CN1775661A - Method for preparing vanadium nitride - Google Patents
Method for preparing vanadium nitride Download PDFInfo
- Publication number
- CN1775661A CN1775661A CN 200510022245 CN200510022245A CN1775661A CN 1775661 A CN1775661 A CN 1775661A CN 200510022245 CN200510022245 CN 200510022245 CN 200510022245 A CN200510022245 A CN 200510022245A CN 1775661 A CN1775661 A CN 1775661A
- Authority
- CN
- China
- Prior art keywords
- vanadium
- preparation
- raw materials
- vanadium nitride
- nitride
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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- SKKMWRVAJNPLFY-UHFFFAOYSA-N azanylidynevanadium Chemical compound [V]#N SKKMWRVAJNPLFY-UHFFFAOYSA-N 0.000 title claims abstract description 46
- 238000000034 method Methods 0.000 title claims abstract description 18
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 claims abstract description 26
- GNTDGMZSJNCJKK-UHFFFAOYSA-N divanadium pentaoxide Chemical compound O=[V](=O)O[V](=O)=O GNTDGMZSJNCJKK-UHFFFAOYSA-N 0.000 claims abstract description 26
- OKTJSMMVPCPJKN-UHFFFAOYSA-N Carbon Chemical compound [C] OKTJSMMVPCPJKN-UHFFFAOYSA-N 0.000 claims abstract description 24
- 229910052799 carbon Inorganic materials 0.000 claims abstract description 20
- 229910052757 nitrogen Inorganic materials 0.000 claims abstract description 16
- 238000006243 chemical reaction Methods 0.000 claims abstract description 11
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims abstract description 10
- 239000000203 mixture Substances 0.000 claims abstract description 9
- 229910052760 oxygen Inorganic materials 0.000 claims abstract description 8
- QGZKDVFQNNGYKY-UHFFFAOYSA-O Ammonium Chemical compound [NH4+] QGZKDVFQNNGYKY-UHFFFAOYSA-O 0.000 claims abstract description 6
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 claims abstract description 6
- 239000001301 oxygen Substances 0.000 claims abstract description 6
- 229910052720 vanadium Inorganic materials 0.000 claims description 36
- QGZKDVFQNNGYKY-UHFFFAOYSA-N Ammonia Chemical compound N QGZKDVFQNNGYKY-UHFFFAOYSA-N 0.000 claims description 30
- LEONUFNNVUYDNQ-UHFFFAOYSA-N vanadium atom Chemical compound [V] LEONUFNNVUYDNQ-UHFFFAOYSA-N 0.000 claims description 28
- 239000002994 raw material Substances 0.000 claims description 24
- 238000002360 preparation method Methods 0.000 claims description 21
- 229910021529 ammonia Inorganic materials 0.000 claims description 15
- QVQLCTNNEUAWMS-UHFFFAOYSA-N barium oxide Chemical compound [Ba]=O QVQLCTNNEUAWMS-UHFFFAOYSA-N 0.000 claims description 14
- VNWKTOKETHGBQD-UHFFFAOYSA-N methane Chemical compound C VNWKTOKETHGBQD-UHFFFAOYSA-N 0.000 claims description 12
- 239000000463 material Substances 0.000 claims description 11
- 239000013078 crystal Substances 0.000 claims description 10
- 235000009508 confectionery Nutrition 0.000 claims description 6
- 239000003345 natural gas Substances 0.000 claims description 6
- 229910052785 arsenic Inorganic materials 0.000 claims description 5
- RQNWIZPPADIBDY-UHFFFAOYSA-N arsenic atom Chemical compound [As] RQNWIZPPADIBDY-UHFFFAOYSA-N 0.000 claims description 5
- XDBSEZHMWGHVIL-UHFFFAOYSA-M hydroxy(dioxo)vanadium Chemical compound O[V](=O)=O XDBSEZHMWGHVIL-UHFFFAOYSA-M 0.000 claims description 5
- PNXOJQQRXBVKEX-UHFFFAOYSA-N iron vanadium Chemical compound [V].[Fe] PNXOJQQRXBVKEX-UHFFFAOYSA-N 0.000 claims description 5
- 229910000628 Ferrovanadium Inorganic materials 0.000 claims description 4
- 230000003068 static effect Effects 0.000 claims description 4
- LSGOVYNHVSXFFJ-UHFFFAOYSA-N vanadate(3-) Chemical compound [O-][V]([O-])([O-])=O LSGOVYNHVSXFFJ-UHFFFAOYSA-N 0.000 claims description 4
- 150000001412 amines Chemical class 0.000 claims description 3
- 229910002804 graphite Inorganic materials 0.000 claims description 3
- 239000010439 graphite Substances 0.000 claims description 3
- -1 vanadium nitrides Chemical class 0.000 claims 7
- UHOVQNZJYSORNB-UHFFFAOYSA-N Benzene Chemical compound C1=CC=CC=C1 UHOVQNZJYSORNB-UHFFFAOYSA-N 0.000 claims 6
