CN1729777A - Imidacloprid-containing liquid formulation for trunk injection of trees - Google Patents
Imidacloprid-containing liquid formulation for trunk injection of trees Download PDFInfo
- Publication number
- CN1729777A CN1729777A CN 200510043092 CN200510043092A CN1729777A CN 1729777 A CN1729777 A CN 1729777A CN 200510043092 CN200510043092 CN 200510043092 CN 200510043092 A CN200510043092 A CN 200510043092A CN 1729777 A CN1729777 A CN 1729777A
- Authority
- CN
- China
- Prior art keywords
- imidacloprid
- injection
- trunk
- liquid formulation
- trunk injection
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000007924 injection Substances 0.000 title claims abstract description 272
- 238000002347 injection Methods 0.000 title claims abstract description 272
- 239000005906 Imidacloprid Substances 0.000 title claims abstract description 161
- YWTYJOPNNQFBPC-UHFFFAOYSA-N imidacloprid Chemical compound [O-][N+](=O)\N=C1/NCCN1CC1=CC=C(Cl)N=C1 YWTYJOPNNQFBPC-UHFFFAOYSA-N 0.000 title claims abstract description 161
- 229940056881 imidacloprid Drugs 0.000 title claims abstract description 161
- 239000012669 liquid formulation Substances 0.000 title abstract description 154
- 239000000575 pesticide Substances 0.000 claims abstract description 30
- 239000002904 solvent Substances 0.000 claims abstract description 8
- 239000002994 raw material Substances 0.000 claims abstract description 6
- 239000004094 surface-active agent Substances 0.000 claims abstract description 5
- OEBRKCOSUFCWJD-UHFFFAOYSA-N dichlorvos Chemical compound COP(=O)(OC)OC=C(Cl)Cl OEBRKCOSUFCWJD-UHFFFAOYSA-N 0.000 claims description 53
- IAZDPXIOMUYVGZ-UHFFFAOYSA-N Dimethylsulphoxide Chemical compound CS(C)=O IAZDPXIOMUYVGZ-UHFFFAOYSA-N 0.000 claims description 40
- 229960002715 nicotine Drugs 0.000 claims description 33
- SNICXCGAKADSCV-UHFFFAOYSA-N nicotine Natural products CN1CCCC1C1=CC=CN=C1 SNICXCGAKADSCV-UHFFFAOYSA-N 0.000 claims description 33
- SNICXCGAKADSCV-JTQLQIEISA-N (-)-Nicotine Chemical compound CN1CCC[C@H]1C1=CC=CN=C1 SNICXCGAKADSCV-JTQLQIEISA-N 0.000 claims description 32
- 239000005875 Acetamiprid Substances 0.000 claims description 27
- ZMXDDKWLCZADIW-UHFFFAOYSA-N N,N-Dimethylformamide Chemical compound CN(C)C=O ZMXDDKWLCZADIW-UHFFFAOYSA-N 0.000 claims description 27
- WCXDHFDTOYPNIE-RIYZIHGNSA-N (E)-acetamiprid Chemical compound N#C/N=C(\C)N(C)CC1=CC=C(Cl)N=C1 WCXDHFDTOYPNIE-RIYZIHGNSA-N 0.000 claims description 26
- JYQUHIFYBATCCY-UHFFFAOYSA-N quinalphos Chemical compound C1=CC=CC2=NC(OP(=S)(OCC)OCC)=CN=C21 JYQUHIFYBATCCY-UHFFFAOYSA-N 0.000 claims description 19
- 239000001089 [(2R)-oxolan-2-yl]methanol Substances 0.000 claims description 15
- BSYVTEYKTMYBMK-UHFFFAOYSA-N tetrahydrofurfuryl alcohol Chemical compound OCC1CCCO1 BSYVTEYKTMYBMK-UHFFFAOYSA-N 0.000 claims description 15
- 239000000463 material Substances 0.000 claims description 11
- 239000000203 mixture Substances 0.000 claims description 11
- CGQCWMIAEPEHNQ-UHFFFAOYSA-N Vanillylmandelic acid Chemical compound COC1=CC(C(O)C(O)=O)=CC=C1O CGQCWMIAEPEHNQ-UHFFFAOYSA-N 0.000 claims description 5
- 241000238631 Hexapoda Species 0.000 abstract description 35
- 230000000694 effects Effects 0.000 abstract description 33
- 241000607479 Yersinia pestis Species 0.000 abstract description 13
- 230000009471 action Effects 0.000 abstract description 4
- 230000008859 change Effects 0.000 abstract description 3
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 3
- 238000001035 drying Methods 0.000 abstract 1
