CN1927229A - Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete - Google Patents

Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete Download PDF

Info

Publication number
CN1927229A
CN1927229A CN 200610053216 CN200610053216A CN1927229A CN 1927229 A CN1927229 A CN 1927229A CN 200610053216 CN200610053216 CN 200610053216 CN 200610053216 A CN200610053216 A CN 200610053216A CN 1927229 A CN1927229 A CN 1927229A
Authority
CN
China
Prior art keywords
vacuum
dry thing
automatic
conveyer belt
cooling
Prior art date
Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
Granted
Application number
CN 200610053216
Other languages
Chinese (zh)
Other versions
CN100458337C (en
Inventor
刘雪松
陈勇
瞿海斌
谢志鹏
王龙虎
程翼宇
Current Assignee (The listed assignees may be inaccurate. Google has not performed a legal analysis and makes no representation or warranty as to the accuracy of the list.)
Zhejiang University ZJU
Original Assignee
Zhejiang University ZJU
Priority date (The priority date is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the date listed.)
Filing date
Publication date
Application filed by Zhejiang University ZJU filed Critical Zhejiang University ZJU
Priority to CNB200610053216XA priority Critical patent/CN100458337C/en
Publication of CN1927229A publication Critical patent/CN1927229A/en
Application granted granted Critical
Publication of CN100458337C publication Critical patent/CN100458337C/en
Expired - Fee Related legal-status Critical Current
Anticipated expiration legal-status Critical

Links

Images

Landscapes

  • Drying Of Solid Materials (AREA)

Abstract

The invention relates to a method for producing porous loose traditional medicine concrete dry matter, and relative device. Wherein, it comprises vacuum system, heater, cooler, material feeding distributor, material transmitter, discharge system, automatic washing system, and automatic control system. Said concrete matter is preheated in feeding pot, via preset feeding speed and distributor to be coated on the transmission band; in vacuum, transmitting it via heating area and cooling area to obtain porous loose pan dry matter; removing it from the transmission band, to be cut by cutter into broker; and discharging via discharger. The invention processes low-temperature continuous dry in vacuum, to improve the producing ability, while the dry process is warm and quick, and the operation condition can meet GMP demand. The product has shadow color, better dissolving ability. And the invention has automatic control, to reduce labor density and improve working efficiency.

