CN1733235A - Method for processing whole leaf aloe 100:1 spray dried powder used for cosmetic - Google Patents
Method for processing whole leaf aloe 100:1 spray dried powder used for cosmetic Download PDFInfo
- Publication number
- CN1733235A CN1733235A CN 200510096965 CN200510096965A CN1733235A CN 1733235 A CN1733235 A CN 1733235A CN 200510096965 CN200510096965 CN 200510096965 CN 200510096965 A CN200510096965 A CN 200510096965A CN 1733235 A CN1733235 A CN 1733235A
- Authority
- CN
- China
- Prior art keywords
- aloe
- leaf
- spray drying
- whole leaf
- drying powder
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
Landscapes
- Preparation Of Fruits And Vegetables (AREA)
Abstract
The invention provides a process for preparing aloe whole leaf 100:1 spray-dried powder for cosmetics, characterized in that fresh leaf of of curasao aloe is used as the raw material, strict technical requirements, related state and industry laws, regulations, standards are based as the foundation for product quality standard, and optimized product production process and procedures are carried out. The obtained spray-drying powder is fine brown powder having a purity of 100%, the biologically active substance in the aloe can be well preserved with safety and hygiene. The product can meet the quality requirement of aloe whole leaf 100:1 spray-dried powder needed in high-grade aloe cosmetics manufacture.
Description
0: 1 spray drying powder processing method of used for cosmetic whole leaf aloe 10:1 relates to the processing of aloe raw material product, and especially Fresh leaf of aloe being processed into industrialized form can be for the processing method of 0: 1 spray drying powder of whole leaf aloe 10:1 of high-grade Aloe cosmetics manufacturing use.
0: 1 spray drying powder processing method of used for cosmetic whole leaf aloe 10:1 background technology situation: Aloe is the very abundant natural plants of a kind of nutritional labeling, is extensive use of in manufacturing fields such as medicine, food, health product, cosmetics in the world.Especially the polysaccharide that contains in the Aloe, mineral, phytosterin compound, and aloin, Aloe resin B, aminoacid, vitamin etc., have many-side and beautify the usefulness of skin, preserve moisture, aspect such as antiinflammatory, antibacterial, antipruritic, antiallergic, softening skin, anti-acne, antiperspirant deodorant has better action.But the Aloe industry development is later in China, and the processing of Fresh leaf of aloe also is in the starting stage, a little less than the conversion capability from aloe raw material to the aloe raw material product, the quality of converted products is low, and product market competitiveness is poor, and resource does not obtain fully, utilization effectively and reasonably.Therefore, strict establishing criteria adopts scientific method, manage to cut down finished cost, produce quality height, quality is good, specification is complete aloe raw material product, satisfying the various market demand of demand that forms day by day, this is China's difficult problem that will solve in the Aloe industry at present just.
The present invention is to provide 0: 1 spray drying powder processing method of a kind of used for cosmetic whole leaf aloe 10:1, not only Fresh leaf of aloe can be processed into and meet 0: 1 spray drying powder of whole leaf aloe 10:1 that standard is used in the cosmetics manufacturing, and be a kind of industrialization processing method, improved the productivity effect of 0: 1 spray drying powder of whole leaf aloe 10:1 greatly.This development to China's Aloe industry has significance.
0: 1 spray drying powder processing method of used for cosmetic whole leaf aloe 10:1 is: be raw material with the Fresh leaf of aloe, with the organoleptic indicator of aloe raw material converted products, physical and chemical index, sanitary index etc. is quality standard, with the relevant sanitary legislation of country and industry, standard is the target level of product quality foundation, select materials 0: 1 spray drying powder of processing used for cosmetic whole leaf aloe 10:1 → cleaning and sterilization → finishing → making beating → squeezing → fine grinding → filtration → spray drying → this technological process of production of sterilization → packing → finished product according to what experiment was determined.
Adopt such scheme, can obtain 0: 1 spray drying powder product of whole leaf aloe 10:1 of accord with Q B/T2488-2000 standard.This product can use for high-grade Aloe cosmetics manufacturing.
The specific embodiment of 0: 1 spray drying powder processing method of used for cosmetic whole leaf aloe 10:1, do as detailed below:
The production environment condition: 0: 1 spray drying powder of processing used for cosmetic whole leaf aloe 10:1 will be finished in the cleaning sterile workshop of GMP compatible, and the air cleaning rank reaches 100,000 grade standards.This environmental requirement is to propose by aloe raw material product machining experiment up to standard.