- 235000013399 edible fruits Nutrition 0.000 abstract 1
- 239000002917 insecticide Substances 0.000 abstract 1
- 230000001681 protective effect Effects 0.000 abstract 1
- 239000003814 drug Substances 0.000 description 87
- 230000003449 preventive effect Effects 0.000 description 64
- 238000000034 method Methods 0.000 description 41
- BWAADSAOZKHIQQ-UHFFFAOYSA-N [O].O=P(OC)(OC=C(Cl)Cl)OC Chemical compound [O].O=P(OC)(OC=C(Cl)Cl)OC BWAADSAOZKHIQQ-UHFFFAOYSA-N 0.000 description 33
- 241000124033 Salix Species 0.000 description 28
- 238000012360 testing method Methods 0.000 description 23
- 238000005516 engineering process Methods 0.000 description 22
- 230000002265 prevention Effects 0.000 description 21
- 244000046101 Sophora japonica Species 0.000 description 17
- 235000010586 Sophora japonica Nutrition 0.000 description 17
- 239000002023 wood Substances 0.000 description 16
- 238000011160 research Methods 0.000 description 15
- 241000162439 Brontispa longissima Species 0.000 description 14
- 241001124076 Aphididae Species 0.000 description 13
- 241001481710 Cerambycidae Species 0.000 description 13
- 230000000857 drug effect Effects 0.000 description 12
- 230000005484 gravity Effects 0.000 description 11
- 239000000843 powder Substances 0.000 description 11
- 238000011835 investigation Methods 0.000 description 10
- 241001520019 Holotrichia oblita Species 0.000 description 9
- 238000004519 manufacturing process Methods 0.000 description 9
- 238000004080 punching Methods 0.000 description 9
- 241001498622 Cixius wagneri Species 0.000 description 8
- 231100000572 poisoning Toxicity 0.000 description 8
- 230000000607 poisoning effect Effects 0.000 description 8
- 238000003756 stirring Methods 0.000 description 8
- 244000103926 Chamaenerion angustifolium Species 0.000 description 7
- 235000008302 Chamaenerion angustifolium Nutrition 0.000 description 7
- 241000320508 Pentatomidae Species 0.000 description 7
- 230000002045 lasting effect Effects 0.000 description 7
- 238000002360 preparation method Methods 0.000 description 7
- 241000196324 Embryophyta Species 0.000 description 6
- 238000004458 analytical method Methods 0.000 description 6
- 239000003153 chemical reaction reagent Substances 0.000 description 6
- 239000007788 liquid Substances 0.000 description 6
- 238000005303 weighing Methods 0.000 description 6
- 235000014443 Pyrus communis Nutrition 0.000 description 5
- 239000003905 agrochemical Substances 0.000 description 5
- -1 desinsection list Chemical compound 0.000 description 5
- 238000007689 inspection Methods 0.000 description 5
- 239000002574 poison Substances 0.000 description 5
- 231100000614 poison Toxicity 0.000 description 5
- 230000008569 process Effects 0.000 description 5
- 238000010998 test method Methods 0.000 description 5
- DUIOKRXOKLLURE-UHFFFAOYSA-N 2-octylphenol Chemical compound CCCCCCCCC1=CC=CC=C1O DUIOKRXOKLLURE-UHFFFAOYSA-N 0.000 description 4
- NNBFNNNWANBMTI-UHFFFAOYSA-M brilliant green Chemical group OS([O-])(=O)=O.C1=CC(N(CC)CC)=CC=C1C(C=1C=CC=CC=1)=C1C=CC(=[N+](CC)CC)C=C1 NNBFNNNWANBMTI-UHFFFAOYSA-M 0.000 description 4
- 230000013872 defecation Effects 0.000 description 4
- 238000011161 development Methods 0.000 description 4
- 230000005611 electricity Effects 0.000 description 4
- 239000003550 marker Substances 0.000 description 4
- 239000003973 paint Substances 0.000 description 4
- 239000000047 product Substances 0.000 description 4
- 239000000126 substance Substances 0.000 description 4