Description

The production method and the equipment of the dry thing of a kind of Chinese medical concrete of porosity and looseness
Technical field
The present invention relates to a kind of production method and equipment of the dry thing of Chinese medical concrete of porosity and looseness, the dry thing that obtains by this method has lighter color, porosity and looseness, characteristics that dissolubility is good, the Chinese medical concrete material that is particularly useful for viscosity height, thermoplasticity, thermal sensitivity belongs to herbal pharmaceutical industrial technology field.
Background technology
The Chinese medical concrete drying is requisite operation in the Chinese medicine preparation production process, and the drying means of Chinese medical concrete mainly contains vacuum drying oven drying, vacuum lyophilization and spray drying at present.These several drying meanss all exist certain defective and the limitation of self.The vacuum drying oven drying can not continuous operation, and drying time is long, and production capacity is little, and energy consumption is big; Need at high temperature manually to stir and discharging, severe operational environment easily causes the cross-contamination of people and storeroom; Dark, the easy caking of dry products color and luster, poorly soluble.Though vacuum lyophilization can obtain high-quality dehydrating prods,, power consumption little because of its production capacity limited its applying in the Chinese medical concrete drying greatly.Spray-dired shortcoming is the device structure complexity, and floor space is big, the cost height; And the Chinese medical concrete sugar content than higher, viscosity is big, has serious sticking wall problem, makes spray-dired yield generally lower, have only about 20% usually.
At present about the existing patent report of the continuous vacuum drying equipment of paste, utility model patent ZL200420079264.2 " plaster material vacuum drying machine host " and ZL01263428.X " vacuum thick glue drying machine " carry out continuous operation though disclosed vacuum drier can satisfy under vacuum state, but the deficiency that also has following several respects: (1) mode of heating is unreasonable, the live (open) steam heating easily produces overheated, coking phenomenon, has a strong impact on product quality; Adopt conduction oil not meet the GMP requirement as heat medium; Adopt 2 sections thermals treatment zone to be difficult to satisfy the exsiccant needs of Chinese medical concrete, and the adjustable temperature range of cooling zone is too narrow, especially can not satisfy the dry requirement of thermoplasticity extractum material; (2) solvent species of Chinese medical concrete is various, can be water and lower boiling organic solvent, and above-mentioned utility model is not considered lower boiling Recovery of Organic Solvent, makes the scope of application of this method and apparatus be subjected to certain restriction.(3) automaticity of above-mentioned utility model is lower, is not real serialization production, and discharging and row's condensed fluid all need manually-operated; For the sideslip problem that occurs in the conveyer belt long-time continuous running, do not extract solution, be difficult to satisfy industrial production requirement.
Summary of the invention
The objective of the invention is to exist that energy consumption is big, automatization level is low, the deficiency of dry products presentation quality difference, a kind of production method of the dry thing of Chinese medical concrete of porosity and looseness is provided at present Chinese medical concrete drying means and drying equipment.
The production method of the dry thing of the Chinese medical concrete of a kind of porosity and looseness of the present invention is achieved through the following technical solutions: be coated on Chinese medical concrete on the conveyer belt equably under vacuum condition, carry out the low temperature continuous drying, Chinese medical concrete is in the head tank preheating, feeding temperature is controlled at 30~60 ℃, then by the charging rate of screw feed pump by 1~10kg/h, be coated on the conveyer belt equably by distributing device, conveyer belt is by the translational speed operation of 3~24m/h, under vacuum condition, the extractum material moves successively through each thermal treatment zone, pass through the cooling zone at last, form a kind of porous, the dry thing of loose pie, thermal treatment zone hot aqueous medium's adjustable temperature range is 40~80 ℃, the adjustable temperature range of cooling zone cooling water medium is 20~-1 ℃, wherein 5~-1 ℃ cooling water is provided by handpiece Water Chilling Units, when dry thing arrives equipment terminal, being peeled off device by product scrapes off from conveyer belt, after cutting off, shearing device falls into strand cage destructor, dry thing after the pulverizing promptly gets the dry thing of Chinese medical concrete of porosity and looseness by having the drawing mechanism discharging of two pneumatic dish valves.
