CN1739725A - Production process of aloe gel concentrated powder for cosmetics - Google Patents
Production process of aloe gel concentrated powder for cosmetics Download PDFInfo
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- CN1739725A CN1739725A CN 200510098864 CN200510098864A CN1739725A CN 1739725 A CN1739725 A CN 1739725A CN 200510098864 CN200510098864 CN 200510098864 CN 200510098864 A CN200510098864 A CN 200510098864A CN 1739725 A CN1739725 A CN 1739725A
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Abstract
The production process of aloe gel concentrated powder for cosmetics features that fresh Aloe vera leaf pulp (gel) as main material is produced into the aloe gel concentrated powder in one optimized production process based on strict technological requirement and relevant standards. The product is brown powder of 100 % purity and with well reserved bioactivity of aloe and high aloe polysaccharide content, safe and hygienic, and may be used for high grade cosmetics.
Description
Production process of aloe gel concentrated powder for cosmetics relates to aloe raw material product processing, and especially Fresh mesophyll of aloe (gel) being processed into industrialized form can be for the processing method of the aloe gel concentrated dried powder of high-grade Aloe cosmetics manufacturing use.
Production process of aloe gel concentrated powder for cosmetics background technology situation: Aloe is the very abundant natural plants of a kind of nutritional labeling, is extensive use of in manufacturing fields such as medicine, food, health product, cosmetics in the world.Especially the polysaccharide that contains in the Aloe, mineral, phytosterin compound, and aloin, Aloe resin B, aminoacid, vitamin etc., have many-side and beautify the usefulness of skin, preserve moisture, aspect such as antiinflammatory, antibacterial, antipruritic, antiallergic, softening skin, anti-acne, antiperspirant deodorant has better action.But the Aloe industry development is later in China, and the processing of Fresh leaf of aloe also is in the starting stage, a little less than the conversion capability from aloe raw material to the aloe raw material product, the quality of converted products is low, and product market competitiveness is poor, and resource does not obtain fully, utilization effectively and reasonably.Therefore, strict establishing criteria adopts scientific method, manage to cut down finished cost, produce quality height, quality is good, specification is complete aloe raw material product, satisfying the various market demand of demand that forms day by day, this is China's difficult problem that will solve in the Aloe industry at present just.Aloe gel concentrated dried powder does not have concrete standard at QB/T 2488-2000, and this product is the product that designs according to QB/T 2488-2000 basic index and the market demand.
The present invention is to provide a kind of production process of aloe gel concentrated powder for cosmetics, not only Fresh leaf of aloe can be processed into and meet the aloe gel concentrated dried powder that standard is used in the cosmetics manufacturing, and be a kind of industrialization processing method, improved the productivity effect of aloe gel concentrated dried powder greatly.This development to China's Aloe industry has significance.
Production process of aloe gel concentrated powder for cosmetics is: with Fresh mesophyll of aloe (gel) is raw material, with the organoleptic indicator of aloe raw material converted products, physical and chemical index, sanitary index etc. is quality standard, with the relevant sanitary legislation of country and industry, standard is the target level of product quality foundation, select materials the processing aloe gel concentrated powder for cosmetics → cleaning and sterilization → peeling → making beating → squeezing → fine grinding → filtration → membrance concentration → vacuum drying → superfine grinding → this technological process of production of sterilization → packing → finished product according to what experiment was determined.
Adopt such scheme, can obtain the aloe gel concentrated dried powder product of accord with Q B/T2488-2000 basic index requirement.This product can use for high-grade Aloe cosmetics manufacturing.
The specific embodiment of production process of aloe gel concentrated powder for cosmetics, do as detailed below:
The production environment condition: the processing aloe gel concentrated powder for cosmetics will be finished in the cleaning sterile workshop of GMP compatible, and the air cleaning rank reaches 100,000 grade standards.This environmental requirement is to propose by aloe raw material product machining experiment up to standard.
