CN1759306A - Validation and revision method of dye solution comprising single or mixed dye for prescribed recipe as standard - Google Patents

Validation and revision method of dye solution comprising single or mixed dye for prescribed recipe as standard Download PDF

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CN1759306A
CN1759306A CNA038261316A CN03826131A CN1759306A CN 1759306 A CN1759306 A CN 1759306A CN A038261316 A CNA038261316 A CN A038261316A CN 03826131 A CN03826131 A CN 03826131A CN 1759306 A CN1759306 A CN 1759306A
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dye solution
concentration
dyestuff
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mixed
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CN100516829C (en
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赵现泰
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DYETEX ENGINEERING Co Ltd
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DYETEX ENGINEERING Co Ltd
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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/84Systems specially adapted for particular applications
    • G01N21/85Investigating moving fluids or granular solids
    • G01N21/8507Probe photometers, i.e. with optical measuring part dipped into fluid sample
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N21/00Investigating or analysing materials by the use of optical means, i.e. using sub-millimetre waves, infrared, visible or ultraviolet light
    • G01N21/17Systems in which incident light is modified in accordance with the properties of the material investigated
    • G01N21/25Colour; Spectral properties, i.e. comparison of effect of material on the light at two or more different wavelengths or wavelength bands
    • G01N21/31Investigating relative effect of material at wavelengths characteristic of specific elements or molecules, e.g. atomic absorption spectrometry

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Abstract

Disclosed is a method of inspecting a concentration of a dye solution including a single or a mixed dye based on a prescribed recipe as a standard to revise the concentration of the dye solution, in which light is transmitted to a first flow sensor installed in a dye solution measuring device, a second flow sensor using first optical fibers, or a dip prober having second optical fibers to directly dip a sensor in the dye solution to obtain absorptivity of the dye solution to calculate a concentration of a single dye solution, or concentrations of dyes constituting a mixed dye solution and a concentration off the mixed dye solution. In this regard, calculated concentrations of the dye solution and dyes are compared with prescribed concentrations of the dye solution and dyes to calculate amounts of the dyes and water additionally fed into the dye solution.