But another object of the present invention provides the low-temperature vacuum drying equipment of full-automatic, the totally-enclosed continuous operation of realizing said method, comprises vacuum system, heating, cooling system, the charging cloth system, material-transporting system, discharge system, automatic cleaning system and automatic control system.Vacuum system has Roots's water ring vacuum unit and the condenser that is connected on the vacuum cavity, and vacuum cavity has heat-insulation layer, is connected with vacuum buffer tank and condensed fluid collecting tank between vacuum unit and condenser; Heating, cooling system have three sections thermals treatment zone and one section cooling zone; The charging cloth system has the head tank of band temperature control and agitator, and the screw feed pump is connected with distributing device by feed pipe, and the pendulum angle of distributing device fork is 10~50 °; Material-transporting system has the politef conveyer belt, and the front end of conveyer belt, rear end are separately fixed on driven shaft, the driving shaft, and driving shaft is by the motor decelerating mechanism driven rotary, and driven shaft is fixed on the conveyer stretcher, and links to each other with automatic deviation correction mechanism; Discharge system has the product that is in the vacuum cavity rear end and peels off device, shearing device, strand cage destructor, and the discharging opening of vacuum cavity is connected with drawing mechanism; Automatic cleaning system has booster pump and two detergent lines, and every detergent line has the 12 cleaning shower nozzles of 360 ° of rotations only; Automatic control system has PLC electrical control cabinet and touch screen operation interface.
The rear and front end of described vacuum cavity has two pneumostop doors, and on the pneumostop door travel switch is installed, and is used to the interlocked control that realizes that two hermatic doors can not be opened simultaneously, to satisfy the requirement of GMP.
The cooling medium of described condenser can be tap water (20 ℃) or industrial chilled water (5~-1 ℃), and industrial chilled water is provided by handpiece Water Chilling Units, is applicable to the dry run of low boiling point organic solvent as the extractum material of solvent.
Have photoelectricity liquid-level switch, condensed fluid feed liquor valve, balanced valve, atmospheric valve, condensed fluid tapping valve on the described condensed fluid collecting tank, realize the automatic row's condensed fluid in the unit running process.
Described automatic deviation correction mechanism has photo-electric near switch and cylinder, promotes the horizontal level that conveyer stretcher is regulated conveyer belt by cylinder, prevents that conveyer belt from deviation phenomenon taking place in running.
Described drawing mechanism has the dry thing transfer jar that is connected with the discharging opening of vacuum cavity, the dry thing collecting tank that links to each other with dry thing transfer jar and the pneumatic dish valve between them, to be implemented in the seriality operation of carrying out the product discharging under the vacuum state and not influencing whole dry run; And dry thing transfer jar has cooling system, is applicable to the further cooling of the dry thing of thermoplastic blocks of solid, improves the fragility of dry thing.
Whole automatic low temperature continuous vacuum drying equipment has PLC electrical control cabinet and touch screen operation interface.
The invention has the beneficial effects as follows:
(1) the low temperature continuous drying is carried out in employing under vacuum condition, whole dry run gentleness (operating temperature 40-80 ℃), drying time lack, the rerum natura that can keep material to greatest extent, the dry products that obtains by this method has lighter color, porosity and looseness, characteristics that dissolubility is good, is particularly useful for the Chinese medical concrete material of viscosity height, thermoplasticity, thermal sensitivity.
(2) solved the problem that present paste continuous vacuum drying equipment exists, make its scope of application wider, really realized the Automatic Control of unit, comprise automatic deviation correction control, hermatic door interlocked control, arrange condensed fluid control, cleaning control etc. automatically automatically, and parameters such as conveyer belt speed, charging rate, temperature and vacuum all can onlinely be regulated.
(3) the inventive method and device therefor are reasonable in design, and be easy and simple to handle, and the equipment making cost is low.
Description of drawings
Fig. 1 is an equipment structure chart of the present invention.
Fig. 2 is a process chart of the present invention.
Fig. 3 is the sketch map of automatic deviation correction mechanism.
Fig. 4 is the sketch map of drawing mechanism.
The specific embodiment
The present invention is further described in conjunction with the accompanying drawings and embodiments.
Embodiment 1
