CN1814022A - Chinese medicine preparation for tonifying yin and supplementing blood, and preparing method - Google Patents
Chinese medicine preparation for tonifying yin and supplementing blood, and preparing method Download PDFInfo
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- CN1814022A CN1814022A CN 200510032464 CN200510032464A CN1814022A CN 1814022 A CN1814022 A CN 1814022A CN 200510032464 CN200510032464 CN 200510032464 CN 200510032464 A CN200510032464 A CN 200510032464A CN 1814022 A CN1814022 A CN 1814022A
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Abstract
The present invention discloses a Chinese medicine preparation with the functions of nourishing yin and supplementing blood and its preparation method. It is an Ajiao Buxue pills preparation or dripping pills or enteric dripping pills or micropills or micropill capsule preparation made up by using 6 Chinese medicinal materials of ass hide glue, cooked rehmannia root, codonopsis root, astraglus root (mix-fried with honey), ovate atractylodes root and lyceum berry through a certain preparation process. Besides, said invention also provides the concrete steps of its preparation method.
Description
Technical field:
The present invention relates to a kind of Chinese medicine preparation and preparation method thereof, relate in particular to Chinese medicine preparation of a kind of nourishing YIN and supplementing blood and preparation method thereof.
Background technology:
Ball or drop pill or enteric coated drop pill or micropill or pellet capsule, change dosage form and manage as new drug research according to the relevant laws and regulations of China's drug control as a kind of pharmaceutical dosage form in the Chinese medicine preparation.The existing dosage form of this product is oral liquid, granule, soft extract, has all listed the national drug ministry standard in.Through patent retrieval, 2005 disclose Colla Corii Asini nourishing blood oral liquid and preparation method thereof (publication number: CN1579435), do not see the ball that Colla Corii Asini nourishing blood is arranged or the relevant patent of drop pill or enteric coated drop pill or micropill or pellet capsule.
The technology features of the Chinese medicine preparation Colla Corii Asini nourishing blood oral liquid of existing nourishing YIN and supplementing blood is except that Colla Corii Asini liquid, and the Radix Rehmanniae Preparata yellow fluid is carried, and extracting solution is standby; The Rhizoma Atractylodis Macrocephalae and Fructus Lycii carry out percolation with 25% ethanol as solvent with 60% ethanol, Radix Codonopsis and the Radix Astragali, merge the liquid of filtering, and leave standstill, filter, reclaim ethanol, concentrate, add Colla Corii Asini liquid, Radix Rehmanniae Preparata extracting solution, mixing adds antiseptic, glucide is an amount of, stir evenly, add water and adjust total amount, leave standstill, filter to 1000ml, embedding, promptly.
The particulate technology features of Chinese medicine preparation Colla Corii Asini nourishing blood of existing nourishing YIN and supplementing blood is except that Colla Corii Asini, and the Radix Rehmanniae Preparata yellow fluid is carried, and extracting solution is standby; The Rhizoma Atractylodis Macrocephalae and Fructus Lycii carry out diafiltration with 60% ethanol, Radix Codonopsis and the Radix Astragali with 25% ethanol, and merging filtrate leaves standstill, and filter, and add Colla Corii Asini and Radix Rehmanniae Preparata extracting solution, and mixing is concentrated into clear paste, and spray drying gets fine powder, and is an amount of with sucrose, makes granule, packing, promptly.
The technology features of the Chinese medicine preparation e-jiao hematinic ointment of existing nourishing YIN and supplementing blood is except that Colla Corii Asini, and the Radix Rehmanniae Preparata yellow fluid is carried, and extracting solution is standby; All the other Rhizoma Atractylodis Macrocephalaes and Fructus Lycii carry out percolation with 60% ethanol, Radix Codonopsis and the Radix Astragali with 25% ethanol, merge the liquid of filtering, and leave standstill, and filter; Add Colla Corii Asini, Radix Rehmanniae Preparata supernatant and simple syrup etc., mixing is evaporated to the relative density of regulation, filters, put cold, promptly.
Existing Colla Corii Asini nourishing blood oral liquid sugar content height, be not suitable for diabetics and take; The Colla Corii Asini nourishing blood granule uses inconvenient, need take after mixing it with hot water; The e-jiao hematinic ointment use is inconvenient, oral dose is wayward.Chinese medicine preparation Colla Corii Asini nourishing blood ball of the present invention or drop pill or enteric coated drop pill or micropill or pellet capsule can overcome the deficiency of above-mentioned dosage form, satisfy clinical demand.
