CN1793442A - Mfg. of fiber for textile by environment protection biological-chemical method - Google Patents
Mfg. of fiber for textile by environment protection biological-chemical method Download PDFInfo
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- CN1793442A CN1793442A CN 200510111703 CN200510111703A CN1793442A CN 1793442 A CN1793442 A CN 1793442A CN 200510111703 CN200510111703 CN 200510111703 CN 200510111703 A CN200510111703 A CN 200510111703A CN 1793442 A CN1793442 A CN 1793442A
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Abstract
The invention relates to a weaving using natural fiber manufacturing method processed by environmental protection type biological-chemical method together. It includes the following steps: boiling; press hammer to form filament; using washing to remove pectin, hemi-cellulose, and lignin; then using mould to remove them and part of cellulose; and microwave processing to gain the need fiber. The fibril plants are bast plants such as bamboo, hemp, mulberry, banana, or dragon-beard grass.
Description
Technical field
The invention belongs to a kind of the weaving, be meant that especially utilizing bamboo to pass through environment protection biological-chemical method produces the technology of weaving with bamboo fiber with the manufacture craft of natural fabric.
Background technology:
Weaving at present has two kinds with bamboo fibre:
A kind of is the cellulose that extracts in bamboo, carry out chemical modification then the cellulose derivative behind the chemical modification, be dissolved in the solvent, carry out wet spinning, obtain fiber, in fact this be that the same thing is that raw material sources are different with existing viscose, general viscose uses wood pulp cellulose to produce, they have been natural fibers no longer all, and great changes have all taken place for the physical arrangement of fiber and original cellulose fibre, are a kind of chemical fibres.The cellulose fibre of making raw material of the bamboo cellulose is bamboo pulp fiber again.Also can not carry out chemical modification with up-to-date technology, directly cellulose dissolution in special solvent, carry out wet spinning again, obtain fiber, but the structure of this fiber is also also different with natural bamboo fibre structure, also belongs to chemical fibre.As patent of invention 03150422.1 (producing the technology of viscose filament yarn with bamboo pulp), 03150659.3 (a kind of viscose filament yarn and goods thereof), 200410066226.8 (Visose rayon with textile function and preparation methods), 02111954.6 (method for making bamboo fibre) is exactly the manufacturing that belongs to this class bamboo pulp fiber.
Another kind is the cellulose fibre that directly extracts in the bamboo, is a kind of natural, primary fiber, keeps the structure and the physicochemical property of original bamboo fiber.Bamboo fibre has the same structure of flax fibre and performance, fiber gloss is beautiful, good antibacterial property and ABRASION RESISTANCE are arranged, inside with good coloring, bounce-back property, drapability, particularly its fiber is covered with big and small space, can absorb moisture fast and the moisture that volatilizees, dress has good gas permeability and comfort.This bamboo fibre is bamboo fiber again.
The invention of producing of natural bamboo fibres is a lot of, but considerable patent is arranged wherein and weaving is irrelevant, produce composite or construction material with thick bamboo fibre.As 02154784.X (processing method of bamboo fibre), 93108031.2 (production methods of bamboo fibre), 01108748.X (technology of extracting bamboo fibre by physical method), 01108747.1 (bamboo fibre process), 01107139.7 (bamboo fibre and manufacture method thereof) etc.
Weaving has 8 with the Chinese invention patent application of bamboo fiber, and application number is 02111380.7 (bamboo fibre and manufacture method thereof), (02151265.5 bamboo wood becomes fine preparation method), (02133494.3 the preparation method of natural bamboo fibres), (01123617.5 the preparation method of bamboo fiber), (200410060809.X bamboo fibre process), (200410046835.7 a kind of preparation method that former bamboo is processed into the spinnability bamboo fibre), (200310108826.1 a kind of preparation method of bamboo fiber), (200410046802.2 a kind of preparation method that former bamboo is processed into the spinnability bamboo fibre).
Wherein number of patent application be 02151265.5,02133494.3 and the weaving of 200410060809.X with will or using bronsted lowry acids and bases bronsted lowry simultaneously and come bamboo is handled with acid or alkali in the method for making bamboo fibre.Can produce a large amount of reluctant sewage.
Number of patent application is that 01123617.5 protection domain is treatment process program and roll unit; 02111380.7 the patent protection content also only be a treatment process program, wherein mention with softening agent is softening and handling, all do not relate to as for the composition and the softening process condition of softening agent.
Application number is that 200310108826.1 the used bating liquor of processing method will be used chemicalss such as alkali, sodium metasilicate, sodium phosphate trimer, sodium thiosulfate, vulcanized sodium, also will react under pressure simultaneously.Also to use mineral acid treatment such as sulfuric acid, phosphoric acid, hydrochloric acid at last.These waste water also are difficult to handle.