Description

Based on the method for measuring and adjust the dye solution that comprises single or mixed dye as the prescribed formula of standard
Technical field
Thereby the present invention relates generally to the method that a kind of concentration that detects the dye solution that comprises single or mixed dye based on the prescribed formula as standard is adjusted described dyes concentration.More specifically, thereby the present invention relates to the method that a kind of concentration that detects the dye solution that comprises single or mixed dye based on the prescribed formula as standard is adjusted described dyes concentration, wherein measure the concentration of homogencous dyes solution, or the concentration of the dyestuff of composition mixed dye solution and the concentration of mixed dye solution, with measurement concentration with homogencous dyes solution, or the normal concentration of the measurement concentration of the measurement concentration of dyestuff and mixed dye solution and the homogencous dyes solution shown in the prescribed formula, or the normal concentration of the normal concentration of dyestuff and mixed dye solution is made comparisons, thereby calculate the dyestuff also will be added in the dye solution and the amount of water, avoid in the dye solution preparation, aberration or batch difference taking place with this.
Background technology
Prepare initial dye solution on demand so that it is very important carrying out RFT (right first time) dyeing processing, in described RFT dyeing processing procedure, need not color correct or redye look.Yet, up to now do not develop as yet and can detect initial dye solution and whether prepare good any device, promptly allow to detect initial dye solution, do not know also how this changes the composition of relatively poor initial dye solution, and relatively poor like this initial dye solution can only abandoned.
Proposed to detect the whole bag of tricks of initial dye solution.For example, earlier in the color that in the laboratory, detects stained specimens, the processing of in factory, dyeing then; Perhaps earlier with the rough product colour that detects with initial dye solution dyeing of filter paper, the processing of dyeing then.Alternatively, the processing of also can under the situation that does not detect initial dye solution, dyeing.
Yet the shortcoming of the method for the initial dye solution of test sample is to postpone the time limit and reduce output after the stained specimens in the laboratory.In addition, do not detect under the situation of initial dye solution separately having, the consistance of dyed color reduces, and the possible look number of times that redyes increases relatively.
Be not used in simple, the accurate standardized method that detects initial dye solution in the prior art, also be not used in the device that detects initial dye solution, therefore when obtaining relatively poor initial dye solution, must discard relatively poor initial dye solution, perhaps must redye look when finding aberration handles, and when finding serious aberration and uneven color, must carry out black dyeing course again.
In addition, in factory, dye handle before, the color sample that will dye in the laboratory is made comparisons with the specified color shown in the prescription, and when color sample and specified color not simultaneously, must use extra dyestuff that sample is redyed look.Therefore, need a kind of accurate standardized system and method that is used to detect initial dye solution of research and development, redye the look processing thereby reduce, minimizing mixes because of mistake and forms the waste water that each component of initial dye solution produces.
Summary of the invention
Therefore, at the problems referred to above of the prior art, thereby one aspect of the present invention provides a kind of concentration that detects the dye solution that comprises single or mixed dye based on the prescribed formula as standard to adjust the method for described dyes concentration, wherein light is by being installed in the first flow sensor in the dye solution measurement mechanism, use second flow sensor of first optical fiber, or directly sensor is immersed the immersion probe that comprises second optical fiber in the dye solution, transfer to dye solution, thereby obtain the absorptance of dye solution, calculate the initial dye solution concentration of single or mixed dye solution thus.At this moment, when the measurement of the dyestuff of forming dye solution mix (concentration) than the regulation that is different from dyestuff mix (concentration) than the time, the ratio of components of change dye solution, thus reduce the aberration that causes because of relatively poor initial dye solution greatly.
Illustrate others of the present invention and/or advantage in the following description, these aspects and/or advantage are conspicuous in instructions, perhaps can draw from enforcement of the present invention.
Thereby realize above-mentioned and/or others by the method that provides the concentration that detects the dye solution that comprises single or mixed dye based on prescribed formula to adjust described dyes concentration as standard, described method comprises: the first step, transmit light to and be installed in the first flow sensor that wherein adds in the dye solution measurement mechanism that single or mixed dye solution are arranged, use second flow sensor of first optical fiber, or directly sensor is immersed the immersion probe that comprises second optical fiber in the dye solution, thereby, in the absorptance that records described dye solution corresponding to described light wavelength place; Second step, analyze the absorptance of described dye solution, calculate the concentration of homogencous dyes solution thus or form the concentration of dyestuff of mixed dye solution and the concentration of mixed dye solution, with with the calculating concentration of the calculating concentration of the calculating concentration of homogencous dyes solution or dyestuff and mixed dye solution with make comparisons as the normal concentration of the homogencous dyes solution shown in the prescribed formula of standard or the normal concentration of dyestuff and the normal concentration of mixed dye solution, thereby determine the concentration difference of dyestuff and dye solution; With the 3rd step, the dyestuff that uses described concentration difference to calculate also will to be added in the dye solution and the amount of water, thereby the normal concentration of the normal concentration of the calculating concentration that makes the calculating concentration of the calculating concentration of homogencous dyes solution or dyestuff and mixed dye solution and homogencous dyes solution or dyestuff and the normal concentration of mixed dye solution are consistent, and show the calculated amount of dyestuff and water.