Summary of the invention:
The objective of the invention is Chinese medicine preparation of a kind of nourishing YIN and supplementing blood and preparation method thereof, overcome the drawback of prior art, improve the quality of product, satisfy the needs of medical treatment better.
The objective of the invention is to be achieved through the following technical solutions.
A kind of Chinese medicine preparation of nourishing YIN and supplementing blood, it is that Main Ingredients and Appearance is Colla Corii Asini nourishing blood ball or drop pill or enteric coated drop pill or the micropill or the pellet capsule of Colla Corii Asini, Radix Rehmanniae Preparata, Radix Codonopsis, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii.
Its preparation method is:
(1) medicine Main Ingredients and Appearance and weight proportion thereof are as follows:
Respectively 100～200 parts of Colla Corii Asini, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii, each 200～400 parts of Radix Rehmanniae Preparata, Radix Codonopsis;
Medicine Main Ingredients and Appearance preferred weight proportioning is:
Respectively 120～180 parts of Colla Corii Asini, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii, each 250～350 parts of Radix Rehmanniae Preparata, Radix Codonopsis.
Medicine Main Ingredients and Appearance preferred weight proportioning is:
Respectively 150 parts of Colla Corii Asini, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii, each 300 parts of Radix Rehmanniae Preparata, Radix Codonopsis.
(2) get Colla Corii Asini and be ground into fine powder, standby;
(3) get Radix Rehmanniae Preparata and decoct with water 1～3 time, each 1～3 hour, collecting decoction filtered, and leaves standstill, and gets supernatant, and device is preserved in addition, and is standby;
(4) get the Rhizoma Atractylodis Macrocephalae, Fructus Lycii carries out percolation with 40～80% ethanol as solvent, get Radix Codonopsis, the Radix Astragali carries out percolation with 10-40% ethanol as solvent, merge the liquid of filtering, leave standstill, filter, add donkey-hide gelatin fine powder of (2) gained and the supernatant of (3) gained, mixing is concentrated into clear paste, drying, pulverize, it is standby to get fine drug powder;
(5) get the fine drug powder of (4) gained, add an amount of adjuvant, pill, coating or coating not promptly get ball;
Adjuvant is one or more combinations or other the suitable adjuvant in the following material, uses with by arbitrary proportion: maltose, Mel, lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid or sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, Polyethylene Glycol;
(6) with one or more of stearic acid or glyceryl monostearate or insect wax or Cera Flava or Polyethylene Glycol (PEG4000 or PEG6000) or sodium stearate or glycerin gelatine or polyoxyethylene monostearate (S-40) or Poloxamer188 or other suitable adjuvant, use with by arbitrary proportion, be heated to the fine drug powder that adds (4) gained after whole fusions, be transferred in the liquid containing bottle rapidly after stirring, airtight and the insulation at 70～100 ℃, under heat-retaining condition, go in the liquid coolant (liquid paraffin or methyl-silicone oil or vegetable oil or water or ethanol) by dropping-pill machine, condensation cured becomes ball, coolant is use up and removed to the drop pill drop of molding, dry, bag film-coat or sugar-coat or coating not promptly get drop pill;
(7) with one or more of stearic acid or glyceryl monostearate or insect wax or Cera Flava or Polyethylene Glycol (PEG4000 or PEG6000) or sodium stearate or glycerin gelatine or polyoxyethylene monostearate (S-40) or Poloxamer188 or other suitable adjuvant, use with by arbitrary proportion, be heated to the fine drug powder that adds (4) gained after whole fusions, be transferred in the liquid containing bottle rapidly after stirring, airtight and the insulation at 70～100 ℃, under heat-retaining condition, go in the liquid coolant (liquid paraffin or methyl-silicone oil or vegetable oil or water or ethanol) by dropping-pill machine, condensation cured becomes ball, coolant is use up and removed to the drop pill drop of molding, dry, enteric coated, promptly get enteric coated drop pill;
The coating material of its enteric coating is the suitable adjuvant of following one or more combinations or other, uses with by arbitrary proportion: acrylic resin II number or III number, cellulose acetate-phthalate (CAP), Lac, zein, the adjacent benzene diacetate (PVAP) of polyethylene, hydroxypropyl emthylcellulose acetic acid succinate (HPMCAS), ethyl cellulose;
(8) get the fine drug powder of (4) gained, concentrate, drying is pulverized, and adds an amount of adjuvant, mix homogeneously, and the micropill of diameter less than 2.5mm made in granulation, and coating or coating not promptly get micropill; Maybe the micropill that makes is incapsulated, promptly get pellet capsule;
Adjuvant is one or more combinations or other the suitable adjuvant in the following material, uses with by arbitrary proportion: ethyl cellulose (EC), the polypropylene polysiloxanes, the wax class, Polyethylene Glycol (PEG), stearic acid, Lac, acrylic resin, polyvinyl alcohol, polyvinylpyrrolidone (PVP), methylcellulose, hydroxypropyl cellulose, cellulose propionate, the acrylic resin aqueous dispersion, the pseudo-latex of ethyl cellulose, cellulose acetate-phthalate (CAP) latex, polyphenyl dioctyl phthalate vinyl acetate (PVAP) aqueous dispersion, propylene glycol, glycerol, triacetin, acetyl list monoglyceride, phthalic acid ester, polyoxyethylene sorbitan monoleate, sodium lauryl sulphate, lactose, fructose, sucrose.