Application number be 200410046802.2 and 200410046835.7 these two apply for a patent do not know why not only content class with and also summary also be the same.His bamboo fiber preparation method is carried out a biological disposal upon to bamboo with the straw mould, handles but need that bamboo is put into the pressure vessel superheated steam early stage.Bamboo soaked 2 hours in straw mould solution, was heated to 80 ℃ more together.This method has two doubtful points, and whether whether mould have so fast reaction speed, mould to also have active at 80 ℃.General mould is high activity 20-40 ℃ of temperature, comprises the straw mould.These can be referring to the microbiology teaching materials.
So what expect to have a kind of environment-friendly type produces weaving with the method for bamboo fiber, to satisfy the living standards of the people needs of optimal growth day by day.
Summary of the invention:
The present invention is that a kind of common processing of biology one chemical method that relates to environment-friendly type produced textile fiber.
The method that the present invention adopts is
At first adopt physical method that natural plants is carried out preliminary treatment,, come digest and decompose lignin, hemicellulose, pectin and part cellulose, so that cellulose fibre separates and attenuates with microorganism again pretreated natural plants silk.Waste water after these two parts are handled contains the organic fertilizer that a large amount of pectin, polysaccharide and mineral matter can be used as plant.
Further the silk after carrying out a biological disposal upon is carried out chemical treatment with microwave again near neutral chemicals again, the lignin of plant, hemicellulose, pectin and cellulose all are polar molecules, the reaction of acceleration of molecule high speed vibration and medicine under microwave action.Processingization is few with chemicals like this, and the time is short.And with the waste water that these medicines reaction back is cleaned after concentrating, can directly burn non-environmental-pollution also recyclable part chemicals recycle.Substantially reach the green production method of non-environmental-pollution.
The present invention is particularly useful for producing the fiber of natural weaving with bamboo, fiber crops, paper mulberry bark, bajiao banana or Chinese alpine rush class bast plant with bamboo, fiber crops, paper mulberry bark, bajiao banana or Chinese alpine rush class bast plant.
Main technique of the present invention can be expressed as follows:
1, at first adopt physical method that natural plants is carried out preliminary treatment, natural plants is blocked or cuts open in flakes, or remove skin, as surf green, surf green can use it for anything else.Put into water then and boil deliquescing, take out crushing, filament hammer out.Put into boiling water again and boiled 0.5-4 hour, to remove part pectin, hemicellulose, lignin.
2, above-mentioned pretreated natural plants silk, immerse fermentation process in the solution that contains mould, allow the plurality of enzymes of mould secretion decompose lignin, hemicellulose, pectin and part cellulose, so that cellulose fibre separates and attenuates.Used mould is white rot mould or bacillus, fermentation time 7-30 days, and temperature 10-40 ℃.Wherein, silk is (1: 5)-(1: 15) with the microbial solution ratio.
3, again fermentation after the silk that cleans, immerse in the mixed solution of sodium sulfite, ammonium oxalate and surfactant, the concentration of mixed liquor is taken out the back drop and is gone redundant solution, and maceration extract can use after replenishing medicine repeatedly, the bamboo silk that contains medicine is through microwave treatment, again through cleaning.
Last method routinely bleach, oils, soft, shredding promptly obtains can be for the natural fabric of the usefulness of weaving.
The dried bacterial content of living in the described microbial solution is 0.5%-3%.
It is characterized in that the microwave frequency that microwave chemical is handled is 915MHZ or 2450MHZ.
The mixing processing solution that adopts among the present invention is a 1. 2. 3. commodity nonionic surface active agent of ammonium oxalate or ammonium citrate of sodium sulfite or sodium hydrogensulfite, the aqueous solution that three parts are formed.The concentration expressed in percentage by weight of contained chemicals is 0.5%-2% in the aqueous solution; Chemicals 1.+2. and ratio 3. be (8: 1)-(2: 1); 1. and ratio 2. be (2: 1)-(1: 2).
The microwave frequency of described microwave treatment is 500～3000MH, and the time of processing is 1-20 minute.The microwave frequency of recommending microwave chemical to handle is 915MHZ or 2450MHZ.
The present invention is the common method of weaving with natural fabric produced of handling of a kind of biological-chemical method of environment-friendly type, and pre-treatment needn't high-tension apparatus, only needs atmospheric cooking to get final product; The waste water of biological treatment can be made fertilizer and use, and chemically treated medicine is neutral, and can reclaim repeated use, uses microwave treatment time short, effective in chemically treated process.
