of matchmaker, the wall agitating device of scraping are fixed with the central stirring shaft, the hollow disk and the cylinder
Inner periphery is fixed, and in the cylinder, the wall agitating device of scraping is N+1 grades total, described total N grades hollow disk of hollow disk
On be equipped with vertical material flow channels；Between material flow channels on the hollow disk of arbitrary neighborhood two-stage, institute is surrounded
It states central stirring shaft deflection and is greater than 0 degree, be less than or equal to 180 degree.Have the technical effect that it is passed through by being arranged in cylinder in fact
The hollow disk of refrigerant, crystallizes material, and by adjusting the position of material flow channels on each hollow disk, extends
Material residence time in cylinder makes material sufficient crystallising in cylinder, and effectively prevent crystallization deposition in cylinder
Inner periphery on.
Detailed description of the invention
Fig. 1 is a kind of structural schematic diagram of the hollow disk bar cooling continuous crystallizer of high effective of the utility model.
Fig. 2 is a kind of vertical view of the cooling disk of the hollow disk bar cooling continuous crystallizer of high effective of the utility model
Figure.
Fig. 3 is a kind of main view of the cooling disk of the hollow disk bar cooling continuous crystallizer of high effective of the utility model
Figure.
Specific embodiment
Please refer to Fig. 1 and Fig. 2, the inventor of the utility model in order to preferably to the technical solution of the utility model into
Row understands, below by specifically embodiment, and will be described in detail with reference to the accompanying drawings:
Referring to Fig. 1, a kind of hollow disk bar cooling continuous crystallizer of high effective of the utility model includes vertical
The top of cylinder 1 and central stirring shaft 4, cylinder 1 is closed by top cover flange apparatus 11, the top surface of top cover flange apparatus 11
It is equipped with feed inlet 111 and exhaust outlet 112.The coaxially connected cone 2 of flange connecting apparatus 12 is bored by cylinder in the bottom of cylinder 1,
It is closed by bottom discharge flange 21 bottom of cone 2.It is separated between cylinder 1 and cone 2 by base bearing bracket 13, lower shaft
Holding bracket 13 is one piece of porous gusset.
The radial outside of cylinder 1 is equipped with cylinder collet 14, and the bottom end of cylinder collet 14 is equipped with collet refrigerant inlet 141,
The top of cylinder collet 14 is equipped with collet refrigerant exit 142.The excircle of cylinder collet 14 is equipped with supporting arrangement 15.
The excircle of cone 2 is socketed with cone collet 22, and the bottom end of cone collet 22 is equipped with cone collet refrigerant inlet
221, the top of cone collet 22 is equipped with cone collet refrigerant exit 222.
In cylinder 1 from top to bottom successively, the total N of hollow disk 3 of the annular fixed with the inner periphery of cylinder 1 is set
Grade, it is equipped with the refrigerant inlet 31 stretched out outside cylinder 1 horizontally outward on the excircle of each hollow disk 3 and horizontal direction is overhanging
Refrigerant exit 32 outside cylinder 1 out, forms mazy refrigerant channel between refrigerant inlet 31 and refrigerant exit 32, make hollow
The temperature of 3 top and bottom of disk meets the requirement of crystallization, and the hollow disk 3 of top is the hollow disk of level-one, lowermost end
Hollow disk 3 is N grades of hollow disks.
Central stirring shaft 4 protrudes into cylinder 1 from the center of top cover flange apparatus 11, and sequentially passes through all hollow disks 3,
And base bearing bracket 13, protrude into cone 2, the bottom end of central stirring shaft 4 and 21 face contact of bottom discharge flange.Central stirring shaft
Base bearing 40 is equipped between 4 and base bearing bracket 13.
In cylinder 1, equipped between top cover flange apparatus 11 and the hollow disk of level-one, arbitrary neighborhood two-stage is hollow
Between disk 3 and between N grades of hollow disks and base bearing bracket 13, fixed wall stirring of scraping is filled with central stirring shaft 4
41 are set, that is, scrapes total N+1 grades of wall agitating device 41, wherein the wall agitating device 41 of scraping of top is that level-one scrapes wall agitating device, most
The wall agitating device 41 of scraping of bottom end scrapes wall agitating device for N+1 grades.