Select materials: select for use by the nuisanceless standard plantation and the fresh blade of Aloe vulgaris in growth 2 anniversaries of expiration, rejecting has the scab position; Should be controlled within 8 hours from Aloe plant harvesting blade to factory process.This technological requirement be by mycete grow the experiment determined.The Fresh leaf of aloe sheet that is mechanically damaged when experimental results show that harvesting is under condition more than 15 ℃, and the blade injury position will have mycete to produce after 8 hours.
Cleaning and sterilization: divided for three steps carried out.The first step is put into the XY type recirculated water cleaning machine made from rustless steel with the Fresh leaf of aloe after selecting materials, and washes Fresh leaf of aloe surface silt and dirt off with the clean water that meets drinking water standard.Second step put into the cleaning and sterilizing pond that fills Ozone Water with Fresh leaf of aloe and soaked 5 minutes, to kill each bacterioid and to remove pesticide residues.Ozone Water is to enter in the water of cleaning and sterilizing pond formedly after gas-liquid mixing pump mixes by the certain density ozone that pretreated air admission ozonator produces, and the ozone concentration of its Ozone Water should be controlled at 10-20mg/m
3The 3rd step was put into mobile sterilized water rinsing 3 minutes with Fresh leaf of aloe, with bacteriological protection cross-contamination in the cleaning and sterilization process.This technological requirement is determined by GB/T7918.2-1987 total number of bacteria assay method and experimental result.
Finishing: the Fresh leaf of aloe behind the cleaning and sterilization is repaired, excised bright blade root portion's white portion and blade tip, ream the thorn on leaf margin both sides.
Making beating: the Fresh leaf of aloe after the beater made from rustless steel will repair breaks into Aloe and starches.
Squeezing: with squeezer the Aloe slurry is squeezed the juice, its juice is whole leaf aloe 1:1: 1 natural juice, income rate are the 70-85% of bright leaf.This is the data of gained by experiment.
Fine grinding: adopt colloid mill that Aloe original juice is ground, make the further refinement of Aloe original juice, and reach the homogenizing purpose.
Filter: through the Aloe original juice that fine grinding obtains, also have the thinner fibrous tissue of part granule to be suspended in the juice, along with the prolongation meeting of resting period is slowly sunk, stable unfavorable to product.Therefore, adopt the centrifugal fine filter of ultrahigh speed to remove the thin sticking granule of slow (≤0.2 mm/second) of those sedimentation velocity.
Spray drying: the Aloe solid content after will filtering is that 1% aloe leaf natural juice enters Highspeedcentrifugingandsprayingdrier and carries out spray drying.Highspeedcentrifugingandsprayingdrier adopts the disc type atomizing of high speed centrifugation motion, aloe leaf natural juice is atomized into vaporific drop, when heat exchange is carried out in the hot-air moment contact that enters tower body through special distribution simultaneously, in the extremely short time, evaporate moisture content, form the dried finished product of uniform powdery, i.e. " 0: 1 spray drying powder of whole leaf aloe 10:1 ".For avoiding too high loss of Aloe bioactive substance Yin Wendu, the inlet temperature of Highspeedcentrifugingandsprayingdrier should be controlled at 180 ℃～200 ℃, and outlet temperature should be controlled at 85 ℃.No matter inlet temperature or outlet temperature, it is very short putting and being added in the lip-deep time of Aloe material, so can not make the Aloe bioactive substance that bigger loss is arranged.Spray-dried, obtain 0: 1 spray drying powder of whole leaf aloe 10:1, income rate is about 1%.This is the data of gained by experiment.
Sterilization: 0: 1 spray drying powder of whole leaf aloe 10:1 is sterilized at last with the ultraviolet sterilization method.Under Burdick lamp, 0: 1 spray drying powder of whole leaf aloe 10:1 is placed thickness and should be controlled at 6～8cm, every 2 hours, 0: 1 spray drying powder of whole leaf aloe 10:1 is stirred once.Sterilization time requires to reach 12 hours.This technological requirement is determined by experiment.
Packing: with aseptic aluminide-coating bag vacuum packaging, every bag of 2.5kg is advisable.
Finished product: be " 0: 1 spray drying powder of used for cosmetic whole leaf aloe 10:1 ".
The organoleptic indicator: brown ceramic powder, purity is 100%, has the aloe plant flavor, does not have other abnormal flavour; Be exposed to irradiation 6h under the Burdick lamp, do not change color.This is the index determined of result by experiment.
Physical and chemical index: absorbance (400nm, 1% aqueous solution)≤1.00; PH value is (1% aqueous solution) 3.5-4.7; Moisture (%)≤8.0; Calcium (mg/kg) 4.48 * 10
41.02 * 10
5Magnesium (mg/kg) 3.30 * 10
3～2.30 * 10
4Aloe polysaccharide (mg/kg) 〉=3.00 * 10
4This is the index determined of result by experiment.