- 230000009286 beneficial effect Effects 0.000 description 3
- 201000010099 disease Diseases 0.000 description 3
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 3
- LQZZUXJYWNFBMV-UHFFFAOYSA-N dodecan-1-ol Chemical class CCCCCCCCCCCCO LQZZUXJYWNFBMV-UHFFFAOYSA-N 0.000 description 3
- 238000003912 environmental pollution Methods 0.000 description 3
- 238000009472 formulation Methods 0.000 description 3
- CSCPPACGZOOCGX-UHFFFAOYSA-N Acetone Chemical compound CC(C)=O CSCPPACGZOOCGX-UHFFFAOYSA-N 0.000 description 2
- 241001093951 Ailanthus altissima Species 0.000 description 2
- 241000167854 Bourreria succulenta Species 0.000 description 2
- 235000013162 Cocos nucifera Nutrition 0.000 description 2
- 244000060011 Cocos nucifera Species 0.000 description 2
- 241001582888 Lobus Species 0.000 description 2
- 235000006541 Opuntia tomentosa Nutrition 0.000 description 2
- 240000005187 Opuntia tomentosa Species 0.000 description 2
- 241000209140 Triticum Species 0.000 description 2
- 235000021307 Triticum Nutrition 0.000 description 2
- 238000001266 bandaging Methods 0.000 description 2
- 230000008901 benefit Effects 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 235000019693 cherries Nutrition 0.000 description 2
- 239000011248 coating agent Substances 0.000 description 2
- 238000000576 coating method Methods 0.000 description 2
- 239000010779 crude oil Substances 0.000 description 2
- 238000003306 harvesting Methods 0.000 description 2
- 238000005259 measurement Methods 0.000 description 2
- 238000005065 mining Methods 0.000 description 2
- 230000000361 pesticidal effect Effects 0.000 description 2
- 238000005096 rolling process Methods 0.000 description 2
- 239000004576 sand Substances 0.000 description 2
- 241000894007 species Species 0.000 description 2
- 239000007921 spray Substances 0.000 description 2
- 230000009885 systemic effect Effects 0.000 description 2
- 230000005068 transpiration Effects 0.000 description 2
- 241001609695 Anoplophora glabripennis Species 0.000 description 1
- 241000273313 Aphis farinosa Species 0.000 description 1
- 235000017166 Bambusa arundinacea Nutrition 0.000 description 1
- 235000017491 Bambusa tulda Nutrition 0.000 description 1
- 239000005946 Cypermethrin Substances 0.000 description 1
- 241001465754 Metazoa Species 0.000 description 1
- 235000014643 Orbignya martiana Nutrition 0.000 description 1
- 244000021150 Orbignya martiana Species 0.000 description 1
- 235000015334 Phyllostachys viridis Nutrition 0.000 description 1
- 244000082204 Phyllostachys viridis Species 0.000 description 1
- 244000141698 Prunus lannesiana Species 0.000 description 1
- 235000014001 Prunus serrulata Nutrition 0.000 description 1
- 244000020191 Salix babylonica Species 0.000 description 1
- 241000254062 Scarabaeidae Species 0.000 description 1
- 238000010521 absorption reaction Methods 0.000 description 1
- 239000002671 adjuvant Substances 0.000 description 1
- QGLZXHRNAYXIBU-WEVVVXLNSA-N aldicarb Chemical compound CNC(=O)O\N=C\C(C)(C)SC QGLZXHRNAYXIBU-WEVVVXLNSA-N 0.000 description 1
- 239000011425 bamboo Substances 0.000 description 1
- DUEPRVBVGDRKAG-UHFFFAOYSA-N carbofuran Chemical compound CNC(=O)OC1=CC=CC2=C1OC(C)(C)C2 DUEPRVBVGDRKAG-UHFFFAOYSA-N 0.000 description 1
- 238000013329 compounding Methods 0.000 description 1
- 238000005520 cutting process Methods 0.000 description 1
- KAATUXNTWXVJKI-UHFFFAOYSA-N cypermethrin Chemical compound CC1(C)C(C=C(Cl)Cl)C1C(=O)OC(C#N)C1=CC=CC(OC=2C=CC=CC=2)=C1 KAATUXNTWXVJKI-UHFFFAOYSA-N 0.000 description 1