Specific embodiments:
The present invention further specifies in conjunction with specific embodiments, can be for reference, do not limit the scope of the invention:
A kind of Chinese medicine preparation of nourishing YIN and supplementing blood, it is that Main Ingredients and Appearance is Colla Corii Asini nourishing blood ball or drop pill or enteric coated drop pill or the micropill or the pellet capsule of Colla Corii Asini, Radix Rehmanniae Preparata, Radix Codonopsis, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii.
Chinese medicine preparation energy nourishing YIN and supplementing blood of the present invention, invigorating the spleen and replenishing QI, spleen invigorating lung moistening.Be used for eipathia asthenia, anemia blurred vision, chronic consumptive disease cough.
The preparation method of Chinese medicine preparation Colla Corii Asini nourishing blood ball of the present invention or drop pill or enteric coated drop pill or micropill or pellet capsule is:
(1) medicine Main Ingredients and Appearance and weight consumption are as follows:
Colla Corii Asini, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), each 150g of Fructus Lycii, Radix Rehmanniae Preparata, each 300g of Radix Codonopsis;
(2) get Colla Corii Asini and be ground into fine powder, standby;
(3) get Radix Rehmanniae Preparata and decoct with water secondary, each 2 hours, collecting decoction filtered, and leaves standstill, and it is standby to get supernatant;
(4) get the Rhizoma Atractylodis Macrocephalae, Fructus Lycii carries out percolation with 60% ethanol as solvent, get Radix Codonopsis, the Radix Astragali carries out percolation with 25% ethanol as solvent, merges the liquid of filtering, leave standstill, filter, add donkey-hide gelatin fine powder of (2) gained and the supernatant of (3) gained, mixing, being concentrated into relative density is the clear paste of 1.04～1.06 (75 ℃), dry, pulverize, get fine drug powder, standby;
(5) a kind of Chinese medicine preparation ball of nourishing YIN and supplementing blood is the Colla Corii Asini nourishing blood ball, and its preparation method is: get the fine drug powder of (4) gained, add suitable water or processed with honey ball, promptly.
(6) a kind of Chinese medicine preparation drop pill of nourishing YIN and supplementing blood is the Colla Corii Asini nourishing blood drop pill, its preparation method is: taking polyethylene glycol PEG6000 120g, stearic acid 60g, Poloxamer188 50g, treat that Polyethylene Glycol PEG6000, stearic acid, Poloxamer188 are heated to the fine drug powder that adds above-mentioned (4) gained after whole fusions, be transferred in the liquid containing bottle rapidly after stirring, airtight and the insulation at 80 ℃, go in the liquid paraffin by dropping-pill machine at heat-retaining condition, be condensed into ball, with the drop pill drop of molding to the greatest extent and the erasing liquor paraffin body, promptly.
(7) a kind of Chinese medicine preparation enteric coated drop pill of nourishing YIN and supplementing blood is the Colla Corii Asini nourishing blood enteric coated drop pill, its preparation method is: taking polyethylene glycol PEG6000 120g, stearic acid 60g, Poloxamer188 50g, treat Polyethylene Glycol PEG6000, stearic acid, Poloxamer188 is heated to the fine drug powder that adds above-mentioned (4) gained after whole fusions, be transferred in the liquid containing bottle rapidly after stirring, airtight and the insulation at 80 ℃, go in the liquid paraffin by dropping-pill machine at heat-retaining condition, be condensed into ball, with the drop pill drop of molding to the greatest extent and the erasing liquor paraffin body, use acrylic resin, phthalic acid diethyl ester, the mixed liquor coating that the Semen Ricini wet goods is made, promptly.
(8) a kind of Chinese medicine preparation micropill of nourishing YIN and supplementing blood is the Colla Corii Asini nourishing blood micropill, its preparation method is: the fine drug powder of getting (4) gained, concentrate, drying is pulverized, with 260g dextrin mix homogeneously, 5%PVP alcohol liquid is binding agent, at first prepares 60 purpose granules and makes parent nucleus, and be binding agent with 5%PVP alcohol liquid again, add the mixed powder amplification and make 40 purpose micropills, promptly.
(9) a kind of Chinese medicine preparation pellet capsule of nourishing YIN and supplementing blood is the Colla Corii Asini nourishing blood pellet capsule, its preparation method is: get the fine drug powder of (4) gained, concentrate drying, pulverize, with 260g dextrin mix homogeneously, 5%PVP alcohol liquid is binding agent, at first prepares 60 purpose granules and makes parent nucleus, be binding agent with 5%PVP alcohol liquid again, add the mixed powder amplification and make 40 purpose micropills, incapsulate, promptly.
Advantage of the present invention is:
Take, easy to carry, be applicable to the difference crowd that takes medicine, can better meet the demand of clinical application.
Claims (4)
1, a kind of Chinese medicine preparation of nourishing YIN and supplementing blood is characterized in that it is that Main Ingredients and Appearance is Colla Corii Asini nourishing blood ball or drop pill or enteric coated drop pill or the micropill or the pellet capsule of Colla Corii Asini, Radix Rehmanniae Preparata, Radix Codonopsis, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii.
2, a kind of preparation method of Chinese medicine preparation of nourishing YIN and supplementing blood, it is the preparation method of Colla Corii Asini nourishing blood ball or drop pill or enteric coated drop pill or micropill or pellet capsule, it is characterized in that:
(1) medicine Main Ingredients and Appearance and weight proportion thereof are as follows:
Respectively 100～200 parts of Colla Corii Asini, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii, each 200～400 parts of Radix Rehmanniae Preparata, Radix Codonopsis;
(2) get Colla Corii Asini and be ground into fine powder, standby;
(3) get Radix Rehmanniae Preparata and decoct with water 1～3 time, each 1～3 hour, collecting decoction filtered, and leaves standstill, and gets supernatant, and device is preserved in addition, and is standby;
(4) get the Rhizoma Atractylodis Macrocephalae, Fructus Lycii carries out percolation with 40～80% ethanol as solvent, get Radix Codonopsis, the Radix Astragali carries out percolation with 10-40% ethanol as solvent, merge the liquid of filtering, leave standstill, filter, add donkey-hide gelatin fine powder of (2) gained and the supernatant of (3) gained, mixing is concentrated into clear paste, drying, pulverize, it is standby to get fine drug powder;
(5) get the fine drug powder of (4) gained, add suitable adjuvant, make ball or drop pill or enteric coated drop pill or micropill or pellet capsule;
The preparation method of its ball is: gets the fine drug powder of (4) gained, adds an amount of adjuvant, and pill, coating or coating not, promptly;
Adjuvant is one or more combinations or other the suitable adjuvant in the following material, uses with by arbitrary proportion: maltose, Mel, lactose, starch, carboxymethyl starch sodium, pregelatinized Starch, sucrose, glucose, mannitol, sorbitol, syrup, microcrystalline Cellulose, methylcellulose, carboxymethyl cellulose, ethyl cellulose, hydroxypropyl emthylcellulose, low-substituted hydroxypropyl cellulose, carboxymethylcellulose calcium, calcium sulfate, calcium hydrogen phosphate, calcium phosphate, calcium carbonate, light magnesium oxide, Pulvis Talci, micropowder silica gel, aluminium hydroxide, boric acid or sodium chloride, dextrin, magnesium stearate, hydrogenated vegetable oil, Polyethylene Glycol;
The preparation method of its drop pill is: with one or more of stearic acid or glyceryl monostearate or insect wax or Cera Flava or Polyethylene Glycol (PEG4000 or PEG6000) or sodium stearate or glycerin gelatine or polyoxyethylene monostearate (S-40) or Poloxamer188 or other suitable adjuvant, use with by arbitrary proportion, be heated to the fine drug powder that adds (4) gained after whole fusions, be transferred in the liquid containing bottle rapidly after stirring, airtight and the insulation at 70～100 ℃, under heat-retaining condition, go in the liquid coolant (liquid paraffin or methyl-silicone oil or vegetable oil or water or ethanol) by dropping-pill machine, condensation cured becomes ball, coolant is use up and removed to the drop pill drop of molding, dry, bag film-coat or sugar-coat or coating not, promptly;
