CN201309898Y - Floating-head type isothermal reaction methyl alcohol synthetic reactor - Google Patents

Floating-head type isothermal reaction methyl alcohol synthetic reactor Download PDF

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Publication number
CN201309898Y
CN201309898Y CNU2008202158221U CN200820215822U CN201309898Y CN 201309898 Y CN201309898 Y CN 201309898Y CN U2008202158221 U CNU2008202158221 U CN U2008202158221U CN 200820215822 U CN200820215822 U CN 200820215822U CN 201309898 Y CN201309898 Y CN 201309898Y
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CN
China
Prior art keywords
body skin
tubesheet
pressure
outer casing
tube plate
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Expired - Fee Related
Application number
CNU2008202158221U
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Chinese (zh)
Inventor
金力农
刘福华
赵玉清
潘传飞
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
NANJING HAOAN INDUSTRY EQUIPMENT Co Ltd
Nanjingg Haoan Science And Technology Engineering Co Ltd
Original Assignee
NANJING HAOAN INDUSTRY EQUIPMENT Co Ltd
Nanjingg Haoan Science And Technology Engineering Co Ltd
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by NANJING HAOAN INDUSTRY EQUIPMENT Co Ltd, Nanjingg Haoan Science And Technology Engineering Co Ltd filed Critical NANJING HAOAN INDUSTRY EQUIPMENT Co Ltd
Priority to CNU2008202158221U priority Critical patent/CN201309898Y/en
Application granted granted Critical
Publication of CN201309898Y publication Critical patent/CN201309898Y/en
Anticipated expiration legal-status Critical
Expired - Fee Related legal-status Critical Current

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Abstract

The utility model discloses a floating-head type isothermal reaction methyl alcohol synthetic reactor. A high-pressure upper channel box, a low-pressure outer casing and an outer casing lower seal head are welded integrally, a gas inlet tube passes through the high-pressure upper channel box to enters the inside of the same, a gas distributor is installed at the end portion of the gas inlet tube, an upper tube plate and a lower tube plate are respectively installed on the upper side and the lower side of the inside of the low-pressure outer casing body, a plurality of reaction tubes are disposed between the upper tube plate and the lower tube plate, and a high-pressure inner seal head is mounted on the lower tube plate. Further, a high-temperature gas outlet tube extending out of the lower seal head of the outer casing body is welded to the bottom of the high-pressure inner seal head, the upper tube plate is fixedly connected with the low-pressure outer casing body, the lower tube plate is in clearance fit with the low-pressure outer casing body, thereby a 'floating head' is assembled by the lower tube plate and the high pressure inner seal head and can move freely relative to the low pressure outer casing. Besides, the reaction tube and the casing body are not in fixed connection, thereby eliminating heat expansion force and avoiding potential safety hazard that the welding joint of the tube plates and the casing body is spited.