The excircle for scraping wall agitating device 41 is contacted with the inner periphery of cylinder 1.Level-one is scraped wall agitating device and is scraped to N grades
The bottom surface of wall agitating device is contacted with the top surface of the hollow disk 3 of lower section, the N+1 grades of bottom surfaces for scraping wall agitating device and base bearing
The top surface of bracket 13 contacts, second level scrape top surface that wall agitating device scrapes wall agitating device to N+1 grades with the hollow disk 3 in top
Bottom surface contact.
The material flow channels 33 of vertical direction are equipped on hollow disk 3, altogether N grades of material flow channels 33, wherein
Material flow channels 33 on the hollow disk of level-one are level-one material flow channels, the material flow channels on N grades of hollow disks
33 be N grades of flow channels.
Material flow channels 33 on feed inlet 111 and the hollow disk of level-one that is, between level-one material flow channels, surround
4 deflection angle α of heart agitating shaft；Central stirring shaft 4 is surrounded between material flow channels 33 on the hollow disk 3 of arbitrary neighborhood two-stage
Deflection angle α, angle [alpha] are greater than 0 degree, are less than or equal to 180 degree.And the direction of rotation in the deflection direction and central stirring shaft 4 of angle [alpha]
On the contrary.The shape of the horizontal cross-section of material flow channels 33 is kidney ellipsoid.
Arrow direction represents the direction of rotation of central stirring shaft 4 in Fig. 2.
The purpose of this design is: making material in the hollow disk of every level-one by being passed through refrigerant into hollow disk 3
On 3 top surface can crystallisation by cooling, simultaneously because the presence of cylinder collet 14, material synchronous knot on the inner periphery of cylinder 1
Crystalline substance, therefore the space in cylinder 1 is taken full advantage of, accomplish sufficient crystallising.
Material from feed inlet 11 enter cylinder 1 after, scrape wall agitating device 41 prevent crystallization deposition in 1 inner circle of cylinder
While all, the crystallization on the hollow disk 3 of correspondence is taken to next stage sky by the material flow channels 33 on corresponding disk 3
The top surface of heart disk 3, and then cone 2 is fallen by base bearing bracket 13.
Since there are deflection angles between material flow channels 33 on the hollow disk 3 of adjacent two-stage, and deflection angle is inclined
Turn the direction of rotation in direction and central stirring shaft 4 on the contrary, therefore material stops abundant length on the top surface of every level-one open circles disk 3
Time, adequately crystallized in cylinder 1, and effectively prevent crystallizing the deposition in cylinder 1.
The K cone agitating device 42 fixed with central stirring shaft 4, K >=1 are equipped in cone 2.Each cone agitating shaft dress
The free end for setting 42 is equipped with scraper 421, and scraper 421 is parallel with the bus of 2 inner periphery of cone and contacts with 2 inner periphery of cone,
Cone stirs shaft device 42 and is evenly distributed with around 4 spiral of central stirring shaft, guarantees that any point on 2 inner periphery of cone can be by least
A piece scraper 421 scrapes.The length of each 42 upper blade 421 of cone agitating device is at least 2 inner periphery bus length of cone
1/K.Such design, can make cone agitating device 42 to the inner periphery of cone 2 carry out it is comprehensive scrape wall, prevent cone 2
The untouched dead angle of cone agitating device 42 is generated on inner periphery, and generates the deposition of crystallization on dead angle, improves yield, is protected
Quality is demonstrate,proved.
The top surface of top cover flange apparatus 11 is equipped with rack 5, and motor 51 and speed reducer 52, center stirring are fixed in rack 5
The top of axis 4 connects motor 51 by speed reducer 52, and axle envelope 43 is equipped between central stirring shaft 4 and top cover flange apparatus 11.
Those of ordinary skill in the art it should be appreciated that more than embodiment be intended merely to illustrate that this is practical new
Type, and be not used as the restriction to the utility model, as long as in the spirit of the utility model, to the above
Variation, the modification of embodiment will all be fallen in the Claims scope of the utility model.