At this moment, described dye solution measurement mechanism comprises spectrophotometer.
In addition, described sensor comprises first or second flow sensor that is connected with the dye solution measurement mechanism, its structure comprises with predetermined space and is installed in two quartz chambers in first or second flow sensor, so that dye solution smooth flow between two quartz chambers, to transmit light to dye solution thus, the structure of first or second flow sensor makes vertical connection of outside surface of first quartz chamber in the 3rd optical fiber and described two quartz chambers, transferring to dye solution by first quartz chamber from the light that the dye solution measurement mechanism comes, and second in the 4th optical fiber and described two quartz chambers quartz chamber outside surface is vertical is connected, delivering to the dye solution measurement mechanism by the light of first quartz chamber and dye solution, or first or second flow sensor comprise the immersion probe, its structure makes light transfer to dye solution by arbitrary of being installed in two second optical fiber in the immersion probe, and is sent to another root in two second optical fiber through the light of mirror reflects.
In addition, according to the present invention, the calculating concentration of the calculating concentration of the calculating concentration of homogencous dyes solution and pH or dyestuff and pH and mixed dye solution and pH; The normal concentration of the homogencous dyes solution shown in the prescribed formula or the normal concentration of dyestuff and the normal concentration of mixed dye solution; The concentration difference of dyestuff and dye solution; The amount that also will be added to dyestuff in the dye solution and water is presented on the monitor and is stored in the database.
Above-mentioned and/or others can realize by the method that also comprises the steps is provided: the automatic or manual water is with the described single or mixed dye solution of predetermined dilution ratio dilution, thereby easily measure the concentration of homogencous dyes solution or form the concentration of dye solution of mixed dye solution and the concentration of mixed dye solution, and the single or mixed dye solution that will dilute is delivered to described first or second flow sensor by ebullator.
Above-mentioned and/or others can realize by the method that also comprises the steps is provided: the solenoid valve of opening installation on pipe, described pipe is used for connecting the beaker that fills single or mixed dye solution or container and is used for dyestuff and water are added to the groove of described beaker or container, with with extra dyestuff and water is added to single or mixed dye solution in, thereby make the calculating concentration of homogencous dyes solution, or the normal concentration of the calculating concentration of the calculating concentration of dyestuff and mixed dye solution and homogencous dyes solution, or the normal concentration of the normal concentration of dyestuff and mixed dye solution is consistent.
Description of drawings
From detailed description below in conjunction with accompanying drawing, can more be expressly understood above-mentioned and others, feature and other advantage of the present invention, wherein:
Fig. 1~3 schematically show dye solution measuring system of the present invention;
Fig. 4 is the automatic dilution device of the dye solution measuring system of displayed map 1~3 schematically;
Fig. 5 is presented at the measurement concentration of using dyestuff and dye solution under the mixed dye solution situation;
Fig. 6 is presented at the measurement concentration of using dyestuff and dye solution under the 0.5g/l yellow mother situation;
Fig. 7 is presented at the measurement concentration of using dyestuff and dye solution under the red mother liquor situation of 0.5g/l; And
Fig. 8 is presented at the measurement concentration of using dyestuff and dye solution under the blue mother liquor situation of 0.5g/l.
Embodiment
With reference now to accompanying drawing,, wherein identical Reference numeral is used in reference to same or analogous element in different accompanying drawings.
Be the concentration of the concentration of measuring homogencous dyes solution or the dyestuff of forming mixed dye solution and the concentration of mixed dye solution, use automatic dilution device 1 shown in Figure 4 with predetermined dilution than dilution after, will be in the laboratory or the single or mixed dye solution that makes of factory use ebullator to deliver to flow sensor.
Specifically, when using electronic balance 16 to weigh to place the single or mixed dye solution of beaker or container 15, center processing and control module 18 are gathered the weight data of single or mixed dye solution in real time by measurement and control module 17, calculate the amount that can dilute the water of single or mixed dye solution with required dilution ratio then.