The specific embodiment:
To help to understand the present invention by following examples, but not limit content of the present invention.
Used chemicals is commercial commodity among the embodiment.
Embodiment 1
Bamboo chip is blocked and cutd open into to mao bamboon, after putting into water and boiling deliquescing, take out crushing, filament hammer out.Put into boiling water again and boiled 4 hours, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated bamboo silk portion, immerse 30 ℃ contained in 5 parts of the 1% white rot mould solution fermentation process 15 days, take out and clean.Immerse again every liter contain 14.5 the gram sodium sulfites, 5.5 the gram ammonium oxalate, 2.5 the gram JFC the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 2450MHZ, handled 1 minute, take out clean, bleach, oil, soft, shredding, obtain average fineness and be 1000 public bamboo natural fabrics.
Embodiment 2
Go mao bamboon rascal to block and cut open into bamboo chip, after putting into water and boiling deliquescing, take out crushing, filament hammer out.Put into boiling water again and boiled 0.5 hour, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated bamboo silk portion, immersed in 10 ℃ 15 parts of the solution that contains 3% white rot mould fermentation process 30 days, take out and clean.Immerse again every liter contain 1.6 the gram sodium hydrogensulfites, 3.2 the gram ammonium citrates, 0.7 the gram MOA-10 the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 2450MHZ, handled 5 minutes, taking-up is cleaned, bleaches, is oiled, soft, shredding, obtains average fineness and be 1240 public bamboo natural fabrics.
Embodiment 3
Small pieces are blocked and cutd open into to green bamboo, after putting into water and boiling deliquescing, take out crushing, filament hammer out.Put into boiling water again and boiled 2 hours, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated bamboo silk portion, immersed in 40 ℃ 10 parts of the solution that contains 2% bacillus fermentation process 7 days, take out and clean.Immerse again every liter contain 2.4 the gram sodium hydrogensulfites, 4.8 the gram ammonium oxalate, 3.6 the gram OP-15 the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 915MHZ, handled 10 minutes, taking-up is cleaned, bleaches, is oiled, soft, shredding, obtains average fineness and be 2350 public bamboo natural fabrics.
Embodiment 4
Henon bamboo blocked and cut open in flakes, after putting into water and boiling deliquescing, take out crushing, filament hammer out.Put into boiling water again and boiled 3 hours, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated bamboo silk portion, immerse 26 ℃ contained in 12 parts of the 12 bacillus solution fermentation process 20 days, take out and clean.Immerse again every liter contain 4.8 the gram sodium sulfites, 2.4 the gram ammonium oxalate, 1.2 the gram AEO-9 the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 2450MHZ, handled 12 minutes, taking-up is cleaned, bleaches, is oiled, soft, shredding, obtains average fineness and be 2600 public bamboo natural fabrics.
Embodiment 5
Go sinocalamus latiflorus rascal to block and cut open into small pieces, after putting into water and boiling deliquescing, take out crushing, filament hammer out.Put into boiling water again and boiled 4 hours, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated bamboo silk portion, immerse 25 ℃ contained in 7 parts of the 1.2% bacillus solution fermentation process 30 days, take out and clean.Immerse again every liter contain 12.6 the gram sodium hydrogensulfites, 6.3 the gram ammonium oxalate, 2.1 the gram OP-10 the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 915MHZ, handled 16 minutes, taking-up is cleaned, bleaches, is oiled, soft, shredding, obtains average fineness and be 2850 public bamboo natural fabrics.
Embodiment 6
Go sinocalamus latiflorus rascal to block and cut open into small pieces, after putting into water and boiling deliquescing, take out crushing, filament hammer out.Put into boiling water again and boiled 4 hours, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated bamboo silk portion, immerse 25 ℃ contained in 14 parts of the 1.8% bacillus solution fermentation process 30 days, take out and clean.Immerse again every liter contain 6.3 the gram sodium hydrogensulfites, 12.6 the gram ammonium oxalate, 4 the gram AEO-9 the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 2450MHZ, handled 20 minutes, taking-up is cleaned, bleaches, is oiled, soft, shredding, obtains average fineness and be 3000 public bamboo natural fabrics.
Embodiment 7
Paper mulberry bark is put into boiling water boiled 3 hours, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated paper mulberry bark portion, immerse 35 ℃ contained in 12 parts of the 1.4% white rot mould solution fermentation process 30 days, take out and clean.Immerse again every liter contain 5.1 the gram sodium hydrogensulfites, 4.6 the gram ammonium oxalate, 0.8 the gram MOA-12 the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 2450MHZ, handled 12 minutes, taking-up is cleaned, bleaches, is oiled, soft, shredding, obtains average fineness and be 2510 public mulberry skin natural fabrics.