- 239000001257 hydrogen Substances 0.000 claims 2
- 229910052739 hydrogen Inorganic materials 0.000 claims 2
- 125000004435 hydrogen atom Chemical class [H]* 0.000 claims 2
- 239000011368 organic material Substances 0.000 claims 2
- 229920002472 Starch Polymers 0.000 claims 1
- 239000006229 carbon black Substances 0.000 claims 1
- 150000001722 carbon compounds Chemical class 0.000 claims 1
- 229910021393 carbon nanotube Inorganic materials 0.000 claims 1
- 239000002041 carbon nanotube Substances 0.000 claims 1
- 239000011295 pitch Substances 0.000 claims 1
- 230000035484 reaction time Effects 0.000 claims 1
- 239000008107 starch Substances 0.000 claims 1
- 235000019698 starch Nutrition 0.000 claims 1
- 229910000831 Steel Inorganic materials 0.000 abstract description 5
- 238000004519 manufacturing process Methods 0.000 abstract description 5
- 239000010959 steel Substances 0.000 abstract description 5
- 229910045601 alloy Inorganic materials 0.000 abstract description 4
- 239000000956 alloy Substances 0.000 abstract description 4
- 239000000654 additive Substances 0.000 abstract description 3
- 239000000843 powder Substances 0.000 abstract description 3
- 229910000640 Fe alloy Inorganic materials 0.000 abstract 1
- XHCLAFWTIXFWPH-UHFFFAOYSA-N [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] Chemical class [O-2].[O-2].[O-2].[O-2].[O-2].[V+5].[V+5] XHCLAFWTIXFWPH-UHFFFAOYSA-N 0.000 abstract 1
- 230000000903 blocking effect Effects 0.000 abstract 1
- 238000002425 crystallisation Methods 0.000 abstract 1
- 230000008025 crystallization Effects 0.000 abstract 1
- 229910001935 vanadium oxide Inorganic materials 0.000 abstract 1
- 239000000047 product Substances 0.000 description 22
- 238000010438 heat treatment Methods 0.000 description 6
- 238000005516 engineering process Methods 0.000 description 5
- 239000007789 gas Substances 0.000 description 5
- 238000005265 energy consumption Methods 0.000 description 4
- QJGQUHMNIGDVPM-UHFFFAOYSA-N nitrogen group Chemical group [N] QJGQUHMNIGDVPM-UHFFFAOYSA-N 0.000 description 4
- 230000002829 reductive effect Effects 0.000 description 4
- YXFVVABEGXRONW-UHFFFAOYSA-N Toluene Chemical compound CC1=CC=CC=C1 YXFVVABEGXRONW-UHFFFAOYSA-N 0.000 description 3
- ZMANZCXQSJIPKH-UHFFFAOYSA-N Triethylamine Chemical compound CCN(CC)CC ZMANZCXQSJIPKH-UHFFFAOYSA-N 0.000 description 3
- 238000000498 ball milling Methods 0.000 description 3
- 238000002156 mixing Methods 0.000 description 3
- 150000004682 monohydrates Chemical class 0.000 description 3
- 229920006395 saturated elastomer Polymers 0.000 description 3
- 239000004484 Briquette Substances 0.000 description 2
- XEEYBQQBJWHFJM-UHFFFAOYSA-N Iron Chemical compound [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 description 2
- 230000000996 additive effect Effects 0.000 description 2
- 230000002411 adverse Effects 0.000 description 2
- UNTBPXHCXVWYOI-UHFFFAOYSA-O azanium;oxido(dioxo)vanadium Chemical compound [NH4+].[O-][V](=O)=O UNTBPXHCXVWYOI-UHFFFAOYSA-O 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000007599 discharging Methods 0.000 description 2
- 239000001307 helium Substances 0.000 description 2
- 229910052734 helium Inorganic materials 0.000 description 2
- SWQJXJOGLNCZEY-UHFFFAOYSA-N helium atom Chemical compound [He] SWQJXJOGLNCZEY-UHFFFAOYSA-N 0.000 description 2
- 238000009413 insulation Methods 0.000 description 2
- 229920000126 latex Polymers 0.000 description 2
- 238000000465 moulding Methods 0.000 description 2
- 238000005121 nitriding Methods 0.000 description 2
- 239000007787 solid Substances 0.000 description 2
- 238000009628 steelmaking Methods 0.000 description 2
- GETQZCLCWQTVFV-UHFFFAOYSA-N trimethylamine Chemical compound CN(C)C GETQZCLCWQTVFV-UHFFFAOYSA-N 0.000 description 2
- WQEVDHBJGNOKKO-UHFFFAOYSA-K vanadic acid Chemical compound O[V](O)(O)=O WQEVDHBJGNOKKO-UHFFFAOYSA-K 0.000 description 2
- 238000003466 welding Methods 0.000 description 2
- INZDTEICWPZYJM-UHFFFAOYSA-N 1-(chloromethyl)-4-[4-(chloromethyl)phenyl]benzene Chemical compound C1=CC(CCl)=CC=C1C1=CC=C(CCl)C=C1 INZDTEICWPZYJM-UHFFFAOYSA-N 0.000 description 1