Referring to Fig. 1~4, full-automatic low temperature continuous vacuum drying equipment of the present invention comprises vacuum system (1), heating, cooling system (2), charging cloth system (3), material-transporting system (4), discharge system (5), automatic cleaning system (6) and automatic control system (7).Vacuum system (1) has Roots's water ring vacuum unit (1-1) and is connected condenser (1-3) on the vacuum cavity (1-2), vacuum cavity has heat-insulation layer, be connected with vacuum buffer tank (1-4) and condensed fluid collecting tank (1-5) between vacuum unit (1-1) and condenser (1-3), steam in the dry run or organic vapor enter condensed fluid collecting tank (1-5) after condenser (1-3) condensation.Heating, cooling system (2) have three sections thermals treatment zone (2-1,2-2,2-3) and one section cooling zone (2-4), thermal treatment zone hot aqueous medium's adjustable temperature range is 40~80 ℃, the adjustable temperature range of cooling zone cooling water medium is 20~-1 ℃, and wherein 5~-1 ℃ cooling water is provided by handpiece Water Chilling Units (2-5).Charging cloth system (3) has the head tank (3-2) of band temperature control and agitator, (3-1) is the extractum material, and screw feed pump (3-3) is connected with distributing device (3-4) by feed pipe (3-6).Material-transporting system (4) has politef conveyer belt (4-1), the front end of conveyer belt, rear end are separately fixed on driven shaft (4-2), the driving shaft (4-3), driving shaft (4-3) is by the motor decelerating mechanism driven rotary, driven shaft (4-2) is fixed on the conveyer stretcher (4-4), and links to each other with automatic deviation correction mechanism (4-5).Discharge system (5) has the product that is in vacuum cavity (1-2) rear end and peels off device (5-2), shearing device (5-3), strand cage destructor (5-4), and the discharging opening of vacuum cavity (1-2) is connected with drawing mechanism (5-5).Automatic cleaning system (6) has booster pump (6-1) and two detergent lines (6-2), and every detergent line has the 12 cleaning shower nozzles (6-3) of 360 ° of rotations only.Automatic control system (7) has PLC electrical control cabinet (7-1) and touch screen operation interface (7-2).
Referring to Fig. 1, have photoelectricity liquid-level switch (1-6), condensed fluid feed liquor valve (1-7), balanced valve (1-8), atmospheric valve (1-9), condensed fluid tapping valve (1-10) on the condensed fluid collecting tank (1-5), realize the automatic row's condensed fluid in the unit running process.When the condensed fluid in the condensed fluid collecting tank (1-5) arrives the liquid level of setting, photoelectricity liquid-level switch (1-6) is opened, start row's condensate system automatically, close condensed fluid feed liquor valve (1-7) and balanced valve (1-8), open atmospheric valve (1-9) and condensed fluid tapping valve (1-10); After condensed fluid drains, close atmospheric valve (1-9) and condensed fluid tapping valve (1-10), open condensed fluid feed liquor valve (1-7) and balanced valve (1-8), proceed condensed fluid and collect.
Referring to Fig. 3, automatic deviation correction mechanism (4-5) has photo-electric near switch (4-5-1) and cylinder (4-5-2), when photo-electric when detecting displacement signal, promotes horizontal level that conveyer stretcher (4-4) regulate conveyer belt (4-1) by cylinder (4-5-2) near switch (4-5-1).
Referring to Fig. 4, drawing mechanism (5-5) has the dry thing transfer jar (5-8) that is connected with the discharging opening of vacuum cavity (1-2), the dry thing collecting tank (5-9) that links to each other with dry thing transfer jar (5-8), and dry thing transfer jar (5-8) has chuck, can link to each other with handpiece Water Chilling Units (2-5), be applicable to the further cooling of the dry thing of thermoplastic blocks of solid, improve the fragility of dry thing.
Full-automatic low temperature continuous vacuum drying equipment can be provided with charging cloth system (3), material-transporting system (4) and heating, the cooling systems (2) organized as required, to enlarge the production capacity of equipment.
Whole automatic low temperature continuous vacuum drying equipment has PLC electrical control cabinet (7-1) and touch screen operation interface (7-2).
Embodiment 2
Referring to Fig. 1-4, the production method of the dry thing of the Chinese medical concrete of porosity and looseness of the present invention is under vacuum condition extractum material (3-1) to be coated on the conveyer belt (4-1) equably, carries out the low temperature continuous drying.Extractum material (3-1) preheating in head tank (3-2), feeding temperature is controlled at 30~60 ℃, after the vacuum (being generally 400pa) that reaches setting in the vacuum cavity (1-2), by the charging rate of screw feed pump (3-3) by 1~10kg/h, by distributing device (3-4) the extractum material is coated on the conveyer belt (4-1) equably, conveyer belt moves through each thermal treatment zone (2-1,2-2,2-3) successively by the speed operation of 3~24m/h, at last by cooling zone (2-4).Under vacuum environment, the evaporation rapidly of extractum material heat absorption back, steam or organic vapor enter condensed fluid collecting tank (1-5) after condenser (1-3) condensation.Dried dry thing (5-1) is peeled off device (5-2) by product and peels off from conveyer belt (4-1), falls into strand cage destructor (5-4) after shearing device (5-3) cuts off, and the dry thing after the pulverizing is by drawing mechanism (5-5) discharging.The charging of whole dry run and discharging are in mode of operation totally-enclosed, serialization, and by automatic control system (7) operating parameters such as conveyer belt speed, charging rate, temperature and vacuum are controlled in real time and regulated.
