CN1947570A - Method for producing capsule contg. super-fine powder of grape seeds - Google Patents
Method for producing capsule contg. super-fine powder of grape seeds Download PDFInfo
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- CN1947570A CN1947570A CNA2006101048643A CN200610104864A CN1947570A CN 1947570 A CN1947570 A CN 1947570A CN A2006101048643 A CNA2006101048643 A CN A2006101048643A CN 200610104864 A CN200610104864 A CN 200610104864A CN 1947570 A CN1947570 A CN 1947570A
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Abstract
A process for preparing the health-care capsules of superfine grape seed powder includes such steps as collecting grape seeds, storage, screening, washing, baking, freezing, adding disperser, superfine pulverizing, packing and sterilizing.
Description
One, technical field:
The present invention relates to a kind of method for producing of grape byproduct, especially relate to a kind of production method of grape pip ultra micro powder capsule.
Two, background technology:
At present, China's grape wine industry has entered new developing period, and industrialized development has certain scale, produces more than 20,000 ton of grape pip every year approximately, and major part goes out of use.The very big pollution that this not only can cause environment also causes the huge waste of resource.Grape is the fruit that people like, people have just recognized the medicinal and nutritive value of grape before several thousand, and grape pip accounts for the 3-6% of grape berry gross weight.Up to the present, from grape pip, isolate the number of chemical composition, wherein be mainly concerned with compositions such as fatty oils, flavones and Polyphenols, particularly glucosidase procyanidins (OPCs), protein.Though also contain these compositions in Grape Skin, grape juice and the grape wine, its content much lower than in the grape pip.In addition, also contain multiple mineral element in the grape pip.
Fat content is abundant in the grape pip, generally is about 14%-17%.In general, in the red grape pip content of oil than the height of white grape pip, the grape variety that sugar content is high, oil content is also high in its grape pip.A large amount of unrighted acids are arranged in the grape-kernel oil, and its mass fraction is up to more than 90%, and is close with soybean, Fructus Hordei Germinatus fat content.Wherein linoleic acid content reaches more than 70%, and than general edible oil, even medicinal oil (walnut oil and safflower oil) is all high.Also contain 20 various trace elements in the grape-kernel oil, as Mg, Ca, K, Na, Fe, Cu, Zn, Mn, Co, and VA, VC, VD, VE etc., wherein contain VE360mg/kg, contain beta carotene 42.55mg/kg, phytosterol content can reach 50mg/kg.
Polyphenols in the grape pip is that content or kind are all much abundant than Grape Skin and grape berry, and the content of polyphenol is in the carpopodium 2.4 times, pericarp 4.3 times, 32.5 times of claret approximately in the grape pip.The polyphenol mixture that extracts from grape pip, people are commonly referred to grape seed extract, and (Grape seedextract, GSE), generally between 75-95%, total phenol content mostly is about 85% its total phenol content among China GSE.The product of GSE is considered to quick, strong antioxidant, and its antioxidant is more effective than VC or VE.
PROANTHOCYANIDINS OF GRAPE SEEDS has superpower oxidation resistance, the heart, cranial vascular disease etc. is had tangible curative effect according to the study, but Polyglucan, anti-ageing, alleviate injury gained in sports and arthralgia, anti-inflammatory and with the free radical diseases associated.Secondly, the linoleic acid in the grape pip has health-care effects such as radioresistance, norcholesterol and anti arteriosclerosis, and also has nutritional labelings such as amounts of protein, cellulose to be utilized in the grape pip.The processing of grape pip only was confined to the separation and Extraction of single component or several compositions, this just causes the waste of losing of other functional components or resource in the past, and simultaneously, may there be potential safety hazard in the organic chemicals that uses when separation and Extraction.
Superfine communication technique is the new technology that the mid-80 grows up, it is to be accompanied by the new comminution engineering technology that Modern High-Tech and new material industry and conventional industries technology, comprehensive utilization of resources, deep processing etc. grow up, ultramicro grinding for Chinese medicine and health food, mainly be meant the ultramicro grinding (abbreviation breaking-wall cell) of cell grade, it is not purpose with the smashing fineness, but pursues the sporoderm-broken rate of cell.Raw material is behind breaking-wall cell, and intracellular active ingredient fully comes out.After entering in the body, soluble component dissolves rapidly, even the low composition of solubility also tightly sticks on the mucous membrane because of ultrafine powder has bigger adhesive force, thereby helps the absorption of active ingredient.And the adhesive force of these active ingredients increased its time of staying in vivo, and it shortens to the required time of the process of extracellular migration in plant cell simultaneously, and this not only makes absorption of human body speed obviously increase, and uptake also has remarkable increase.