- FFRBMBIXVSCUFS-UHFFFAOYSA-N 2,4-dinitro-1-naphthol Chemical group C1=CC=C2C(O)=C([N+]([O-])=O)C=C([N+]([O-])=O)C2=C1 FFRBMBIXVSCUFS-UHFFFAOYSA-N 0.000 description 1
- 240000000233 Melia azedarach Species 0.000 description 1
- HJIYJLZFNBHCAN-UHFFFAOYSA-N [V].[C] Chemical compound [V].[C] HJIYJLZFNBHCAN-UHFFFAOYSA-N 0.000 description 1
- 239000011230 binding agent Substances 0.000 description 1
- 238000003763 carbonization Methods 0.000 description 1
- 238000006555 catalytic reaction Methods 0.000 description 1
- 238000000748 compression moulding Methods 0.000 description 1
- 238000010276 construction Methods 0.000 description 1
- 238000010924 continuous production Methods 0.000 description 1
- 230000008021 deposition Effects 0.000 description 1
- 239000000428 dust Substances 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 238000009851 ferrous metallurgy Methods 0.000 description 1
- 239000013067 intermediate product Substances 0.000 description 1
- 230000001788 irregular Effects 0.000 description 1
- 238000000462 isostatic pressing Methods 0.000 description 1
- 238000012423 maintenance Methods 0.000 description 1
- 238000002844 melting Methods 0.000 description 1
- 230000008018 melting Effects 0.000 description 1
- 210000003205 muscle Anatomy 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 230000036961 partial effect Effects 0.000 description 1
- 238000000634 powder X-ray diffraction Methods 0.000 description 1
- 238000009702 powder compression Methods 0.000 description 1
- 230000001681 protective effect Effects 0.000 description 1
- 239000000376 reactant Substances 0.000 description 1
- 238000011946 reduction process Methods 0.000 description 1
- 230000002787 reinforcement Effects 0.000 description 1
- 239000011347 resin Substances 0.000 description 1
- 229920005989 resin Polymers 0.000 description 1
- 238000007789 sealing Methods 0.000 description 1
- 230000035939 shock Effects 0.000 description 1
- 239000011343 solid material Substances 0.000 description 1
- 239000010935 stainless steel Substances 0.000 description 1
- 229910001220 stainless steel Inorganic materials 0.000 description 1
- 239000000126 substance Substances 0.000 description 1
- 238000002076 thermal analysis method Methods 0.000 description 1
- 238000007669 thermal treatment Methods 0.000 description 1
- 150000004684 trihydrates Chemical class 0.000 description 1
- 150000003682 vanadium compounds Chemical class 0.000 description 1
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- Inorganic Compounds Of Heavy Metals (AREA)
Abstract
Description
Claims (9)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 200510022245 CN1775661A (en) | 2005-12-07 | 2005-12-07 | Method for preparing vanadium nitride |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 200510022245 CN1775661A (en) | 2005-12-07 | 2005-12-07 | Method for preparing vanadium nitride |
Publications (1)
Publication Number | Publication Date |
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CN1775661A true CN1775661A (en) | 2006-05-24 |
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Family Applications (1)
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CN 200510022245 Pending CN1775661A (en) | 2005-12-07 | 2005-12-07 | Method for preparing vanadium nitride |
Country Status (1)
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CN (1) | CN1775661A (en) |
Cited By (11)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100457605C (en) * | 2006-07-06 | 2009-02-04 | 四川大学 | Process for preparing nano vanadium nitride and nano vanadium carbonitride powder |
CN101851749A (en) * | 2010-03-12 | 2010-10-06 | 江苏工业学院 | Method for preparing vanadium nitride coating by using low-temperature flowing layer and device thereof |
CN101392333B (en) * | 2007-09-20 | 2010-12-22 | 杭州天港生物科技有限公司 | Vanadium-nitrogen alloy preparation method and device |
CN103754839A (en) * | 2013-11-15 | 2014-04-30 | 上海大学 | Preparation method of nanocrystal vanadium nitride powder |