Embodiment 3:
Referring to Fig. 1-4, the production method and the equipment of the dry thing of the Chinese medical concrete of porosity and looseness of the present invention, operating process is as follows: the automatic control system (7) of opening full-automatic low temperature continuous vacuum drying equipment, finish the head tank temperature, Heating Zone Temperature, the cooling zone temperature, the coolant temperature of condenser, charging rate, conveyer belt speed, the setting of technological parameters such as cloth angle, when the head tank temperature, Heating Zone Temperature, after the cooling zone temperature reaches setting value, vacuum system (1) begins to start, when the vacuum of vacuum cavity (1-2) reaches 400pa, start charging cloth system (3) and material-transporting system (4), the extractum material is coated on the conveyer belt (4-1) equably, the extractum material along with conveyer belt successively through the three sections thermal treatment zone (2-1,2-2,2-3), form a kind of porous with one section cooling zone (2-4), loose pie material (5-1).When deviation phenomenon takes place in conveyer belt (4-1) in running, start automatic deviation correction mechanism (4-5), make conveyer belt (4-1) come back to the normal position.When dried material arrives the rear end of vacuum cavity (1-2), open discharge system (5), the pie material is peeled off from conveyer belt (4-1), be cut off to fall into after device (5-3) cuts off and twist in the cage destructor (5-4).Pneumatic dish valve this moment (5-6) is in opening, and pneumatic dish valve (5-7) is in closed condition.Dry thing after the pulverizing falls in the dry thing transfer jar (5-8) of drawing mechanism (5-5), when dry thing runs up to a certain degree, close pneumatic dish valve (5-6), open pneumatic dish valve (5-7), dry thing enters collecting tank (5-9), closes pneumatic dish valve (5-7) then, opens pneumatic dish valve (5-6), take off the collecting tank (5-9) that dried material is housed, change empty dry thing collecting tank.Whole dry run is carried out so continuously, up to end.After whole dry run finishes, start automatic cleaning system (6), the equipment of finishing cleans.
Embodiment 4:
This embodiment is on the basis of the foregoing description 1-3, and Radix Salviae Miltiorrhizae extractum (solvent is a water) is carried out the low temperature continuous vacuum drying, and its data are as follows:
Radix Salviae Miltiorrhizae extractum (solvent is a water)
Density: 1264kg/m 3Water content: 40%;
Head tank temperature: 45 ℃; The thermal treatment zone one temperature: 60 ℃;
The thermal treatment zone two temperature: 65 ℃; The thermal treatment zone three temperature: 60 ℃;
Cooling zone temperature: 20 ℃; The coolant temperature of condenser: 20 ℃;
Vacuum: 400pa; Charging rate: 6kg/h;
Conveyer belt speed: 6m/h; Cloth angle: 45 °;
Dry water content of matter: 2.91%; Production capacity: 3.0kg/h.
Embodiment 5:
This embodiment is on the basis of embodiment 1-3, under different technology conditions Radix Salviae Miltiorrhizae extractum (solvent is a water) is carried out the low temperature continuous vacuum drying, and its data are as follows:
Radix Salviae Miltiorrhizae extractum (solvent is a water)
Density: 1306Kg/m 3Water content: 35%;
Head tank temperature: 55 ℃; The thermal treatment zone one temperature: 55 ℃;
The thermal treatment zone two temperature: 60 ℃; The thermal treatment zone three temperature: 55 ℃;
Cooling zone temperature: 20 ℃; The coolant temperature of condenser: 20 ℃;
Vacuum: 400pa; Charging rate: 2kg/h;
Conveyer belt speed: 3m/h; Cloth angle: 45 °;
Dry water content of matter: 2.70%; Production capacity: 1.30kg/h.
Embodiment 6:
This embodiment is on the basis of embodiment 1-3, and Radix Notoginseng extractum (solvent is 40% ethanol) is carried out dry situation, and its data are as follows:
Radix Notoginseng extractum (solvent is 40% ethanol)
Density: 1298Kg/m 3Head tank temperature: 40 ℃;
The thermal treatment zone one temperature: 70 ℃; The thermal treatment zone two temperature: 60 ℃;
The thermal treatment zone three temperature: 50 ℃; Cooling zone temperature: 10 ℃;
The coolant temperature of condenser: 2 ℃; Charging rate: 10kg/h;
Vacuum: 400pa; Conveyer belt speed: 10m/h;
Cloth angle: 45 °; Dry water content of matter: 4.6%;
Production capacity: 5kg/h.
Embodiment 7:
This embodiment is on the basis of embodiment 1-3, under different technology conditions Radix Notoginseng extractum (solvent is 40% ethanol) is carried out dry situation, and its data are as follows:
Radix Notoginseng extractum (solvent is 40% ethanol)
Density: 1298kg/m 3Head tank temperature: 35 ℃;
The thermal treatment zone one temperature: 80 ℃; The thermal treatment zone two temperature: 70 ℃;
The thermal treatment zone three temperature: 60 ℃; Cooling zone temperature: 10 ℃;
The coolant temperature of condenser: 2 ℃; Charging rate: 2kg/h;
Vacuum: 400pa; Conveyer belt speed: 24m/h;
Cloth angle: 45 °; Dry water content of matter: 8.36%;
Production capacity: 4.2kg/h.