Three, summary of the invention:
The present invention is in order to solve the weak point in the above-mentioned background technology, a kind of production method of grape pip ultra micro powder capsule is provided, the method of its application of pure physics, ultra micro powder technology is applied in the deep processing of grape pip, the grape pip ultra micro powder capsule that obtains, can keep the various nutritional labelings in the grape pip to greatest extent, and make wherein functional components can be fast, comprehensively be absorbed by the body, be a kind of novel health food.
For achieving the above object, the technical solution used in the present invention is:
A kind of production method of grape pip ultra micro powder capsule, its special character are to comprise following operating procedure: the collection of (1) grape pip raw material; (2) store; (3) select cleaning; (4) oven dry; (5) freezing; (6) add anticaking agent; (7) ultra micro powder processing; (8) packing; (9) sterilization.
In the collection step of grape pip raw material, the moisture of grape pip is less than 10%; Aflatoxin in the grape pip is no more than 20ug/kg.
In baking step, clean the back grape pip and enter aeration cabinet immediately, equal till 8% up to moisture after the drying.
In freezing step, cryogenic temperature is between-15 ℃～-20 ℃, and the time is between 40min-80min; The grape pip that freezes is put into rapidly and has been met the requirements of pulverizer.
In adding the anticaking agent process, the anticaking agent of interpolation is a microcrystalline cellulose, and addition is 30g/kg～40g/kg.
In ultra micro powder procedure of processing: cryogenic temperature is-25 ℃～-30 ℃ before pulverizing, and the pulverizing time is 25～35min.
Compared with prior art, the advantage and the effect that have of the present invention is as follows:
1, the method for application of pure physics of the present invention; ultra micro powder technology is applied in the deep processing of grape pip; avoided unsafe factor and thermal sensitivity function in the separation and Extraction process to lose fully; keep the various nutritional labelings in the grape pip to greatest extent; finally determined the production method of best grape pip ultra micro powder capsule; formulated rational industrialized producing technology flow process, grape pip ultra micro powder capsule is produced on a large scale.
2, the present invention has kept the various nutritional labelings in the grape pip to greatest extent, as protein, vine polyphenol (grape proanthocyanidin, resveratrol etc.), linoleic acid, dietary fiber, trace element, VA, VC, VD, VE, beta carotene etc., be a health product balanced in nutrition.
3, the oven dry among the present invention, freezing, add anticaking agent, the ultra micro powder is processed the aridity in each step; Cryogenic temperature; Anticaking agent kind and addition; Technological parameters such as cryogenic temperature in the ultra micro powder processing and pulverizing time are through drawing on a large amount of experiment basis, can avoid unsafe factor and thermal sensitivity function in the separation and Extraction process to lose fully, keep the various nutritional labelings in the grape pip to greatest extent.
Four, description of drawings:
Accompanying drawing is a process chart of the present invention.
Five, the specific embodiment:
The present invention includes following operating procedure: the collection of (1) grape pip raw material; (2) store; (3) select cleaning; (4) oven dry; (5) freezing; (6) add the processing of anticaking agent (7) ultra micro powder; (8) packing; (9) sterilization.Promptly earlier to raw material low temperature drying, superfreeze, add anticaking agent then, carry out ultramicro grinding under ultralow temperature, in the desinfection chamber inner packing, sterilization at last obtains product.
Embodiment one:
1, the collection of grape pip raw material: raw material checks that supplier's grape pip source place environment proves when receiving, not the collecting of no safety assurance; Utilize sense organ to judge look, the flavor of grape pip, unusual does not collect, and does not damaged by verminly collect; Press the assay method of moisture in the GB/T5009.3 food, measure the moisture of grape pip, do not receive greater than 10%; Press the aflatoxin in the GB/T5009.25-2003 standard test grape pip, surpass 20ug/kg and do not receive.
2, store: conscientiously carry out the storehouse safety inspection before the grape pip warehouse-in, guarantee the firm safety in warehouse, rain-tight, not moist, door and window is complete, possesses firm, moistureproof, heat insulation, ventilation, performance such as airtight.Before the warehouse-in, clear up completely, foreign material and dust are cleaned out, and fumigate and sterilize, should in time ventilate after sterilization is finished, to reduce the influence of poor environment as far as possible to raw material to storehouse to storehouse; Storage person is careful and responsible, makes regular check on the storehouse storage temperature, relative humidity, and the ventilation situation prevents that the grape pip mildew phenomena from taking place.