Description

A kind of floating head type isothermal reaction methanol synthesis reactor
Technical field:
The utility model belongs to mechanical field, is specifically related to be used for the employed synthesis reactor of strong heat release isothermal reaction of chemical industry, petrochemical industry and other engineering, the synthetic tower of especially suitable methyl alcohol building-up reactions.
Background technology:
Present known strong heat release isothermal reaction, more use shell and tube-type reactor.Its basic structure is: two blocks of stationary tubesheets of upper and lower settings in reactor shell, and reaction tubes and housing weld with tube sheet simultaneously; Catalyzer places in the reaction tubes, relies on the boiling of the outer water of pipe (or liquid) to remove reaction heat.This kind structure is owing to exist thermal expansion force between reaction tubes and housing, the time regular meeting's generating pipe plate and housing weld seam by the phenomenon of drawing crack, serious threat is to production and personnel safety.
In order to reduce the destruction of thermal expansion force to equipment, the tube length of reaction tube of shell and tube-type reactor is shorter mostly, generally is controlled at 6~7m, and requires the linear expansivity of reaction tubes and shell material close.The tube and shell type methanol synthesis converter reaction tubes material that domestic methyl alcohol, synthetic ammonia industry are introduced the technology manufacturing of German LURGI is 2205 (duplex stainless steels), and shell material is 13MnNiMoNbR.So not only make the manufacturing cost of equipment high, the equipment of identical production capacity is because the restricted volume of tube length of reaction tube is huge, and influences the raising of transformation efficiency in the production process, reduced energy-saving effect.
The utility model content:
The purpose of this utility model is exactly to provide a kind of floating head type isothermal reaction methanol synthesis reactor of high efficiency, low cost in order to address the above problem, and it has overcome tube sheet and housing weld seam easily by the defective of drawing crack.
A kind of floating head type isothermal reaction methanol synthesis reactor described in the utility model, mainly comprise the low pressure body skin, the body skin lower cover, the high-temperature gas fairlead, the high pressure upper tube box, end socket in the high pressure, upper tubesheet, lower tubesheet, the reaction tubes of catalyzer is equipped with in inside, gas distributor and gas inlet tube, its mesohigh upper tube box, low pressure body skin and body skin lower cover are welded as a whole, gas inlet tube passes the high pressure upper tube box and enters its inside, at the gas feed tube end gas distributor is installed, upper tubesheet and lower tubesheet are installed in both sides up and down, low pressure body skin inside respectively, many reaction tubess are installed between upper tubesheet and the lower tubesheet, end socket is installed on the lower tubesheet in the high pressure, the high-temperature gas fairlead is welded on high pressure interior end socket bottom and extends the body skin lower cover, it is characterized in that: described upper tubesheet is fixedlyed connected with the low pressure body skin, running fit between lower tubesheet and the low pressure body skin, be equivalent to like this end socket in lower tubesheet and the high pressure is formed " floating head ", this floating head can move freely by the relatively low pressure body skin.
Adopt running fit between high-temperature gas fairlead and the body skin lower cover, can relatively move between the two, and seal with lock packing.The extension of high-temperature gas fairlead is equipped with expansion joint.
In high pressure upper tube box outside the discharging hand hole that is communicated with inside is housed, is convenient for changing the catalyzer in the high pressure upper tube box.
The utlity model has following advantage:
(1) because refrigerant (water) can triflux (heat transfer) reaction tubes outside, so fabulous temp effect such as grade is arranged.
(2) catalyzer or the protective material of upper tube box filling can draw off independent replacing by three hand holes that are provided with are all or part of.
(3) owing to do not fixedly connected between reaction tubes and housing, eliminated thermal expansion force, so there is not the potential safety hazard of tube sheet and the drawing crack of housing weld seam; Reaction tubes and shell material need not to have saved a large amount of noble metals with import or homemade duplex stainless steel, have reduced equipment manufacturing cost; The length of reaction tubes can extend according to the needs of reaction kinetics, thereby transformation efficiency is improved, and the device diameters of identical production capacity reduces.The difficult problem of large-scale reactor transportation is alleviated.
(4) the utility model reaction tubes can freely stretch in housing, " energy-saving and emission-reduction " technological transformation of the methyl alcohol of domestic low middling scale preferably, synthetic ammonia installation.
Description of drawings:
Fig. 1 is a structural representation of the present utility model.
Fig. 2 is the partial enlarged drawing at I place among Fig. 1.
Fig. 3 is the partial enlarged drawing at II place among Fig. 1.
Embodiment:
As shown in Figure 1, floating head type isothermal reaction methanol synthesis reactor of the present utility model, mainly comprise low pressure body skin 1, body skin lower cover 2, high-temperature gas fairlead 3, high pressure upper tube box 5, end socket 7 in the high pressure, upper tubesheet 8, lower tubesheet 9, the reaction tubes 11 of catalyzer is equipped with in inside, gas distributor 12 and gas inlet tube 13, its mesohigh upper tube box 5, low pressure body skin 1 and body skin lower cover 2 are welded as a whole, gas inlet tube 13 passes high pressure upper tube box 5 and enters its inside, gas distributor 12 is installed in gas inlet tube 13 ends, upper tubesheet 8 and lower tubesheet 9 are installed in low pressure body skin 1 inner both sides up and down respectively, upper tubesheet 8 is fixedlyed connected with low pressure body skin 1, running fit between lower tubesheet 9 and the low pressure body skin 1.Many reaction tubess 11 are installed between upper tubesheet 8 and the lower tubesheet 9, are equipped with in high pressure upper tube box 5 outsides to be communicated with inner discharging hand hole 6; End socket 7 is installed on the lower tubesheet 9 in the high pressure, high-temperature gas fairlead 3 is welded on interior end socket 7 bottoms of high pressure and extends body skin lower cover 2, adopt running fit (Fig. 2) between high-temperature gas fairlead 3 and the body skin lower cover 2, can relatively move between the two, and seal with lock packing.The extension of high-temperature gas fairlead 3 also is equipped with expansion joint 4 (Fig. 3), material dumping device 10 is installed in the end socket 7 in high pressure, can change catalyzer in the reaction tubes 11 easily by dumping device 10, be provided with water inlet pipe 14 in the bottom of body skin lower cover 2.
Basic functional principle of the present utility model: catalyzer is packed in the reaction tubes 11, the outer water (or liquid) that is full of of pipe, unreacted gas enters high pressure upper tube box 5 from inlet pipe 13, by gas distributor 12 uniformly with gas distribution to catalyst coating and enter reaction tubes, gas in by the process of reaction tubes catalyzer, react liberated heat managed outside water absorb, the steam of attached product is drawn by steam fairlead 15, and reacted gas is then led to outside the reactor by high-temperature gas fairlead 3.Between reaction tubes and the low pressure body skin 1, the relative displacement that produces because of heat expansion is passed to the high-temperature gas fairlead by " floating head ", by fairlead bellow expansion joint 4 compensation that are provided with; The displacement of high-temperature gas fairlead is then compensated by the reactor Outer Tube.So just eliminated the thermal expansion force that exists between conventional tube shell-type reactor reaction pipe and housing.
The utility model provides floating head type isothermal reaction methanol synthesis reactor thinking; should be understood that; for those skilled in the art; under the prerequisite that does not break away from the utility model principle; can also make some improvement and variation, these improvement and variation also should be considered as protection domain of the present utility model.