Embodiment 8
Dried Chinese alpine rush is put into boiling water boiled 3.5 hours, to remove part pectin, hemicellulose, lignin.Above-mentioned pretreated Chinese alpine rush portion, immerse 30 ℃ contained in 10 parts of the 0.9% white rot mould solution fermentation process 30 days, take out and clean.Immerse again every liter contain 8.5 the gram sodium hydrogensulfites, 3.2 the gram ammonium oxalate, 1.4 the gram MOA-10 the aqueous solution in, soak into take out drop and go redundant solution after, in the microwave of 2450MHZ, handled 15 minutes, taking-up is cleaned, bleaches, is oiled, soft, shredding, obtains average fineness and be 2400 public Chinese alpine rush natural fabrics.
Claims (9)
1, the preparation method of a kind of environment protection biological-chemical method textile fiber is characterized in that adopting following method to make:
A, at first natural fabric plant peeling is boiled deliquescing in water, take out crushing, filament hammer out, put into the boiling water boiling-off again 0.5-4 hour;
B, above-mentioned pretreated silk, immersed in the solution that contains mould temperature 10-40 ℃ fermentation process 7-30 days; Used mould is white rot mould or bacillus;
C, again fermentation after the silk that cleans, immerse and soak into the back in the treatment fluid and take out drop and go redundant solution, through microwave treatment, again through cleaning; Described treatment fluid is 1. sodium sulfite or sodium hydrogensulfite, 2. ammonium oxalate or ammonium citrate and the 3. aqueous solution of the 0.5%-2% of the concentration expressed in percentage by weight formed of commodity nonionic surface active agent, and wherein 1.+2. compound is 8 with 3. weight ratio: 1-2: 1; 1. be 2 with 2. weight ratio: 1-1: 2;
Again method routinely bleach, oil, soft, shredding promptly obtains can be for the natural fabric of weaving usefulness.
2, the preparation method of a kind of environment protection biological according to claim 1-chemical method textile fiber is characterized in that described boiling-off temperature is 80-100 ℃.
3, the preparation method of a kind of environment protection biological according to claim 1-chemical method textile fiber is characterized in that the described silk and the ratio of microbial solution are (1: 5)-(1: 15).
4, the preparation method of a kind of environment protection biological according to claim 1-chemical method textile fiber, the dried bacterial content that it is characterized in that living in the described microbial solution is 0.5%-3%.
5, the preparation method of one one kinds of environment protection biologicals according to claim 1-chemical method textile fiber is characterized in that the microwave frequency that described microwave chemical is handled is 500～3000MH.
6, the preparation method of a kind of environment protection biological according to claim 5-chemical method textile fiber is characterized in that the microwave frequency that described microwave chemical is handled is 915MHZ or 2450MHZ.
7, the preparation method of a kind of environment protection biological according to claim 1-chemical method textile fiber is characterized in that the time that microwave chemical is handled is 1-20 minute.
8, the preparation method of a kind of environment protection biological according to claim 1-chemical method textile fiber is characterized in that described natural fabric plant is bamboo, fiber crops, mulberry tree, bajiao banana or Chinese alpine rush class bast plant.
9, the preparation method of a kind of environment protection biological according to claim 1-chemical method textile fiber is characterized in that described natural fabric is the natural textile fiber of bamboo, fiber crops, mulberry tree, bajiao banana or Chinese alpine rush class bast plant.