Claims (8)

1, the production method of the dry thing of a kind of Chinese medical concrete of porosity and looseness, be under vacuum condition, extractum material (3-1) to be coated on the conveyer belt (4-1) equably, carry out the low temperature continuous drying, it is characterized in that: extractum material (3-1) preheating in head tank (3-2), feeding temperature is controlled at 30~60 ℃, then by the charging rate of screw feed pump (3-3) by 1~10kg/h, be coated on equably on the conveyer belt (4-1) by distributing device (3-4), conveyer belt (4-1) is by the speed operation of 3~24m/h, under vacuum condition, the extractum material moves successively through each thermal treatment zone (2-1,2-2,2-3), thermal treatment zone hot aqueous medium's adjustable temperature range is 40~80 ℃, at last by cooling zone (2-4), the temperature range of cooling zone cooling water medium is 20~-1 ℃, wherein 5~-1 ℃ cooling water is provided by handpiece Water Chilling Units (2-5), form a kind of porous, the dry thing (5-1) of loose pie, when dry thing arrives equipment terminal, being peeled off device (5-2) by product scrapes off from conveyer belt, fall in the strand cage destructor (5-4) after shearing device (5-3) cuts off, the dry thing after the pulverizing is by having two pneumatic dish valve (5-6, drawing mechanism 5-7) (5-5) discharging.
2, the production method of the dry thing of the Chinese medical concrete of a kind of porosity and looseness according to claim 1, it is characterized in that: the density of Chinese medical concrete is 1100kg/m 3~1400kg/m 3
3, the production method of the dry thing of the Chinese medical concrete of a kind of porosity and looseness according to claim 1, it is characterized in that: the cooling medium of described condenser (1-3) can be tap water or industrial chilled water.
4, the full-automatic low temperature continuous vacuum drying equipment that the production method of the dry thing of the Chinese medical concrete of a kind of porosity and looseness according to claim 1 designs and produces, comprise vacuum system (1), heating, cooling system (2), charging cloth system (3), material-transporting system (4), discharge system (5), automatic cleaning system (6) and automatic control system (7), it is characterized in that: vacuum system (1) has Roots's water ring vacuum unit (1-1) and is connected condenser (1-3) on the vacuum cavity (1-2), vacuum cavity (1-2) has heat-insulation layer, is connected with vacuum buffer tank (1-4) and condensed fluid collecting tank (1-5) between vacuum unit (1-1) and condenser (1-3); Heating, cooling system (2) have three sections thermals treatment zone (2-1,2-2,2-3) and one section cooling zone (2-4); Charging cloth system (3) has the head tank (3-2) of band temperature control and agitator, and screw feed pump (3-3) is connected with distributing device (3-4) by feed pipe (3-6), and the pendulum angle of distributing device fork (3-5) is 10~50 °; Material-transporting system (4) has politef conveyer belt (4-1), the front end of conveyer belt, rear end are separately fixed on driven shaft (4-2), the driving shaft (4-3), driving shaft (4-3) is by the motor decelerating mechanism driven rotary, driven shaft (4-2) is fixed on the conveyer stretcher (4-4), and links to each other with automatic deviation correction mechanism (4-5); Discharge system (5) has the product that is in vacuum cavity (1-2) rear end and peels off device (5-2), shearing device (5-3), strand cage destructor (5-4), and the discharging opening of vacuum cavity is connected with the drawing mechanism (5-5) that has two Pneumatic butterfly valves (5-6,5-7); Automatic cleaning system (6) has booster pump (6-1) and two detergent lines (6-2), and every detergent line has the 12 cleaning shower nozzles (6-3) of 360 ° of rotations only; Automatic control system (7) has PLC electrical control cabinet (7-1) and touch screen operation interface (7-2).
5, full-automatic low temperature continuous vacuum drying equipment according to claim 4, it is characterized in that: the rear and front end of described vacuum cavity (1-2) has two pneumostop doors (1-11), and travel switch (1-12) is installed on the pneumostop door.
6, full-automatic low temperature continuous vacuum drying equipment according to claim 4 is characterized in that: have photoelectricity liquid-level switch (1-6), condensed fluid feed liquor valve (1-7), balanced valve (1-8), atmospheric valve (1-9), condensed fluid tapping valve (1-10) on the described condensed fluid collecting tank (1-5).
7, full-automatic low temperature continuous vacuum drying equipment according to claim 4, it is characterized in that: described automatic deviation correction mechanism (4-5) has photo-electric near switch (4-5-1) and cylinder (4-5-2), promotes the horizontal level that conveyer stretcher (4-4) is regulated conveyer belt (4-1) by cylinder (4-5-2).
8, full-automatic low temperature continuous vacuum drying equipment according to claim 4, it is characterized in that: described drawing mechanism (5-5) has the dry thing transfer jar (5-8) that is connected with the discharging opening of vacuum cavity (1-2), the dry thing collecting tank (5-9) that links to each other with dry thing transfer jar (5-8) and the pneumatic dish valve (5-6,5-7) between them, and wherein dry thing transfer jar (5-8) has cooling system.
CNB200610053216XA 2006-08-30 2006-08-30 Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete Expired - Fee Related CN100458337C (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CNB200610053216XA CN100458337C (en) 2006-08-30 2006-08-30 Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CNB200610053216XA CN100458337C (en) 2006-08-30 2006-08-30 Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete

Publications (2)

Publication Number Publication Date
CN1927229A true CN1927229A (en) 2007-03-14
CN100458337C CN100458337C (en) 2009-02-04

Family

ID=37857459

Family Applications (1)

Application Number Title Priority Date Filing Date
CNB200610053216XA Expired - Fee Related CN100458337C (en) 2006-08-30 2006-08-30 Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete

Country Status (1)

Country Link
CN (1) CN100458337C (en)

Cited By (12)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN101413751B (en) * 2008-11-27 2010-09-29 北京理工大学 Restaurant rubbish squeezing machine
CN102503743A (en) * 2008-11-26 2012-06-20 石家庄成功机电有限公司 Powdery ammonium nitrate explosive, preparation method for same and preparation equipment for same
CN102716589A (en) * 2011-03-30 2012-10-10 北京普照机电技术开发有限公司 Hanging slurry type drying equipment
CN103134273A (en) * 2011-11-23 2013-06-05 天津天士力现代中药资源有限公司 Drying method for blood nourishing and brain refreshing pill extractive
CN103822461A (en) * 2014-03-17 2014-05-28 无锡市海昌机械设备有限公司 Improved structure of material distributing system for vacuum belt liquid continuous dryer
CN104482726A (en) * 2014-12-30 2015-04-01 中山凯旋真空技术工程有限公司 Vacuum drying equipment and automatic condensate discharge device
CN105135830A (en) * 2015-09-22 2015-12-09 苏州维艾普新材料股份有限公司 Method for drying VIP core material through baking channel
CN106728824A (en) * 2016-12-15 2017-05-31 扬子江药业集团有限公司 A kind of drying process of the herbal mixture medicinal extract for the treatment of of insomnia patients
CN106802061A (en) * 2015-11-25 2017-06-06 衡阳屹顺化工有限公司 A kind of drying process of neopentyl glycol production
CN107449264A (en) * 2017-09-15 2017-12-08 四川宏图普新微波科技有限公司 A kind of polytetrafluoroethyldispersion dispersion resin particle wet feed drying system and method
CN108553927A (en) * 2018-04-27 2018-09-21 丁涛 Rapid draing medicinal extract is dried under reduced pressure case
CN113146729A (en) * 2021-04-13 2021-07-23 常州新舜干燥工程有限公司 Low-temperature film drying system

Family Cites Families (3)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN1073257A (en) * 1992-10-09 1993-06-16 姜国全 Vertical electric vacunm drying technology and equipment
CN2505787Y (en) * 2001-10-26 2002-08-14 徐洪池 Vacuum thick glue drier
CN2754629Y (en) * 2004-09-04 2006-02-01 常州市范群干燥设备有限公司 Host computer of cream material vacuum drier

Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN102503743A (en) * 2008-11-26 2012-06-20 石家庄成功机电有限公司 Powdery ammonium nitrate explosive, preparation method for same and preparation equipment for same
CN101413751B (en) * 2008-11-27 2010-09-29 北京理工大学 Restaurant rubbish squeezing machine
CN102716589A (en) * 2011-03-30 2012-10-10 北京普照机电技术开发有限公司 Hanging slurry type drying equipment
CN103134273A (en) * 2011-11-23 2013-06-05 天津天士力现代中药资源有限公司 Drying method for blood nourishing and brain refreshing pill extractive
CN103822461A (en) * 2014-03-17 2014-05-28 无锡市海昌机械设备有限公司 Improved structure of material distributing system for vacuum belt liquid continuous dryer
CN104482726A (en) * 2014-12-30 2015-04-01 中山凯旋真空技术工程有限公司 Vacuum drying equipment and automatic condensate discharge device
CN105135830A (en) * 2015-09-22 2015-12-09 苏州维艾普新材料股份有限公司 Method for drying VIP core material through baking channel
CN106802061A (en) * 2015-11-25 2017-06-06 衡阳屹顺化工有限公司 A kind of drying process of neopentyl glycol production
CN106728824A (en) * 2016-12-15 2017-05-31 扬子江药业集团有限公司 A kind of drying process of the herbal mixture medicinal extract for the treatment of of insomnia patients
CN106728824B (en) * 2016-12-15 2021-05-11 扬子江药业集团江苏龙凤堂中药有限公司 Drying process of compound traditional Chinese medicine extract for treating insomnia
CN107449264A (en) * 2017-09-15 2017-12-08 四川宏图普新微波科技有限公司 A kind of polytetrafluoroethyldispersion dispersion resin particle wet feed drying system and method
CN107449264B (en) * 2017-09-15 2023-05-26 四川宏图普新微波科技有限公司 Polytetrafluoroethylene dispersion resin particle wet material drying system and method
CN108553927A (en) * 2018-04-27 2018-09-21 丁涛 Rapid draing medicinal extract is dried under reduced pressure case
CN113146729A (en) * 2021-04-13 2021-07-23 常州新舜干燥工程有限公司 Low-temperature film drying system