Select materials: select for use by the nuisanceless standard plantation and the fresh blade of Aloe vulgaris in growth 2 anniversaries of expiration, rejecting has the scab position; Should be controlled within 8 hours from Aloe plant harvesting blade to factory process.This technological requirement be by mycete grow the experiment determined.The Fresh leaf of aloe sheet that is mechanically damaged when experimental results show that harvesting is under condition more than 15 ℃, and the blade injury position will have mycete to produce after 8 hours.
Cleaning and sterilization: divided for three steps carried out.The first step is put into the XY type recirculated water cleaning machine made from rustless steel with the Fresh leaf of aloe after selecting materials, and washes Fresh leaf of aloe surface silt and dirt off with the clean water that meets drinking water standard.Second step put into the cleaning and sterilizing pond that fills Ozone Water with Fresh leaf of aloe and soaked 5 minutes, to kill each bacterioid and to remove pesticide residues.Ozone Water is to enter in the water of cleaning and sterilizing pond formedly after gas-liquid mixing pump mixes by the certain density ozone that pretreated air admission ozonator produces, and the ozone concentration of its Ozone Water should be controlled at 10-20mg/m
3The 3rd step was put into mobile sterilized water rinsing 3 minutes with Fresh leaf of aloe, with bacteriological protection cross-contamination in the cleaning and sterilization process.This technological requirement is determined by GB/T7918.2-1987 total number of bacteria assay method and experimental result.
Peeling: with the peeling machine that rustless steel is made, with the Fresh leaf of aloe de-epithelization behind the cleaning and sterilization, it is standby to get meat (gel).
Making beating: the Fresh mesophyll of aloe (gel) after the beater made from rustless steel will be removed the peel breaks into aloe juice.
Squeezing: with squeezer aloe juice is squeezed the juice, its juice is Aloe gel stock solution.It is dried more good more to squeeze the juice, with the no longer excessive degree of being of juice.
Fine grinding: adopt colloid mill that aloe stoste is ground, make the further refinement of aloe stoste, and reach the homogenizing purpose.
Filter: through the aloe stoste that fine grinding obtains, also have the thinner fibrous tissue of part granule to be suspended in the juice, along with the prolongation meeting of resting period is slowly sunk, stable unfavorable to product.Therefore, adopt the centrifugal fine filter of ultrahigh speed to remove the thin sticking granule of slow (≤0.2 mm/second) of those sedimentation velocity.
Membrance concentration: the Aloe gel stock solution after will filtering enters membrane separation concentrated compression apparatus and carries out membrance concentration.The membrance concentration biggest advantage is to realize that normal temperature condition concentrates down, avoids in the course of processing Yin Wendu too high and the Aloe bioactive ingredients is run off, and has kept the color and luster and the local flavor of product, has guaranteed the quality of product.Membrance separation is to utilize the macromolecule semipermeable membrane, with the pressure differential of film both sides, when impelling some molecule in the fluid to see through semipermeable membrane and be retained down, to obtain a kind of isolation technics of some composition in the fluid.When by semipermeable membrane be solvent, then solution has obtained to concentrate, this process is exactly a membrance concentration.The Aloe gel stock solution membrance concentration should adopt the reverse osmosis isolation method, and osmotic pressure should be controlled at 2.0～6.5MPa.This technological requirement is determined by Aloe gel stock solution membrance concentration experimental result.Through membrance concentration, when the volume of concentrated solution reach the Aloe gel stock solution volume 40～45% the time, the concentrated solution of this moment is a thick liquid, stopper film concentrates.
Vacuum drying: adopt YZG, FZG vacuum drier that the aloe gel concentrate behind membrance concentration is carried out vacuum drying.Vacuum drying is to utilize the vacuum pump dehumidifier of bleeding to make in the operating room and to form vacuum state, and aloe extract is in carries out heat drying under the static vacuum condition, its objective is that realization obtains higher rate of drying at a lower temperature, avoid Aloe bioactive substance Yin Wendu too high and run off.The vacuum drier vacuum pressure is controlled at below the 0.784MPa, and under-this condition of 0.1MPa, when heating-up temperature was 110 ℃, the vaporization rate of water can reach 7.2kg/m in the aloe extract
2H, this technological requirement is determined by the aloe extract drying experiment.Aloe gel concentrate has obtained material after vacuum drying treatment, for Aloe gel concentrates material.Aloe gel concentrates the material degree of drying and requires to reach water content below 8%.