Sanitary index: plumbous (mg/L)≤30; Hydrargyrum (mg/L)≤1; Arsenic (mg/L)≤10; Total number of bacteria (individual/mL)≤500; Excrement colibacillus group (every mL), staphylococcus aureus (every mL), bacillus pyocyaneus (every mL) must not detect.Above sanitary index is pressed GB/T7917.3-1987, GB/T7917.1-1987, GB/T7917.2-1987, GB/T7918.2-1987, GB/T7918.3-1987, GB/T7918.5-1987, the determined index of GB/T7918.4-1987 assay respectively.
Claims (3)
1,0: 1 spray drying powder processing method of a kind of used for cosmetic whole leaf aloe 10:1.It is characterized in that: be raw material with the Fresh leaf of aloe, with the organoleptic indicator of aloe raw material converted products, physical and chemical index, sanitary index etc. is quality standard, with the relevant sanitary legislation of country and industry, standard is the target level of product quality foundation, select materials 0: 1 spray drying powder of processing used for cosmetic whole leaf aloe 10:1 → cleaning and sterilization → finishing → making beating → squeezing → fine grinding → filtration → spray drying → this technological process of production of sterilization → packing → finished product according to what experiment was determined.
2,0: 1 spray drying powder processing method of used for cosmetic whole leaf aloe 10:1 according to claim 1, it is characterized in that: the technological process of production and processing method are defined as, select materials: select for use by the nuisanceless standard plantation and the fresh blade of Aloe vulgaris in growth 2 anniversaries of expiration, rejecting has the scab position; Should be controlled within 8 hours from Aloe plant harvesting blade to factory process.Cleaning and sterilization: divided for three steps carried out.The first step is put into the XY type recirculated water cleaning machine made from rustless steel with the Fresh leaf of aloe after selecting materials, and washes Fresh leaf of aloe surface silt and dirt off with the clean water that meets drinking water standard.Second step put into the cleaning and sterilizing pond that fills Ozone Water with Fresh leaf of aloe and soaked 5 minutes, to kill each bacterioid and to remove pesticide residues.The 3rd step was put into mobile sterilized water rinsing 3 minutes with Fresh leaf of aloe, with bacteriological protection cross-contamination in the cleaning and sterilization process.Finishing: the Fresh leaf of aloe behind the cleaning and sterilization is repaired, excised bright blade root portion's white portion and blade tip, ream the thorn on leaf margin both sides.Making beating: the Fresh leaf of aloe after the beater made from rustless steel will repair breaks into Aloe and starches.Squeezing: with squeezer the Aloe slurry is squeezed the juice, its juice is whole leaf aloe 1:1: 1 natural juice, income rate are the 70-85% of bright leaf.This is the data of gained by experiment.Fine grinding: adopt colloid mill that Aloe original juice is ground, make the further refinement of Aloe original juice, and reach the homogenizing purpose.Filter: through the Aloe original juice that fine grinding obtains, also have the thinner fibrous tissue of part granule to be suspended in the juice, along with the prolongation meeting of resting period is slowly sunk, stable unfavorable to product.Therefore, adopt the centrifugal fine filter of ultrahigh speed to remove the thin sticking granule of slow (≤0.2 mm/second) of those sedimentation velocity.Spray drying: the Aloe solid content after will filtering is that 1% aloe leaf natural juice enters Highspeedcentrifugingandsprayingdrier and carries out spray drying.The inlet temperature of Highspeedcentrifugingandsprayingdrier should be controlled at 180 ℃～200 ℃, and outlet temperature should be controlled at 85 ℃.Spray-dried, obtain 0: 1 spray drying powder of whole leaf aloe 10:1, income rate is about 1%.Sterilization: 0: 1 spray drying powder of whole leaf aloe 10:1 is sterilized at last with the ultraviolet sterilization method.Under Burdick lamp, 0: 1 spray drying powder of whole leaf aloe 10:1 is placed thickness and should be controlled at 6～8cm, every 2 hours, 0: 1 spray drying powder of whole leaf aloe 10:1 is stirred once.Sterilization time requires to reach 12 hours.Packing: with aseptic aluminide-coating bag vacuum packaging, every bag of 2.5kg is advisable.Finished product: be " 0: 1 spray drying powder of used for cosmetic whole leaf aloe 10:1 ".