Also Published As

Publication number Publication date
CN100458337C (en) 2009-02-04

Similar Documents

Publication Publication Date Title
CN1927229A (en) Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete
CN111849641A (en) Preparation process of plant essential oil
CN108517258A (en) A kind of continuous steam distillation extraction element of woody essential oil and its apparatus system
CN201485438U (en) Blumea balsamifera processing and extracting equipment
CN101429477B (en) Belt type continuous distillation method
CN103131616A (en) Device of producing wine by continuously distilling solid fermented grains
CN105771293B (en) Molasses alcohol waste liquid Reverse evaporation concentration systems
CN219614924U (en) Evaporation crystallization device
CN201183784Y (en) Wax decolorizing kettle
CN216864104U (en) Distillation device for turpentine
CN112923716B (en) Intelligent drying device for rumen-bypass product processing
CN203904309U (en) Tea seed cake evaporation and condensation equipment
CN109099683A (en) The drying means of vacuum belt drier and molasses mash
CN105016598B (en) Sludge heating and drying device
CN203904307U (en) Evaporation machine with top-end heating device
CN210646372U (en) Stirring device for reaction kettle
CN206910819U (en) A kind of evaporative desalination device
CN218025494U (en) Marigold fermentation wastewater comprehensive treatment device
CN1650835A (en) Integrated device for concentrating and drying chinese medicine oxtracted liquid
CN213885042U (en) Fractionation device based on medicine organic intermediate impurity
CN221093815U (en) Ammonium sulfate waste water evaporation crystallization equipment
CN216073690U (en) Bamboo vinegar extracting device
CN220939128U (en) Thin film evaporator
CN103710257B (en) Method and apparatus for continuous preparation of alcohol from solid phase raw material
CN104095253A (en) Fish meal drier

Legal Events

Date Code Title Description
C06 Publication
PB01 Publication
C10 Entry into substantive examination
SE01 Entry into force of request for substantive examination
C14 Grant of patent or utility model
GR01 Patent grant
EE01 Entry into force of recordation of patent licensing contract

Assignee: Sanjiu Medical & Pharmaceutical Co.,Ltd.

Assignor: Zhejiang University

Contract fulfillment period: 2009.4.15 to 2014.4.14

Contract record no.: 2009330001557

Denomination of invention: Method and device for producing poriferous and loose dry product of traditional Chinese medicine concrete

Granted publication date: 20090204

License type: Exclusive license

Record date: 20090706

LIC Patent licence contract for exploitation submitted for record

Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2009.4.15 TO 2014.4.14; CHANGE OF CONTRACT

Name of requester: SANJIU PHARMACEUTICAL CO., LTD.

Effective date: 20090706

EM01 Change of recordation of patent licensing contract

Change date: 20120425

Contract record no.: 2009330001557

Assignee after: CHINA RESOURCES SANJIU MEDICAL & PHARMACEUTICAL Co.,Ltd.

Assignee before: Sanjiu Medical & Pharmaceutical Co.,Ltd.

EC01 Cancellation of recordation of patent licensing contract

Assignee: CHINA RESOURCES SANJIU MEDICAL & PHARMACEUTICAL Co.,Ltd.

Assignor: Zhejiang University

Contract record no.: 2009330001557

Date of cancellation: 20140507

LICC Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model
CF01 Termination of patent right due to non-payment of annual fee
CF01 Termination of patent right due to non-payment of annual fee

Granted publication date: 20090204