Claims (9)
1. a kind of hollow disk bar cooling continuous crystallizer of high effective, including vertical cylinder and from the cylinder top surface
Center vertical protrude into the central stirring shaft of the cylinder；It is characterized by:
The coaxially connected cone in the bottom of the cylinder is equipped with base bearing bracket between the cylinder and the cone, described
Central stirring shaft runs through the base bearing bracket, protrudes into the cone；
It is arranged alternately from top to bottom in the cylinder and scrapes wall agitating device and the interior hollow disk for having refrigerant, it is described to scrape wall stirring
Device is fixed with the central stirring shaft, and the inner periphery of the hollow disk and the cylinder is fixed, in the cylinder, institute
It states and scrapes that wall agitating device is N+1 grades total, and the hollow disk is N grades total；
Vertical material flow channels are equipped on the hollow disk；Material overcurrent on the hollow disk of arbitrary neighborhood two-stage
Between channel, it is greater than 0 degree around central stirring shaft deflection, is less than or equal to 180 degree.
2. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 1, it is characterised in that: described
It is equipped with the refrigerant inlet for stretching out the cylinder horizontally outward on the excircle of hollow disk and stretches out the circle horizontally outward
The refrigerant exit of cylinder.
3. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 1, it is characterised in that: described
The radial outside of cylinder is equipped with cylinder collet, and the bottom end of the cylinder collet is equipped with collet refrigerant inlet, the cylinder collet
Top equipped with collet refrigerant import and export.
4. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 1, it is characterised in that: described
The radial outside of cone is equipped with cone collet, and the bottom end of the cone collet is equipped with cone collet refrigerant inlet, the cone folder
The top of set is equipped with cone collet refrigerant exit.
5. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 1, it is characterised in that: level-one
It scrapes the bottom surface that wall agitating device scrapes wall agitating device to N grades to contact with the top surface of the hollow disk of lower section, N+1 grades are scraped wall stirring
The bottom surface of device is contacted with the top surface of the base bearing bracket, and second level scrapes the top that wall agitating device scrapes wall agitating device to N+1 grades
Face is contacted with the bottom surface of the hollow disk in top, level-one scrape excircle that wall agitating device scrapes wall agitating device to N+1 grades with
The inner periphery of the cylinder contacts.
6. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 1, it is characterised in that: described
The top of cylinder is equipped with feed inlet and exhaust outlet；The bottom of the cone passes through bottom discharge flange closure, the feed inlet
Between the material flow channels on the hollow disk of top, it is greater than 0 degree around central stirring shaft deflection, is less than or equal to
180 degree.
7. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 1, it is characterised in that: described
The cone agitating device connecting equipped with K with the central stirring shaft in cone, the free end of the cone agitating device is equipped with
Scraper, the scraper are contacted along the direction of the cone inner circle circumference bus with the inner circle contour of the cone, K >=1.
8. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 7, it is characterised in that: described
Cone agitating device be around the central stirring shaft peripheral helical it is uniformly distributed.
9. the hollow disk bar cooling continuous crystallizer of a kind of high effective according to claim 7, it is characterised in that: described
Base bearing is equipped between central stirring shaft and the base bearing bracket.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821307804.6U CN208726784U (en) | 2018-08-14 | 2018-08-14 | A kind of hollow disk bar cooling continuous crystallizer of high effective |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN201821307804.6U CN208726784U (en) | 2018-08-14 | 2018-08-14 | A kind of hollow disk bar cooling continuous crystallizer of high effective |
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| CN208726784U true CN208726784U (en) | 2019-04-12 |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110124338A (en) * | 2019-06-20 | 2019-08-16 | 江苏瑾瑜节能环保科技有限公司 | A kind of vertical internal-circulating heat exchange vacuum evaporation tank and its concentration systems |
| WO2022117169A1 (en) * | 2020-12-02 | 2022-06-09 | Lübbers FTS GmbH | Crystallization device for crystallizing a precursor, and drying device |
-
2018
- 2018-08-14 CN CN201821307804.6U patent/CN208726784U/en active Active
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110124338A (en) * | 2019-06-20 | 2019-08-16 | 江苏瑾瑜节能环保科技有限公司 | A kind of vertical internal-circulating heat exchange vacuum evaporation tank and its concentration systems |
| WO2022117169A1 (en) * | 2020-12-02 | 2022-06-09 | Lübbers FTS GmbH | Crystallization device for crystallizing a precursor, and drying device |
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