3,0: 1 spray drying powder processing method of used for cosmetic whole leaf aloe 10:1 according to claim 1 is characterized in that: the organoleptic indicator who determines is, brown ceramic powder, and purity is 100%, has the aloe plant flavor; Be exposed to irradiation 6h under the Burdick lamp, do not change color.The physical and chemical index of determining is absorbance (400nm, 1% aqueous solution)≤1.00; PH value is (1% aqueous solution) 3.5-4.7; Moisture (%)≤8.0; Calcium (mg/kg) 4.48 * 10
4～1.02 * 10
5Magnesium (mg/kg) 3.30 * 10
3～2.30 * 10
4Aloe polysaccharide (mg/kg) 〉=3.00 * 10
4The sanitary index of determining is plumbous (mg/L)≤30; Hydrargyrum (mg/L)≤1; Arsenic (mg/L)≤10; Total number of bacteria (individual/mL)≤500; Excrement colibacillus group (every mL), staphylococcus aureus (every mL), bacillus pyocyaneus (every mL) must not detect.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200510096965 CN1733235A (en) | 2005-08-26 | 2005-08-26 | Method for processing whole leaf aloe 100:1 spray dried powder used for cosmetic |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 200510096965 CN1733235A (en) | 2005-08-26 | 2005-08-26 | Method for processing whole leaf aloe 100:1 spray dried powder used for cosmetic |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1733235A true CN1733235A (en) | 2006-02-15 |
Family
ID=36075990
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 200510096965 Pending CN1733235A (en) | 2005-08-26 | 2005-08-26 | Method for processing whole leaf aloe 100:1 spray dried powder used for cosmetic |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1733235A (en) |
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104693315A (en) * | 2015-03-16 | 2015-06-10 | 云南万绿生物股份有限公司 | Processing method for 1000: 1 aloe gel dry powder |
-
2005
- 2005-08-26 CN CN 200510096965 patent/CN1733235A/en active Pending
Cited By (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104693315A (en) * | 2015-03-16 | 2015-06-10 | 云南万绿生物股份有限公司 | Processing method for 1000: 1 aloe gel dry powder |
Similar Documents
| Publication | Publication Date | Title |
|---|---|---|
| CN1733235A (en) | Method for processing whole leaf aloe 100:1 spray dried powder used for cosmetic | |
| CN1739723A (en) | Production process of decolorized aloe leaf powder for cosmetics | |
| CN1733238A (en) | Method for processing decoloured whole leaf aloe 100:1 spray dried powder used for cosmetic | |
| CN1733241A (en) | Method for processing aloe gel 200:1 spray dried powder used for cosmetic | |
| CN1733210A (en) | Method for processing whole leaf aloe 1:1 raw juice used for cosmetic | |
| CN1733236A (en) | Method for processing aloe gel 100:1 spray dried powder used for cosmetic | |
| CN1676034A (en) | Method for producing full-leaf aloe 100:1 spray drying powder reaching food-level stardard | |
| CN1733232A (en) | Method for processing whole leaf aloe 100:1 freeze dried powder used for cosmetic | |
| CN1733219A (en) | Method for processing aloe gel 1:1 raw juice used for cosmetic | |
| CN1733239A (en) | Method for processing decoloured aloe gel 200:1 spray dried powder used for cosmetic | |
| CN1739725A (en) | Production process of aloe gel concentrated powder for cosmetics | |
| CN1733211A (en) | Method for processing whole leaf aloe 40:1 raw juice used for cosmetic | |
| CN1733233A (en) | Method for processing decoloured aloe gel 100:1 spray dried powder used for cosmetic | |
| CN1733229A (en) | Method for processing aloe gel 20:1 concentrated juice used for cosmetic | |
| CN1739722A (en) | Production process of aloe leaf powder for cosmetics | |
| CN1733230A (en) | Method for processing decoloured aloe gel 200:1 freeze dried powder used for cosmetic | |
| CN1733158A (en) | Method for processing decolored whole leaf aloe 1:1 raw juice used for cosmetic | |
| CN1733234A (en) | Method for processing aloe gel 200:1 freeze dried powder used for cosmetic | |
| CN1733240A (en) | Method for processing decoloured whole leaf aloe 100:1 freeze dried powder used for cosmetic | |
| CN1733212A (en) | Method for processing whole leaf aloe 10:1 raw juice used for cosmetic | |
| CN1733213A (en) | Method for processing decolored whole leaf aloe 10:1 condensed juice used for cosmetic | |
| CN1733217A (en) | Method for processing decolored whole leaf aloe 40:1 condensed juice used for cosmetic | |
| CN1733214A (en) | Method for processing decolored whole leaf aloe 20:1 condensed juice used for cosmetic | |
| CN1733159A (en) | Method for processing whole leaf aloe 20:1 raw juice used for cosmetic | |
| CN1733226A (en) | Method for processing decoloured aloe gel 1:1 raw juice used for cosmetic |
Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |