CN1733221A - Method for processing decolored aloe gel 20:1 concentrated solution used for cosmetic - Google Patents

Abstract

The invention provides a process for preparing decolored aloe gelatin 20:1 concentrated liquid for cosmetics, characterized in that fresh leaf mesophyll (gelatin) of curasao aloe is used as the raw material, strict technical requirements, related state and industry laws, regulations, standards are based as the foundation for product quality standard, and optimized product production process and procedures are carried out. The concentrated liquid is a yellow and brown liquid with a micro amount of precipitation, the biologically active substance in the aloe can be well preserved with safety and hygiene. The product can meet the quality requirement of decolored aloe gelatin 20:1 concentrated liquid needed in high-grade aloe cosmetics manufacture.

Description

Used for cosmetic decolored aloe gel 20:1: 1 concentrated solution processing method

The used for cosmetic decolored aloe gel 20:1: 1 concentrated solution processing method relates to aloe raw material product processing, and especially Fresh mesophyll of aloe (gel) being processed into industrialized form can be for the decolored aloe gel 20:1 of high-grade Aloe cosmetics manufacturing use: the processing method of 1 concentrated solution.

The used for cosmetic decolored aloe gel 20:1: 1 concentrated solution processing method background technology situation: Aloe is the very abundant natural plants of a kind of nutritional labeling, is extensive use of in manufacturing fields such as medicine, food, health product, cosmetics in the world.The particularly polysaccharide that contains in the Aloe, mineral, phytosterin compound, and aloin, Aloe resin B, aminoacid, vitamin etc., have many-side and beautify the usefulness of skin, preserve moisture, aspect such as antiinflammatory, antibacterial, antipruritic, antiallergic, softening skin, anti-acne, antiperspirant deodorant has better action.The processing of China's Fresh leaf of aloe is in the starting stage, and a little less than the conversion capability from aloe raw material to the aloe raw material product, the quality of converted products is low, and product market competitiveness is not strong, and resource does not obtain fully, utilization effectively and reasonably.Therefore, strict " the used for cosmetic aloe products " formulated according to country be standard (QB/T2488-2000), adopt scientific method, manage to cut down finished cost, produce quality height, the measured aloe raw material product of matter, satisfying the market demand that forms day by day, this is China's difficult problem that will solve in the Aloe industry at present just.

The present invention is to provide a kind of used for cosmetic decolored aloe gel 20:1: 1 concentrated solution processing method, not only Fresh mesophyll of aloe (gel) can be processed into and meet the decolored aloe gel 20:1 that standard is used in the cosmetics manufacturing: 1 concentrated solution, and be a kind of industrialized preparing process, improved decolored aloe gel 20:1 greatly: the productivity effect of 1 concentrated solution, this development to China's Aloe industry has significance.

The used for cosmetic decolored aloe gel 20:1: 1 concentrated solution processing method is: with Fresh mesophyll of aloe (gel) is raw material, with the organoleptic indicator of used for cosmetic aloe products, physical and chemical index, sanitary index etc. is quality standard, with country and industry relevant criterion and sanitary legislation is the target level of product quality foundation, select materials processing used for cosmetic decolored aloe gel 20:1: 1 concentrated solution → cleaning and sterilization → peeling → making beating → squeezing → fine grinding → filtration → decolouring → secondary filter → this processing process of membrance concentration → sterilization → packing → finished product according to what experiment was determined.

Adopt such scheme, can be met " used for cosmetic aloe products " (QB/T2488-2000) decolored aloe gel 20:1 of standard: 1 concentrated solution product.This product can use for making high-grade Aloe cosmetics.

The used for cosmetic decolored aloe gel 20:1: the specific embodiment of 1 concentrated solution processing method, do as detailed below:

The processing environment condition: processing used for cosmetic decolored aloe gel 20:1: 1 concentrated solution will be finished in the cleaning sterile workshop of GMP compatible, and the air cleaning rank satisfies 100,000 grade standards.This environmental requirement is that the machining experiment by aloe raw material product up to standard proposes.