Center processing is used for opening at pipe 14a, 14b place and the solenoid valve 13a, the 13b that are connected with warm water tank 12 with cold rinse bank 11 by measuring with control module 17 with control module 18, thereby cold water and warm water are delivered to beaker or container 15.In this, the weight of center processing and 18 fens bleeds of control module, electronic balance 16 measure single or mixed dye solution with control electromagnetic valve 13a, 13b, check that simultaneously whether the water of capacity is sent to beaker or container 15.
Preferably, cold rinse bank 11 links to each other with beaker or container 15 with the pipe of warm water tank 12 by different-diameter.At this moment, solenoid valve is installed in respectively on the described pipe.During beginning, the solenoid valve that is installed on the larger-diameter pipe is opened so that relatively large water is being supplied to beaker or container in the short period relatively.When the water yield during near scheduled volume, being installed in is opened than the solenoid valve on the minor diameter delivers to the water yield of beaker or container with accurate control, thereby shortens the dilution time of dye solution, and accurately controls the dilution ratio of dye solution.
Selectively, the technician can manually dilute the dye solution that comprises single or mixed dye, and does not use automatic dilution device 1.
Shown in Fig. 1~3, the single or mixed dye solution of dilution is delivered to the first or second flow sensor 3a, 3b by ebullator 2, or dye solution container 21.That is to say, when the end of circulation pipe 8 10b is immersed in the single or mixed dye solution in beaker or the container 15, operation cycle pump 2, single or mixed dye solution is delivered to the first or second flow sensor 3a, 3b by circulation pipe 8, and when shut-down operation ebullator 2, end 10b by circulation pipe 8 discharges single or mixed dye solution, or collects into dye solution container 21 by the end 10b of circulation pipe 8.
In this, transmit light to single or mixed dye solution comprising the dye solution measurement mechanism 4 of first flow sensor 3a, deliver to center processing and control module 5 with the data of the absorptance that will be used to calculate single or mixed dye solution by circulation pipe 8.
Be suitable among the present invention and make the spectrophotometer of dye solution measurement mechanism 4 and the first flow sensor 3a of Fig. 1 is combined into one, or use the second flow sensor 3b of optical fiber 9a, 9b and Fig. 2 to make up, or use the immersion probe 3c combination of optical fiber 9a, 9b and Fig. 3.
Its structure of flow sensor 3b of using with dye solution measurement mechanism 4 among Fig. 2 comprises with predetermined space and is installed in two quartz chambers on the flow sensor 3b, so that dye solution smooth flow between two quartz chambers, to transmit light to dye solution thus.Selectively, the structure of flow sensor 3b makes vertical connection of outside surface of first quartz chamber in an optical fiber and described two quartz chambers, transferring to dye solution by first quartz chamber from the light that the dye solution measurement mechanism comes, and second in another root optical fiber and described two quartz chambers quartz chamber outside surface is vertical is connected, delivering to the dye solution measurement mechanism by the light of first quartz chamber and dye solution.
In addition, as shown in Figure 3, its structure of immersion probe 3c of using with dye solution measurement mechanism 4 makes light by being installed in arbitrary dye solution that transfers in the dye solution container 21 in two second optical fiber among the immersion probe 3c, and is sent to another root in two second optical fiber through the light of mirror reflects.
Center processing and control module 5 be used for using the memory that is installed on wherein or separately the algorithm of memory explain the data of sending from dye solution measurement mechanism 4, to calculate the concentration of homogencous dyes solution, or the concentration of the dyestuff of composition mixed dye solution and the concentration of mixed dye solution, thereby calculating concentration with homogencous dyes solution, or the calculating concentration of the calculating concentration of dyestuff and mixed dye solution with as the normal concentration of the homogencous dyes solution shown in the prescribed formula of standard, or the normal concentration of the normal concentration of dyestuff and mixed dye solution makes comparisons, thereby calculates the dyestuff that also will be added in single or the mixed dye solution and the amount of water.Calculated amount with dyestuff and water is presented on the monitor 6 then.
At this moment, calculating concentration and the calculating concentration of pH or dyestuff and the calculating concentration and the pH of pH and mixed dye solution of the homogencous dyes solution that calculates by center processing and control module 5; The normal concentration of the homogencous dyes solution shown in the prescribed formula or the normal concentration of dyestuff and the normal concentration of mixed dye solution; The concentration difference of dyestuff and dye solution; The amount that also will be added to dyestuff in the dye solution and water is presented on the monitor 6 and is stored in the database 7.
As mentioned above, (beaker or the container that are used for filling single or mixed dye solution are connected with groove at pipe by opening installation, so that dyestuff and water are added in beaker or the container) on solenoid valve, extra dyestuff and water are added in the single or mixed dye solution in beaker or the container, thereby make the calculating concentration of homogencous dyes solution, or the normal concentration of the calculating concentration of the calculating concentration of dyestuff and mixed dye solution and homogencous dyes solution, or the normal concentration of the normal concentration of dyestuff and mixed dye solution is consistent, thereby obtains having with prescribed formula the dye solution of same mixture ratio.Therefore, improved repeatability, and greatly reduced the number of times that redyes look with poststaining.