Claims (4)

1, a kind of floating head type isothermal reaction methanol synthesis reactor, mainly comprise low pressure body skin (1), body skin lower cover (2), high-temperature gas fairlead (3), high pressure upper tube box (5), end socket (7) in the high pressure, upper tubesheet (8), lower tubesheet (9), the reaction tubes (11) of catalyzer is equipped with in inside, gas distributor (12) and gas inlet tube (13), its mesohigh upper tube box (5), low pressure body skin (1) and body skin lower cover (2) are welded as a whole, gas inlet tube (13) passes high pressure upper tube box (5) and enters its inside, gas distributor (12) is installed in gas inlet tube (13) end, upper tubesheet (8) and lower tubesheet (9) are installed in the inner both sides up and down of low pressure body skin (1) respectively, many reaction tubess (11) are installed between upper tubesheet (8) and the lower tubesheet (9), end socket (7) is installed on the lower tubesheet (9) in the high pressure, high-temperature gas fairlead (3) is welded on high pressure interior end socket (7) bottom and extends body skin lower cover (2), it is characterized in that: described upper tubesheet (8) is fixedlyed connected with low pressure body skin (1), running fit between lower tubesheet (9) and the low pressure body skin (1).
2, floating head type isothermal reaction methanol synthesis reactor according to claim 1 is characterized in that: adopt running fit between high-temperature gas fairlead (3) and the body skin lower cover (2), can relatively move between the two, and seal with lock packing.
3, floating head type isothermal reaction methanol synthesis reactor according to claim 1 and 2 is characterized in that: the extension of high-temperature gas fairlead (3) is equipped with expansion joint (4).
4, floating head type isothermal reaction methanol synthesis reactor according to claim 1 and 2 is characterized in that: the discharging hand hole (6) that is communicated with inside is housed in high pressure upper tube box (5) outside.
CNU2008202158221U 2008-11-27 2008-11-27 Floating-head type isothermal reaction methyl alcohol synthetic reactor Expired - Fee Related CN201309898Y (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNU2008202158221U CN201309898Y (en) 2008-11-27 2008-11-27 Floating-head type isothermal reaction methyl alcohol synthetic reactor

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNU2008202158221U CN201309898Y (en) 2008-11-27 2008-11-27 Floating-head type isothermal reaction methyl alcohol synthetic reactor

Publications (1)

Publication Number Publication Date
CN201309898Y true CN201309898Y (en) 2009-09-16

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Cited By (5)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102160981A (en) * 2010-02-24 2011-08-24 杭州林达化工技术工程有限公司 Catalytic reaction equipment
CN101514142B (en) * 2009-03-12 2012-10-03 南京昊安科技工程有限公司 Self-unloading floating head isothermal reaction methanol synthesis reactor
CN103566836A (en) * 2013-11-25 2014-02-12 南京国昌化工科技有限公司 Uniform-temperature hydrogenation reactor
CN105967976A (en) * 2016-05-09 2016-09-28 山西阳煤化工机械(集团)有限公司 Methanol synthetic tower with high efficiency and high pressure
CN107570088A (en) * 2017-10-10 2018-01-12 湖南安淳高新技术有限公司 The catalyst uninstalling system and discharging method of a kind of shell-and-tube reactor

Cited By (7)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101514142B (en) * 2009-03-12 2012-10-03 南京昊安科技工程有限公司 Self-unloading floating head isothermal reaction methanol synthesis reactor
CN102160981A (en) * 2010-02-24 2011-08-24 杭州林达化工技术工程有限公司 Catalytic reaction equipment
CN102160981B (en) * 2010-02-24 2015-01-07 杭州林达化工技术工程有限公司 Catalytic reaction equipment
CN103566836A (en) * 2013-11-25 2014-02-12 南京国昌化工科技有限公司 Uniform-temperature hydrogenation reactor
CN105967976A (en) * 2016-05-09 2016-09-28 山西阳煤化工机械(集团)有限公司 Methanol synthetic tower with high efficiency and high pressure
CN107570088A (en) * 2017-10-10 2018-01-12 湖南安淳高新技术有限公司 The catalyst uninstalling system and discharging method of a kind of shell-and-tube reactor
CN107570088B (en) * 2017-10-10 2023-11-17 湖南安淳高新技术有限公司 Catalyst unloading system and method for shell-and-tube reactor

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Legal Events

Date Code Title Description
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Anhui Sunson Chemical Co., Ltd.

Assignor: Nanjing Hao Hao science and Technology Engineering (industrial equipment) Co., Ltd.

Contract record no.: 2011340000145

Denomination of utility model: Floating-head type isothermal reaction methyl alcohol synthetic reactor

Granted publication date: 20090916

License type: Exclusive License

Record date: 20110720

CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20090916

Termination date: 20161127