Select materials: select for use by the nuisanceless standard plantation and the fresh blade of Aloe vulgaris at growth 18 monthly ages of expiration, rejecting has the scab position; The freshness requirement should be controlled within 8 hours from Aloe plant harvesting blade to factory process.This technological requirement be by mycete grow the experiment determined.The fresh blade of Aloe that is mechanically damaged when experimental results show that harvesting is under condition more than 15 ℃, and the blade injury position will have mycete to produce after 8 hours.

Cleaning and sterilization: divided for three steps carried out.The first step is put into the XY type recirculated water cleaning machine made from rustless steel with the Fresh leaf of aloe after selecting materials, and washes Fresh leaf of aloe surface silt and dirt off with meeting " drinking water sanitary standard " clean water (GB5749).Second step put into the cleaning and sterilizing pond that fills Ozone Water with Fresh leaf of aloe and soaked 5 minutes, and Fresh leaf of aloe is sterilized and removes pesticide residues and handle.Ozone Water is to enter in the water of cleaning and sterilizing pond formedly after gas-liquid mixing pump mixes by the certain density ozone that pretreated air admission ozonator produces, and the ozone concentration of its Ozone Water should be controlled at 10-20mg/m ³The 3rd step was put into mobile sterilized water rinsing 3 minutes with Fresh leaf of aloe, with bacteriological protection cross-contamination in the cleaning and sterilization process.This technological requirement is determined by GB/T7918.2-1987 total number of bacteria assay method and experimental result.

Peeling: the Fresh leaf of aloe of the Aloe peeling machine made from rustless steel after with cleaning and sterilization carries out peeling to be handled, and the meat (gel) of bright leaf is separated with skin, and it is standby to get Aloe mesophyll (gel).

Making beating: the Aloe beater made from rustless steel breaks into aloe juice with Aloe mesophyll (gel).

Squeezing: with squeezer aloe juice is squeezed the juice, its juice is aloe gel 1:1: 1 stock solution.It is dried more good more to squeeze the juice, with the no longer excessive degree of being of juice.

Fine grinding: adopt colloid mill that aloe stoste is ground, make the further refinement of aloe stoste, and reach the homogenizing purpose.

Filter: through the aloe stoste that fine grinding obtains, also have the thinner fibrous tissue of part granule to be suspended in the juice, along with the prolongation meeting of resting period is slowly sunk, stable unfavorable to product.Therefore, adopt the centrifugal fine filter of ultrahigh speed to remove the thin sticking granule of slow (≤0.2 mm/second) of those sedimentation velocity.

Decolouring: the aloe gel 1:1 that obtains after filtering: the 1 stock solution processing of decolouring.Aloe gel 1:1: adsorption decoloring method is adopted in the decolouring of 1 stock solution, and adsorbent uses the fine powder active carbon.Fine powder active carbon addition is an aloe gel 1:1: 1.5% of 1 stock solution weight.During operation, with the aloe gel 20:1 that adds behind the fine powder active carbon: 1 concentrated solution, make its temperature bring up to 48 ℃～50 ℃, the time kept 20 minutes, was cooled to room temperature then.This technological requirement is determined according to experimental result.

Secondary filter: will be through the aloe gel 1:1 after decolouring is handled: 1 stock solution adopts the deckle board filter press to remove the activated carbon adsorption thing, and aloe gel 1:1: remaining colloid, fiber and impurity etc. in 1 stock solution.