The present invention may be better understood by reading the following examples, and wherein embodiment is used to illustrate rather than is used to limit the present invention.
Embodiment 1
Fig. 5 shows mixed dye solution is delivered to the first flow sensor 3a of dye solution measuring system shown in Figure 2 by ebullator after, transmit light to the result of the absorptance of the measured mixed dye solution that comprises three kinds of dyestuffs of mixed dye solution by optical fiber 9a, 9b, be the two ends that quartz chamber is connected to optical fiber 9a, 9b in the sensor, do not have water diluted mixture dye solution.
In Fig. 5, the normal concentration of three kinds of dyestuffs shown in the prescribed formula (weld (001), orchil (002), blue dyes (003)) is as follows: the concentration of mixed dye solution is 1.500g/l, and the concentration of three kinds of dyestuffs is respectively 0.500g/l, 0.500g/l and 0.500g/l.In addition, the measurement concentration of mixed dye solution is 1.4838g/l, and the measurement concentration of yellow, redness and blue dyes is respectively 0.4810g/l, 0.4986g/l and 0.5041g/l.In addition, the measurement of three kinds of dyestuffs and the concentration difference between normal concentration are respectively-3.80% ,-0.28% and 0.82%.
Based on dye solution total amount and dilution ratio (measurement of three kinds of dyestuffs with all different each other situation of normal concentration under) automatically calculating also to be added to amount of dye in the mixed dye solution (0.023g, 0.006g, 0.000g) and the water yield (0.011).
Simultaneously, even the dyeing that the prescribed formula of determining according to the sample dyeing course in the laboratory carries out in the factory is handled, still between factory products and laboratory sample, still can produce aberration.Multiple reason all can cause aberration.For example, using under the situation of transferring liquid systems (CCK) preparation dye solution automatically, when replacing the dye solution of using with new dye solution under the situation of not considering the accurate concentration of CCK mother liquor, mother liquor term of life, dyestuff batch difference, aberration may appear.In addition, because high temperature and high humidity atmosphere in the dyeing company laboratory, and the mother liquor that contains dye solution is higher than the mother liquor original concentration than the mother liquid concentration of lower part, and do not have the mother liquor of dye solution wetting by the thermogenetic dew that condenses because of steam than top, thereby the vaporization of CCK mother liquor acceleration, so aberration may take place.In addition, even the mother liquor regular regeneration is produced or replace used mother liquor according to the dye solution amount that consumes with new mother liquor in good time, but because different technician prepares mother liquor, so also concentration difference may take place.
Embodiment 2
Fig. 6, Fig. 7 and Fig. 8 show mixed dye solution is delivered to the first flow sensor 3a of Fig. 2 dye solution measuring system by ebullator after, transmit light to the result of the absorptance of the measured yellow of mixed dye solution, redness and blue dyes solution (each dyes concentration is 0.5g/l) by optical fiber 9a, 9b, be the two ends that quartz chamber is connected to optical fiber 9a, 9b in the sensor, do not have the dilute with water dye solution.At this moment, the normal concentration of yellow, redness and blue dyes is respectively 0.5g/l, 0.5g/l, 0.5g/l, and it measures concentration is respectively 0.5017g/l, 0.5035g/l, 0.5016g/l.Therefore, concentration difference is 0.34%, 0.70%, 0.32%, and measuring error is less than 1%.
Therefore, according to the present invention, the concentration by measuring the dye solution make in the CCK process and the concentration (CCK mother liquor) of homogencous dyes solution can be controlled the CCK mother liquor effectively, thereby avoid in the preparation of dye solution aberration taking place.
Industrial applicibility
From above-mentioned instructions as can be seen, the invention has the advantages that, when in factory, preparing dye solution, when the normal concentration of the measurement concentration of dye solution and dye solution not simultaneously, whether decision need be added to extra dyestuff and water in the dye solution according to breadboard prescribed formula, thereby avoids in the dye solution preparation aberration or batch difference taking place.
Other advantage of the present invention is, the concentration difference of the initial dye solution by reducing laboratory and factory can reduce the water yield that redyes look number of times, consumption and the amount of pollutant, thereby improves the output and the quality of product.
In sum, the invention has the advantages that 1) the measurement absorptance by dye solution relatively and the regulation absorptance of dye solution to be to reduce the aberration that concentration difference can avoid the dyes concentration difference to cause; 2) can easily determine the batch difference of dyestuff by standard of comparison dyes concentration and the dyes concentration newly bought; 3) dyes concentration keeps constant, can accurately determine the dye solution amount of discharging from circulation pipe by checking mother liquid concentration; And 4) when the measurement concentration of dye solution and normal concentration differ from one another, under dip dyeing, continuous dyeing and cold liquid roll compacting (CPB) dyeing situation, can accurately measure dyes concentration, thereby the method that detects and adjust dyes concentration according to the prescribed formula as standard is provided.
Although disclose the preferred embodiments of the invention, it should be understood by those skilled in the art that, in not breaking away from the disclosed scope of the invention of claims and spirit, can make various modifications, increase or replacement.