CN105087994A (en) * | 2015-09-06 | 2015-11-25 | 湖南众鑫新材料科技股份有限公司 | Method for preparing high-nitrogen high-purity vanadium-nitrogen alloy |
CN106006736A (en) * | 2016-05-16 | 2016-10-12 | 武汉理工大学 | Method of using hydrogen for preparing vanadium trioxide from vanadium-containing solution |
CN106399786A (en) * | 2016-11-25 | 2017-02-15 | 南通汉瑞新材料科技有限公司 | Novel method for preparing vanadium-nitrogen alloy |
CN106809808A (en) * | 2015-11-27 | 2017-06-09 | 中国科学院大连化学物理研究所 | A kind of preparation method of uniform hollow ball-shape VN nano particles |
CN109437126A (en) * | 2018-10-29 | 2019-03-08 | 福州大学 | A kind of method and application of simple synthesis VN hollow sphere |
CN114318015A (en) * | 2021-12-31 | 2022-04-12 | 马鞍山钢铁股份有限公司 | Treatment and utilization method of waste vanadium catalyst |
CN114873569A (en) * | 2022-06-15 | 2022-08-09 | 昆明理工大学 | Method for preparing high-quality vanadium nitride by vanadium oxide reduction nitridation under reducing atmosphere |
-
2005
- 2005-12-07 CN CN 200510022245 patent/CN1775661A/en active Pending
Cited By (14)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN100457605C (en) * | 2006-07-06 | 2009-02-04 | 四川大学 | Process for preparing nano vanadium nitride and nano vanadium carbonitride powder |
CN101392333B (en) * | 2007-09-20 | 2010-12-22 | 杭州天港生物科技有限公司 | Vanadium-nitrogen alloy preparation method and device |
CN101851749A (en) * | 2010-03-12 | 2010-10-06 | 江苏工业学院 | Method for preparing vanadium nitride coating by using low-temperature flowing layer and device thereof |
CN101851749B (en) * | 2010-03-12 | 2012-08-29 | 江苏工业学院 | Method for preparing vanadium nitride coating by using low-temperature flowing layer and device thereof |
CN103754839B (en) * | 2013-11-15 | 2016-01-13 | 上海大学 | A kind of preparation method of nanocrystal vanadium nitride powder |
CN103754839A (en) * | 2013-11-15 | 2014-04-30 | 上海大学 | Preparation method of nanocrystal vanadium nitride powder |
CN105087994A (en) * | 2015-09-06 | 2015-11-25 | 湖南众鑫新材料科技股份有限公司 | Method for preparing high-nitrogen high-purity vanadium-nitrogen alloy |
CN106809808A (en) * | 2015-11-27 | 2017-06-09 | 中国科学院大连化学物理研究所 | A kind of preparation method of uniform hollow ball-shape VN nano particles |
CN106006736A (en) * | 2016-05-16 | 2016-10-12 | 武汉理工大学 | Method of using hydrogen for preparing vanadium trioxide from vanadium-containing solution |
CN106399786A (en) * | 2016-11-25 | 2017-02-15 | 南通汉瑞新材料科技有限公司 | Novel method for preparing vanadium-nitrogen alloy |
CN109437126A (en) * | 2018-10-29 | 2019-03-08 | 福州大学 | A kind of method and application of simple synthesis VN hollow sphere |
CN114318015A (en) * | 2021-12-31 | 2022-04-12 | 马鞍山钢铁股份有限公司 | Treatment and utilization method of waste vanadium catalyst |
CN114318015B (en) * | 2021-12-31 | 2023-08-15 | 马鞍山钢铁股份有限公司 | Treatment and utilization method of waste vanadium catalyst |
CN114873569A (en) * | 2022-06-15 | 2022-08-09 | 昆明理工大学 | Method for preparing high-quality vanadium nitride by vanadium oxide reduction nitridation under reducing atmosphere |
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C06 | Publication | ||
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ASS | Succession or assignment of patent right |
Owner name: ZHEJIANG PROV JINXIN NEW MATERIAL TECHNOLOGY CO., Free format text: FORMER OWNER: FENG LIANGRONG Effective date: 20070105 |
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C41 | Transfer of patent application or patent right or utility model | ||
TA01 | Transfer of patent application right |
Effective date of registration: 20070105 Address after: 314511 Chong Fu Industrial Development Zone, Zhejiang, Tongxiang Applicant after: Zhejiang Jin Xin new Mstar Technology Ltd Address before: 610041 Chengdu Institute of organic chemistry, Chinese Academy of Sciences, No. two, 16 south section of the first ring road, Chengdu, Sichuan Applicant before: Feng Liangrong |
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C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
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Open date: 20060524 |