Superfine grinding: concentrate material with the Aloe gel of WFJ-30 type atomizer after with vacuum drying and pulverize, fineness of powder is determined between 350 order to 400 orders.The powder that obtains after crushed is an aloe gel concentrated dried powder.
Sterilization: aloe gel concentrated dried powder is sterilized at last with the ultraviolet sterilization method.Under Burdick lamp, aloe gel concentrated dried powder is placed thickness should be controlled at 6～8cm, every 2 hours, aloe gel concentrated dried powder is stirred once.Sterilization time requires to reach 12 hours.This technological requirement is determined by experiment.
Packing: with aseptic aluminide-coating bag vacuum packaging, every bag of 2.5kg is advisable.
Finished product: be " aloe gel concentrated powder for cosmetics ".
The organoleptic indicator: brown ceramic powder, purity is 100%, has the aloe plant flavor, does not have other abnormal flavour; Be exposed to irradiation 6h under the Burdick lamp, do not change color.This is the index determined of result by experiment.
Physical and chemical index: absorbance (400m, 0.5% aqueous solution)≤0.10; PH value (0.5% aqueous solution) is 3.5-4.7; Moisture (%)≤8.0; Calcium (mg/kg) 〉=1.96 * 10
4Magnesium (mg/kg) 〉=4.68 * 10
3Aloe polysaccharide (mg/kg) 〉=1.20 * 10
3This is the index determined of result by experiment.
Sanitary index: plumbous (mg/kg)≤30; Hydrargyrum (mg/kg)≤1; Arsenic (mg/kg)≤10; Total number of bacteria (individual/g)≤500; Excrement colibacillus group (every gram), staphylococcus aureus (every gram), bacillus pyocyaneus (every gram) must not detect.Above sanitary index is pressed GB/T7917.3-1987, GB/T7917.1-1987, GB/T7917.2-1987, GB/T7918.2-1987, GB/T7918.3-1987, GB/T7918.5-1987, the determined index of GB/T7918.4-1987 assay respectively.
Claims (3)
1, a kind of production process of aloe gel concentrated powder for cosmetics.It is characterized in that: with Fresh mesophyll of aloe (gel) is raw material, with the organoleptic indicator of aloe raw material converted products, physical and chemical index, sanitary index etc. is quality standard, with the relevant sanitary legislation of country and industry, standard is the target level of product quality foundation, select materials the processing aloe gel concentrated powder for cosmetics → cleaning and sterilization → peeling → making beating → squeezing → fine grinding → filtration → membrance concentration → vacuum drying → superfine grinding → this technological process of production of sterilization → packing → finished product according to what experiment was determined.