Claims (6)

1. thereby a concentration that detects the dye solution that comprises single or mixed dye based on the prescribed formula as standard is adjusted the method for described dyes concentration, and this method comprises:
The first step, transmit light to and be installed in wherein the first flow sensor that adds in the dye solution measurement mechanism that single or mixed dye solution are arranged, second flow sensor that uses first optical fiber or directly sensor immersed the immersion probe that comprises second optical fiber in the dye solution, thereby in the absorptance that records described dye solution corresponding to described light wavelength place;
Second step, analyze the absorptance of described dye solution, calculate the concentration of homogencous dyes solution thus or form the concentration of dyestuff of mixed dye solution and the concentration of mixed dye solution, with with the calculating concentration of the calculating concentration of the calculating concentration of homogencous dyes solution or dyestuff and mixed dye solution with make comparisons as the normal concentration of the homogencous dyes solution shown in the prescribed formula of standard or the normal concentration of dyestuff and the normal concentration of mixed dye solution, thereby determine the concentration difference of dyestuff and dye solution; And
The 3rd step, the dyestuff that uses described concentration difference to calculate also will to be added in the dye solution and the amount of water, thereby the normal concentration of the normal concentration of the calculating concentration that makes the calculating concentration of the calculating concentration of homogencous dyes solution or dyestuff and mixed dye solution and homogencous dyes solution or dyestuff and the normal concentration of mixed dye solution are consistent, and show the calculated amount of described dyestuff and water.
2. the method for claim 1, wherein said dye solution measurement mechanism comprises spectrophotometer.
3. the method for claim 1, wherein said sensor comprises first or second flow sensor that is connected with the dye solution measurement mechanism, its structure comprises with predetermined space and is installed in two quartz chambers in first or second flow sensor, so that dye solution smooth flow between two quartz chambers, to transmit light to dye solution thus, the structure of first or second flow sensor makes vertical connection of outside surface of first quartz chamber in the 3rd optical fiber and described two quartz chambers, transferring to dye solution by first quartz chamber from the light that the dye solution measurement mechanism comes, and second in the 4th optical fiber and described two quartz chambers quartz chamber outside surface is vertical is connected, delivering to the dye solution measurement mechanism by the light of first quartz chamber and dye solution, or first or second flow sensor comprise the immersion probe, its structure makes light transfer to dye solution by arbitrary of being installed in two second optical fiber in the immersion probe, and is sent to another root in two second optical fiber through the light of mirror reflects.
4. the method for claim 1, the wherein calculating concentration of the calculating concentration of the calculating concentration of homogencous dyes solution and pH or dyestuff and pH and mixed dye solution and pH; The normal concentration of the homogencous dyes solution shown in the prescribed formula or the normal concentration of dyestuff and the normal concentration of mixed dye solution; The concentration difference of dyestuff and dye solution; The amount that also will be added to dyestuff in the dye solution and water is presented on the monitor and is stored in the database.
5. the method for claim 1, it comprises that also the automatic or manual water is with the described single or mixed dye solution of predetermined dilution ratio dilution, thereby easily measure the concentration of homogencous dyes solution or form the concentration of dye solution of mixed dye solution and the concentration of mixed dye solution, and the single or mixed dye solution that will dilute is delivered to described first or second flow sensor by ebullator.
6. the method for claim 1, it also comprises the solenoid valve of opening installation on pipe, described pipe is used for connecting the beaker that fills single or mixed dye solution or container and is used for dyestuff and water are added to the groove of described beaker or container, with with extra dyestuff and water is added to single or mixed dye solution in, thereby the normal concentration of the normal concentration of the normal concentration of the calculating concentration that makes the calculating concentration of the calculating concentration of homogencous dyes solution or dyestuff and mixed dye solution and homogencous dyes solution or dyestuff and mixed dye solution is consistent.
CNB038261316A 2003-03-10 2003-03-21 Validation and revision method of dye solution comprising single or mixed dye for prescribed recipe as standard Expired - Fee Related CN100516829C (en)

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KR100348103B1 (en) * 1999-08-11 2002-08-09 주식회사 다이텍스 엔지니어링 The real time dyeing control method and its system

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* Cited by examiner, † Cited by third party
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CN100458415C (en) * 2007-02-02 2009-02-04 威海拓展纤维有限公司 Method for detecting concentration of oil solution in producing polyacrylonitrile raw yarn in use for carbon fiber
CN102818776A (en) * 2012-08-08 2012-12-12 赵晓明 Dye liquor concentration in-situ on-line monitoring system
CN103383351A (en) * 2013-07-22 2013-11-06 上海嘉麟杰纺织品股份有限公司 Method for testing capacity expansion quantity of disperse dyes by auxiliaries
CN111272670A (en) * 2020-02-26 2020-06-12 北京机科国创轻量化科学研究院有限公司 Dyeing quality detection method and device, storage medium and processor

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WO2004081544A1 (en) 2004-09-23
AU2003215948A1 (en) 2004-09-30

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