Membrance concentration: the decolored aloe gelin proportion collagen solution behind the secondary filter is entered membrane separation concentrated compression apparatus carry out membrance concentration.The membrance concentration biggest advantage is to realize that normal temperature condition concentrates down, avoids in the course of processing Yin Wendu too high and the Aloe bioactive ingredients is run off, and has kept the color and luster and the local flavor of product, has guaranteed the quality of product.Membrance separation is to utilize the macromolecule semipermeable membrane, with the pressure differential of film both sides, when impelling some molecule in the fluid to see through semipermeable membrane and be retained down, to obtain a kind of isolation technics of some composition in the fluid.When by semipermeable membrane be solvent, then solution has obtained to concentrate, this process is exactly a membrance concentration.Decolored aloe gelin proportion collagen solution membrance concentration should adopt the reverse osmosis isolation method, and osmotic pressure should be controlled at 5.0～8.0MPa.This technological requirement is determined by decolored aloe gelin proportion collagen solution membrance concentration experimental result.Through membrance concentration, when the volume of concentrated solution reach decolored aloe gel stock solution volume 1/20th the time, the concentrated solution of this moment is decolored aloe gel 20:1: 1 concentrated solution.

Sterilization: decolored aloe gel 20:1: the sterilization of 1 concentrated solution is to guarantee the constant important step of Aloe stable components.Sterilizing methods adopts pasteurization, and sterilising temp is controlled at 70 ℃, and sterilization time is 20min.This technological requirement is to pass through decolored aloe gel 20:1: 1 concentrated solution sterilization experiment is determined.

Packing: with the vacuum packaging of 10Kg Aluminum-plastic composite bag.

Finished product: be " used for cosmetic decolored aloe gel 20:1: 1 concentrated solution ".

Organoleptic indicator: the yellowish-brown thick liquid of microprecipitation is arranged, have the aloe plant flavor, do not have other abnormal flavour; Be exposed to irradiation 6h under the Burdick lamp, do not change color.This is the index determined of result by experiment.

Physical and chemical index: absorbance (400nm, 5% aqueous solution)≤0.10; PH value is (5% aqueous solution) 3.5-4.7; Relative density is 1.004～1.028; Total solid 〉=9.2%; Calcium (mg/L) 1.96 * 10 ³～8.96 * 10 ³Magnesium (mg/L) 4.68 * 10 ²～2.36 * 10 ³Aloe polysaccharide (mg/L) 〉=1.20 * 10 ⁴This is the index determined of result by experiment.

Sanitary index: plumbous (mg/L)≤30; Hydrargyrum (mg/L)≤1; Arsenic (mg/L)≤10; Total number of bacteria (individual/mL)≤500; Excrement colibacillus group (every mL), staphylococcus aureus (every mL), bacillus pyocyaneus not (every mL) must not detect.Above sanitary index is pressed GB/T7917.3-1987, GB/T7917.1-1987, GB/T7917.2-1987, GB/T7918.2-1987, GB/T7918.3-1987, GB/T7918.5-1987, the determined index of GB/T7918.4-1987 assay respectively.

Claims (3)

1, a kind of used for cosmetic decolored aloe gel 20:1: 1 concentrated solution processing method.It is characterized in that: with Fresh mesophyll of aloe (gel) is raw material, with the organoleptic indicator of used for cosmetic aloe products, physical and chemical index, sanitary index etc. is quality standard, with country and industry relevant criterion and sanitary legislation is the target level of product quality foundation, select materials processing used for cosmetic decolored aloe gel 20:1: 1 concentrated solution → cleaning and sterilization → peeling → making beating → squeezing → fine grinding → filtration → decolouring → secondary filter → this processing process of membrance concentration → sterilization → packing → finished product according to what experiment was determined.