2, production process of aloe gel concentrated powder for cosmetics according to claim 1, it is characterized in that: the technological process of production and processing method are defined as, select materials: select for use by the nuisanceless standard plantation and the fresh blade of Aloe vulgaris in growth 2 anniversaries of expiration, rejecting has the scab position; Should be controlled within 8 hours from Aloe plant harvesting blade to factory process.Cleaning and sterilization: divided for three steps carried out.The first step is put into the XY type recirculated water cleaning machine made from rustless steel with the Fresh leaf of aloe after selecting materials, and washes Fresh leaf of aloe surface silt and dirt off with the clean water that meets drinking water standard.Second step put into the cleaning and sterilizing pond that fills Ozone Water with Fresh leaf of aloe and soaked 5 minutes, to kill each bacterioid and to remove pesticide residues.The 3rd step was put into mobile sterilized water rinsing 3 minutes with Fresh leaf of aloe, with bacteriological protection cross-contamination in the cleaning and sterilization process.Peeling: with the peeling machine that rustless steel is made, with the Fresh leaf of aloe de-epithelization behind the cleaning and sterilization, it is standby to get meat (gel).Making beating: the Fresh mesophyll of aloe (gel) after the beater made from rustless steel will be removed the peel breaks into aloe juice.Squeezing: with squeezer aloe juice is squeezed the juice, its juice is Aloe gel stock solution.Fine grinding: adopt colloid mill that aloe stoste is ground, make the further refinement of aloe stoste, and reach the homogenizing purpose.Filter: adopt the centrifugal fine filter of ultrahigh speed to remove the thin sticking granule of slow (≤0.2 mm/second) of those sedimentation velocity.Membrance concentration: the Aloe gel stock solution after will filtering enters membrane separation concentrated compression apparatus and carries out membrance concentration.The Aloe gel stock solution membrance concentration adopts the reverse osmosis isolation method, and osmotic pressure is controlled at 2.0～6.5MPa.Through membrance concentration, when the volume of concentrated solution reach the Aloe gel stock solution volume 40～45% the time, the concentrated solution of this moment is a thick liquid, stopper film concentrates.Vacuum drying: adopt YZG, FZG vacuum drier that the aloe gel concentrate behind membrance concentration is carried out vacuum drying.The vacuum drier vacuum pressure is controlled at below the 0.784MPa, and under-this condition of 0.1MPa, when heating-up temperature was 110 ℃, the vaporization rate of water can reach 7.2kg/m in the aloe extract
2H.Aloe gel concentrate has obtained material after vacuum drying treatment, for Aloe gel concentrates material.Aloe gel concentrates the material degree of drying and requires to reach water content below 8%.Superfine grinding: concentrate material with the Aloe gel of WFJ-30 type atomizer after with vacuum drying and pulverize, fineness of powder is determined between 350 order to 400 orders.The powder that obtains after crushed is an aloe gel concentrated dried powder.Sterilization: aloe gel concentrated dried powder is sterilized at last with the ultraviolet sterilization method.Under Burdick lamp, aloe gel concentrated dried powder is placed thickness should be controlled at 6～8cm, every 2 hours, aloe gel concentrated dried powder is stirred once.Sterilization time requires to reach 12 hours.Packing: with aseptic aluminide-coating bag vacuum packaging, every bag of 2.5kg is advisable.Finished product: be " aloe gel concentrated powder for cosmetics ".
3, production process of aloe gel concentrated powder for cosmetics according to claim 1 is characterized in that: the organoleptic indicator who determines is, brown ceramic powder, and purity is 100%, has the aloe plant flavor; Be exposed to irradiation 6h under the Burdick lamp, do not change color.The physical and chemical index of determining is absorbance (400nm, 0.5% aqueous solution)≤0.10; PH value (0.5% aqueous solution) is 3.5-4.7; Moisture (%)≤8.0; Calcium (mg/kg) 〉=1.96 * 10
4Magnesium (mg/kg) 〉=4.68 * 10
3Aloe polysaccharide (mg/kg) 〉=1.20 * 10
3The sanitary index of determining is plumbous (mg/kg)≤30; Hydrargyrum (mg/kg)≤1; Arsenic (mg/kg)≤10; Total number of bacteria (individual/g)≤500; Excrement colibacillus group (every gram), staphylococcus aureus (every gram), bacillus pyocyaneus (every gram) must not detect.
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| CN 200510098864 CN1739725A (en) | 2005-09-04 | 2005-09-04 | Production process of aloe gel concentrated powder for cosmetics |
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Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118240106A (en) * | 2024-04-02 | 2024-06-25 | 广州市东源药业科技有限公司 | Preparation method for forming colloid bundle emulsion by using aloe polysaccharide mediated silicone oil |
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Cited By (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN118240106A (en) * | 2024-04-02 | 2024-06-25 | 广州市东源药业科技有限公司 | Preparation method for forming colloid bundle emulsion by using aloe polysaccharide mediated silicone oil |
| CN118240106B (en) * | 2024-04-02 | 2024-10-08 | 广州市东源药业科技有限公司 | Preparation method for forming colloid bundle emulsion by using aloe polysaccharide mediated silicone oil |
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