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| CNB2005101117032A CN100334266C (en) | 2005-12-20 | 2005-12-20 | Mfg. of fiber for textile by environment protection biological-chemical method |
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Cited By (12)
| Publication number | Priority date | Publication date | Assignee | Title |
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| CN101285212B (en) * | 2008-05-27 | 2011-07-20 | 广西大学 | Degumming process for mulberry fibre by bacilli compound bacteria |
| CN102776577A (en) * | 2012-06-19 | 2012-11-14 | 华中科技大学 | Preprocessing methods for degummed ramie production |
| CN104178877A (en) * | 2014-07-29 | 2014-12-03 | 宁波华乐特汽车装饰布有限公司 | Processing method for automotive bamboo fiber interior fabric |
| CN105200532A (en) * | 2015-11-09 | 2015-12-30 | 长兴业美纺织有限公司 | Eulaliopsis binata fiber used for weaving with high elongation |
| CN105212813A (en) * | 2015-11-09 | 2016-01-06 | 长兴业美纺织有限公司 | A kind of novel environment friendly towel fabric |
| CN105220242A (en) * | 2015-11-09 | 2016-01-06 | 长兴业美纺织有限公司 | Chinese alpine rush fiber is used in weaving of a kind of softness |
| CN105231502A (en) * | 2015-11-09 | 2016-01-13 | 长兴业美纺织有限公司 | Novel anti-microbial fabric for underwear |
| CN105401224A (en) * | 2015-10-31 | 2016-03-16 | 湖州新南海织造厂 | Environment-friendly and degradable excellent modified bamboo fiber |
| CN105442059A (en) * | 2015-11-09 | 2016-03-30 | 长兴业美纺织有限公司 | Chinese alpine rush fibers having good antibacterial performance and used for weaving |
| CN106283793A (en) * | 2016-09-21 | 2017-01-04 | 东莞市联洲知识产权运营管理有限公司 | Bamboo fiber that a kind of nano-cellulose is whisker modified and preparation method thereof |
| CN108823645A (en) * | 2018-08-21 | 2018-11-16 | 随月丽 | A kind of preparation method of high-strength bamboo fiber |
| CN111778608A (en) * | 2019-04-03 | 2020-10-16 | 上海水星家用纺织品股份有限公司 | Preparation method of paper mulberry fiber fabric |
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| DE19617909A1 (en) * | 1996-05-03 | 1997-11-13 | Arnold Moebius | Opening natural fibres into single fibres |
| US6464338B1 (en) * | 1996-07-31 | 2002-10-15 | Canon Kabushiki Kaisha | Ink jet head with separable tank holding member and recording unit |
| RU2181797C2 (en) * | 2000-06-19 | 2002-04-27 | Костромская государственная сельскохозяйственная академия | Method to obtain dew-retting treated plant fibers of fiber flax under controlled conditions |
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| KR100317476B1 (en) * | 2001-05-17 | 2001-12-22 | 박선규 | A method of removing pectin in bast fiber |
| CN1624212A (en) * | 2004-09-22 | 2005-06-08 | 刘忆萍 | Method of processing raw bamboo into spinnable bamboo fiber |
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| CN101285212B (en) * | 2008-05-27 | 2011-07-20 | 广西大学 | Degumming process for mulberry fibre by bacilli compound bacteria |
| CN102776577A (en) * | 2012-06-19 | 2012-11-14 | 华中科技大学 | Preprocessing methods for degummed ramie production |
| CN104178877A (en) * | 2014-07-29 | 2014-12-03 | 宁波华乐特汽车装饰布有限公司 | Processing method for automotive bamboo fiber interior fabric |
| CN105401224A (en) * | 2015-10-31 | 2016-03-16 | 湖州新南海织造厂 | Environment-friendly and degradable excellent modified bamboo fiber |
| CN105231502A (en) * | 2015-11-09 | 2016-01-13 | 长兴业美纺织有限公司 | Novel anti-microbial fabric for underwear |
| CN105220242A (en) * | 2015-11-09 | 2016-01-06 | 长兴业美纺织有限公司 | Chinese alpine rush fiber is used in weaving of a kind of softness |
| CN105212813A (en) * | 2015-11-09 | 2016-01-06 | 长兴业美纺织有限公司 | A kind of novel environment friendly towel fabric |
| CN105200532A (en) * | 2015-11-09 | 2015-12-30 | 长兴业美纺织有限公司 | Eulaliopsis binata fiber used for weaving with high elongation |
| CN105442059A (en) * | 2015-11-09 | 2016-03-30 | 长兴业美纺织有限公司 | Chinese alpine rush fibers having good antibacterial performance and used for weaving |
| CN105212813B (en) * | 2015-11-09 | 2018-03-16 | 长兴业美纺织有限公司 | A kind of novel environment friendly towel fabric |
| CN105442059B (en) * | 2015-11-09 | 2018-06-15 | 广东亨瑞织造科技有限公司 | A kind of anti-microbial property good weaving dragon grass fiber |
| CN106283793A (en) * | 2016-09-21 | 2017-01-04 | 东莞市联洲知识产权运营管理有限公司 | Bamboo fiber that a kind of nano-cellulose is whisker modified and preparation method thereof |
| CN106283793B (en) * | 2016-09-21 | 2018-05-11 | 东莞市联洲知识产权运营管理有限公司 | Whisker modified bamboo fiber of a kind of nano-cellulose and preparation method thereof |
| CN108823645A (en) * | 2018-08-21 | 2018-11-16 | 随月丽 | A kind of preparation method of high-strength bamboo fiber |
| CN111778608A (en) * | 2019-04-03 | 2020-10-16 | 上海水星家用纺织品股份有限公司 | Preparation method of paper mulberry fiber fabric |
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