The preparation method of its enteric coated drop pill is: with one or more of stearic acid or glyceryl monostearate or insect wax or Cera Flava or Polyethylene Glycol (PEG4000 or PEG6000) or sodium stearate or glycerin gelatine or polyoxyethylene monostearate (S-40) or Poloxamer188 or other suitable adjuvant, use with by arbitrary proportion, be heated to the fine drug powder that adds (4) gained after whole fusions, be transferred in the liquid containing bottle rapidly after stirring, airtight and the insulation at 70～100 ℃, under heat-retaining condition, go in the liquid coolant (liquid paraffin or methyl-silicone oil or vegetable oil or water or ethanol) by dropping-pill machine, condensation cured becomes ball, coolant is use up and removed to the drop pill drop of molding, dry, enteric coated, promptly;
The coating material of its enteric coating is the suitable adjuvant of following one or more combinations or other, uses with by arbitrary proportion: acrylic resin II number or III number, cellulose acetate-phthalate (CAP), Lac, zein, the adjacent benzene diacetate (PVAP) of polyethylene, hydroxypropyl emthylcellulose acetic acid succinate (HPMCAS), ethyl cellulose;
The preparation method of its micropill or pellet capsule is: get the fine drug powder of (4) gained, concentrate, drying is pulverized, and adds an amount of adjuvant, mix homogeneously, and the micropill of diameter less than 2.5mm made in granulation, and coating or coating not promptly get micropill; Maybe the micropill that makes is incapsulated, promptly get pellet capsule;
Adjuvant is one or more combinations or other the suitable adjuvant in the following material, uses with by arbitrary proportion: ethyl cellulose (EC), the polypropylene polysiloxanes, the wax class, Polyethylene Glycol (PEG), stearic acid, Lac, acrylic resin, polyvinyl alcohol, polyvinylpyrrolidone (PVP), methylcellulose, hydroxypropyl cellulose, cellulose propionate, the acrylic resin aqueous dispersion, the pseudo-latex of ethyl cellulose, cellulose acetate-phthalate (CAP) latex, polyphenyl dioctyl phthalate vinyl acetate (PVAP) aqueous dispersion, propylene glycol, glycerol, triacetin, acetyl list monoglyceride, phthalic acid ester, polyoxyethylene sorbitan monoleate, sodium lauryl sulphate, lactose, fructose, sucrose.
3, the preparation method of the Chinese medicine preparation of a kind of nourishing YIN and supplementing blood according to claim 2 is characterized in that the preferred weight proportioning of its Main Ingredients and Appearance is:
Respectively 120～180 parts of Colla Corii Asini, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii, each 250～350 parts of Radix Rehmanniae Preparata, Radix Codonopsis.
4, the preparation method of the Chinese medicine preparation of a kind of nourishing YIN and supplementing blood according to claim 2 is characterized in that the optimum weight proportioning of its Main Ingredients and Appearance is:
Respectively 150 parts of Colla Corii Asini, the Radix Astragali (processed with honey), the Rhizoma Atractylodis Macrocephalae (parched with bran), Fructus Lycii, each 300 parts of Radix Rehmanniae Preparata, Radix Codonopsis.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
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| CN 200510032464 CN1814022A (en) | 2005-11-30 | 2005-11-30 | Chinese medicine preparation for tonifying yin and supplementing blood, and preparing method |
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| Application Number | Priority Date | Filing Date | Title |
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| CN 200510032464 CN1814022A (en) | 2005-11-30 | 2005-11-30 | Chinese medicine preparation for tonifying yin and supplementing blood, and preparing method |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102090462A (en) * | 2010-12-31 | 2011-06-15 | 万勤劳 | Preparation technology for soft beancurd containing Chinese medicinal herbs |
| CN101293053B (en) * | 2008-05-19 | 2012-01-11 | 河南省新四方制药有限公司 | Detection method for E-jiao hematinic ointment |
-
2005
- 2005-11-30 CN CN 200510032464 patent/CN1814022A/en active Pending
Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101293053B (en) * | 2008-05-19 | 2012-01-11 | 河南省新四方制药有限公司 | Detection method for E-jiao hematinic ointment |
| CN102090462A (en) * | 2010-12-31 | 2011-06-15 | 万勤劳 | Preparation technology for soft beancurd containing Chinese medicinal herbs |
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