2, used for cosmetic decolored aloe gel 20:1 according to claim 1: 1 concentrated solution processing method, it is characterized in that: processing process and processing method are defined as, select materials: select for use by the nuisanceless standard plantation and the fresh blade of Aloe vulgaris at growth 18 monthly ages of expiration, rejecting has the scab position; The freshness requirement should be controlled within 8 hours from Aloe plant harvesting blade to factory process.Cleaning and sterilization: divided for three steps carried out.The first step is put into the XY type recirculated water cleaning machine made from rustless steel with the Fresh leaf of aloe after selecting materials, and washes Fresh leaf of aloe surface silt and dirt off with meeting " drinking water sanitary standard " clean water (GB5749).Second step put into the cleaning and sterilizing pond that fills Ozone Water with Fresh leaf of aloe and soaked 5 minutes, and Fresh leaf of aloe is sterilized and removes pesticide residues and handle.Ozone concentration is controlled at 10-20mg/m ³The 3rd step was put into mobile sterilized water rinsing 3 minutes with Fresh leaf of aloe, with bacteriological protection cross-contamination in the cleaning and sterilization process.Peeling: the Fresh leaf of aloe of the Aloe peeling machine made from rustless steel after with cleaning and sterilization carries out peeling to be handled, and the meat (gel) of bright leaf is separated with skin, and it is standby to get Aloe mesophyll (gel).Making beating: the Aloe beater made from rustless steel breaks into aloe juice with Aloe mesophyll (gel).Squeezing: with squeezer aloe juice is squeezed the juice, its juice is aloe gel 1:1: 1 stock solution.Fine grinding: adopt colloid mill that aloe stoste is ground, make the further refinement of aloe stoste, and reach the homogenizing purpose.Filter: adopt the centrifugal fine filter of ultrahigh speed to remove the thin sticking granule of slow (≤0.2 mm/second) of those sedimentation velocity.Decolouring: the aloe gel 1:1 that obtains after filtering: the 1 stock solution processing of decolouring.Aloe gel 1:1: adsorption decoloring method is adopted in the decolouring of 1 stock solution, and adsorbent uses the fine powder active carbon.Fine powder active carbon addition is an aloe gel 1:1: 1.5% of 1 stock solution weight.During operation, with the aloe gel 1:1 that adds behind the fine powder active carbon: 1 stock solution, make its temperature bring up to 48 ℃～50 ℃, the time kept 20 minutes, was cooled to room temperature then.Secondary filter: will be through the aloe gel 1:1 after decolouring is handled: 1 stock solution adopts the deckle board filter press to remove the activated carbon adsorption thing, and aloe gel 1:1: remaining colloid, fiber and impurity etc. in 1 stock solution.Membrance concentration: the decolored aloe gelin proportion collagen solution behind the secondary filter is entered membrane separation concentrated compression apparatus carry out membrance concentration.Decolored aloe gelin proportion collagen solution membrance concentration adopts the reverse osmosis isolation method, and osmotic pressure should be controlled at 5.0～8.0MPa.Through membrance concentration, when the volume of concentrated solution reach decolored aloe gel stock solution volume 1/20th the time, the concentrated solution of this moment is decolored aloe gel 20:1: 1 concentrated solution.Sterilization: method adopts pasteurization, and sterilising temp is controlled at 70 ℃, and sterilization time is 20min.Packing: with the vacuum packaging of 10Kg Aluminum-plastic composite bag.Finished product: be " used for cosmetic decolored aloe gel 20:1: 1 concentrated solution ".

3, used for cosmetic decolored aloe gel 20:1 according to claim 1: 1 concentrated solution processing method is characterized in that: the organoleptic indicator who determines is, the yellowish-brown thick liquid of microprecipitation is arranged, and has the aloe plant flavor; Be exposed to irradiation 6h under the Burdick lamp, do not change color.The physical and chemical index of determining is absorbance (400nm, 5% aqueous solution)≤0.10; PH value is (5% aqueous solution) 3.5-4.7; Relative density is 1.004～1.028; Total solid 〉=9.2%; Calcium (mg/L) 1.96 * 10 ³～8.96 * 10 ³Magnesium (mg/L) 4.68 * 10 ²～2.36 * 10 ³Aloe polysaccharide (mg/L) 〉=1.20 * 10 ⁴The sanitary index of determining is plumbous (mg/L)≤30; Hydrargyrum (mg/L)≤1; Arsenic (mg/L)≤10; Total number of bacteria (individual/mL)≤500; Excrement colibacillus group (every mL), staphylococcus aureus (every mL), bacillus pyocyaneus not (every mL) must not detect.