3, select cleaning: it is careful and responsible that personnel are chosen in choosing, firmly rejects not reaching requirement; Water for cleaning meets the GB5749 drinking water sanitary standard; Accelerate cleaning speed, reduce soak time.
4, oven dry: check drying equipment before dry, guarantee that the dry run machine run is normal; Clean the back grape pip and enter aeration cabinet at once, equal till 8% up to moisture after the drying.
5, freezing: as to check refrigerator before freezing, guarantee to work well between the refrigerator pool period; Guarantee cryogenic temperature at-15 ℃, the time is at 40min; The grape pip that freezes is put into rapidly and has been met the requirements of pulverizer.
6, add anticaking agent: according to the interpolation process of GB2760-1996 " food additives use sanitary standard " control additive; Additive therefor must be the qualified products that quality assurance is arranged.The anticaking agent that adds is a microcrystalline cellulose, and addition is 30g/kg.
7, ultra micro powder processing: check the pulverizer and the refrigeration machine of micronizer before pulverizing, guarantee that it is good during operation; Atomizer must carry out cleaning and sterilizing before pulverizing; Refrigeration must reach-25 ℃ before pulverizing, and pulverizes time 25min.
8, packing: the powder of accomplishing fluently is packed at desinfection chamber; The packing capsule shells satisfies the national quality requirement; The packing net content meets country's " quantification packing commodity supervision regulation ".
9, sterilization: total number of bacteria, coliform count, pathogenic bacteria, the mould of sterilization back product all meets country's health care (function) food universal standard (GB 16740-1997).
Embodiment two:
1, the collection of grape pip raw material: raw material checks that supplier's grape pip source place environment proves when receiving, not the collecting of no safety assurance; Utilize sense organ to judge look, the flavor of grape pip, unusual does not collect, and does not damaged by verminly collect; Press the assay method of moisture in the GB/T5009.3 food, measure the moisture of grape pip, do not receive greater than 10%; Press the aflatoxin in the GB/T5009.25-2003 standard test grape pip, surpass 20ug/kg and do not receive.
2, store: conscientiously carry out the storehouse safety inspection before the grape pip warehouse-in, guarantee the firm safety in warehouse, rain-tight, not moist, door and window is complete, possesses firm, moistureproof, heat insulation, ventilation, performance such as airtight.Before the warehouse-in, clear up completely, foreign material and dust are cleaned out, and fumigate and sterilize, should in time ventilate after sterilization is finished, to reduce the influence of poor environment as far as possible to raw material to storehouse to storehouse; Storage person is careful and responsible, makes regular check on the storehouse storage temperature, relative humidity, and the ventilation situation prevents that the grape pip mildew phenomena from taking place.
3, select cleaning: it is careful and responsible that personnel are chosen in choosing, firmly rejects not reaching requirement; Water for cleaning meets the GB5749 drinking water sanitary standard; Accelerate cleaning speed, reduce soak time.
4, oven dry: check drying equipment before dry, guarantee that the dry run machine is good; Clean the back grape pip and enter aeration cabinet at once, equal till 8% up to moisture after the drying.
5, freezing: as to check refrigerator before freezing, guarantee between the refrigerator pool period good; Guarantee cryogenic temperature at-20 ℃, the time is at 80min; The grape pip that freezes is put into rapidly and has been met the requirements of pulverizer.
6, add anticaking agent: according to the interpolation process of GB2760-1996 " food additives use sanitary standard " control additive; Additive therefor must be the qualified products that quality assurance is arranged.The anticaking agent that adds is a microcrystalline cellulose, and addition is 40g/kg.
7, ultra micro powder processing: check the pulverizer and the refrigeration machine of micronizer before pulverizing, guarantee that it is good during operation; Atomizer must carry out cleaning and sterilizing before pulverizing; Refrigeration must reach-30 ℃ before pulverizing, and pulverizes time 35min.
8, packing: the powder of accomplishing fluently is packed at desinfection chamber; The packing capsule shells satisfies the national quality requirement; The packing net content meets country's " quantification packing commodity supervision regulation ".
9, sterilization: total number of bacteria, coliform count, pathogenic bacteria, the mould of sterilization back product all meets country's health care (function) food universal standard (GB 16740-1997).
Product quality is among the present invention: outward appearance is the yellowish-brown powder, fine granularity≤25 μ m, moisture≤8%, total number of bacteria/(cfu/g)≤30000 reference: health care (function) food universal standard (GB16740-1997), coliform/(MPN/100g)≤90, mould/(cfu/g)≤25, no pathogenic bacteria.
Claims (6)
1, a kind of production method of grape pip ultra micro powder capsule is characterized in that comprising following operating procedure: the collection of (1) grape pip raw material; (2) store; (3) select cleaning; (4) oven dry; (5) freezing; (6) add anticaking agent; (7) ultra micro powder processing; (8) packing; (9) sterilization.
2, the production method of a kind of grape pip ultra micro powder capsule according to claim 1 is characterized in that: in the collection step of grape pip raw material, the moisture of grape pip is less than 10%; Aflatoxin in the grape pip is no more than 20ug/kg.
3, the production method of a kind of grape pip ultra micro powder capsule according to claim 2 is characterized in that: oven dry: in baking step, clean the back grape pip and enter aeration cabinet immediately, equal till 8% up to moisture after the drying.
4, the production method of a kind of grape pip ultra micro powder capsule according to claim 3 is characterized in that: in freezing step, cryogenic temperature is between-15 ℃～-20 ℃, and the time is between 40min-80min; The grape pip that freezes is put into rapidly and has been met the requirements of pulverizer.
5, the production method of a kind of grape pip ultra micro powder capsule according to claim 4 is characterized in that: in adding the anticaking agent process, the anticaking agent of interpolation is a microcrystalline cellulose, and addition is 30g/kg～40g/kg.
6, the production method of a kind of grape pip ultra micro powder capsule according to claim 5 is characterized in that: in ultra micro powder procedure of processing: cryogenic temperature is-25 ℃～-30 ℃ before pulverizing, and the pulverizing time is 25～35min.
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Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN103211227A (en) * | 2013-05-07 | 2013-07-24 | 扬州大学 | Method for preparing ultramicro dietary supplement from grape seeds and wine lees materials |
| CN104473271A (en) * | 2014-11-28 | 2015-04-01 | 中国科学院过程工程研究所 | Preparation method of grape seed ultrafine powder suspending beverage |
| CN104543817A (en) * | 2013-10-29 | 2015-04-29 | 中国科学院广州生物医药与健康研究院 | Blueberry seed powder as well as preparation method and application of blueberry seed powder |
| CN105454454A (en) * | 2016-01-16 | 2016-04-06 | 李义民 | Preparation method of grape pip and fruity soybean milk powder |
| CN107397159A (en) * | 2017-01-09 | 2017-11-28 | 西北农林科技大学 | A kind of preparation method and its chewable tablets of the high meals Kiwi berry Ultramicro-powder of energy defaecation |
| CN110433230A (en) * | 2012-04-30 | 2019-11-12 | 索那麦提科有限责任公司 | The therapeutical uses of Chardonnay seed products |
| CN110558499A (en) * | 2019-09-19 | 2019-12-13 | 福建启元堂生物技术有限公司 | Pretreatment method for double-super-extraction of marine nutrients |
| CN110575680A (en) * | 2019-09-19 | 2019-12-17 | 福建启元堂生物技术有限公司 | Method for double super-extraction of marine nutrients |
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2006
- 2006-11-07 CN CNB2006101048643A patent/CN100571537C/en active Active
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN110433230A (en) * | 2012-04-30 | 2019-11-12 | 索那麦提科有限责任公司 | The therapeutical uses of Chardonnay seed products |
| CN103211227A (en) * | 2013-05-07 | 2013-07-24 | 扬州大学 | Method for preparing ultramicro dietary supplement from grape seeds and wine lees materials |
| CN104543817A (en) * | 2013-10-29 | 2015-04-29 | 中国科学院广州生物医药与健康研究院 | Blueberry seed powder as well as preparation method and application of blueberry seed powder |
| CN104473271A (en) * | 2014-11-28 | 2015-04-01 | 中国科学院过程工程研究所 | Preparation method of grape seed ultrafine powder suspending beverage |
| CN105454454A (en) * | 2016-01-16 | 2016-04-06 | 李义民 | Preparation method of grape pip and fruity soybean milk powder |
| CN107397159A (en) * | 2017-01-09 | 2017-11-28 | 西北农林科技大学 | A kind of preparation method and its chewable tablets of the high meals Kiwi berry Ultramicro-powder of energy defaecation |
| CN107397159B (en) * | 2017-01-09 | 2021-08-27 | 西北农林科技大学 | Preparation method of high-meal kiwi fruit superfine powder capable of relaxing bowels and chewable tablet thereof |
| CN110558499A (en) * | 2019-09-19 | 2019-12-13 | 福建启元堂生物技术有限公司 | Pretreatment method for double-super-extraction of marine nutrients |
| CN110575680A (en) * | 2019-09-19 | 2019-12-17 | 福建启元堂生物技术有限公司 | Method for double super-extraction of marine nutrients |
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| CN100571537C (en) | 2009-12-23 |
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