- 229960005424 cypermethrin Drugs 0.000 description 1
- 238000009792 diffusion process Methods 0.000 description 1
- MCWXGJITAZMZEV-UHFFFAOYSA-N dimethoate Chemical compound CNC(=O)CSP(=S)(OC)OC MCWXGJITAZMZEV-UHFFFAOYSA-N 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000008030 elimination Effects 0.000 description 1
- 238000003379 elimination reaction Methods 0.000 description 1
- 238000002474 experimental method Methods 0.000 description 1
- 210000003608 fece Anatomy 0.000 description 1
- 230000005669 field effect Effects 0.000 description 1
- 239000012467 final product Substances 0.000 description 1
- 238000004401 flow injection analysis Methods 0.000 description 1
- 239000012530 fluid Substances 0.000 description 1
- 235000013305 food Nutrition 0.000 description 1
- 239000004615 ingredient Substances 0.000 description 1
- 238000003780 insertion Methods 0.000 description 1
- 230000037431 insertion Effects 0.000 description 1
- 239000004922 lacquer Substances 0.000 description 1
- 230000001418 larval effect Effects 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 239000003921 oil Substances 0.000 description 1
- PZXOQEXFMJCDPG-UHFFFAOYSA-N omethoate Chemical compound CNC(=O)CSP(=O)(OC)OC PZXOQEXFMJCDPG-UHFFFAOYSA-N 0.000 description 1
- 230000037361 pathway Effects 0.000 description 1
- 230000000737 periodic effect Effects 0.000 description 1
- 239000008194 pharmaceutical composition Substances 0.000 description 1
- MBNMHBAJUNHZRE-UHFFFAOYSA-M thiosultap monosodium Chemical compound [Na+].OS(=O)(=O)SCC(N(C)C)CSS([O-])(=O)=O MBNMHBAJUNHZRE-UHFFFAOYSA-M 0.000 description 1
- 230000001018 virulence Effects 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
- Catching Or Destruction (AREA)
Abstract
Description
Prevent and treat method | Operating time (minute/strain) | Operating efficiency (strain/man day) | The injection apparatus | Injection power | Cost | Technical characterstic | |
Form | Be worth (unit/strain) | ||||||
The high-pressure injection method | 10~15 | 25~30 | Filling machine | Electric machinery power manpower | Filling machine medicament power manpower | 1.2 ~ 1.4 | Preventive effect is better, and the roundheaded borer drug effect between 75~85%, but is needed 3~5 professional and technical personnel's compounding practices. Special-purpose medicine injection machine needs power, stops and amass greatly, is difficult to carry, and operation is subject to the geographical environment impact. (there is considerable influence in aperture 0.8~1.0cm) to the timber economic worth to need setting the hole that vertically make a call to dark approximately a 5~8cm on the body during dispenser. Filling machine price more expensive (600~1500 yuan) is restricted promoted extension. The medicine device separates, and a whole set of technology can not industrialization. |
The gravity medicine-injecting method | 15~20 | 20~30 | The transfusion bottle medicine injecting device | Self gravitation | Punching facility medicine injecting device medicament, manpower | 1.3 ~ 1.5 | Preventive effect is better, to the roundheaded borer preventive effect between 70~80%, but the one man operation, but work efficiency is extremely low, generally needs 3 people operation. A medicine bottle is hung by section in the tree, liquid is imported in the hole of butt with conduit, and it is all pretty troublesome that bottle is received in powder charge, is subjected to the geographical environment restriction larger. A whole set of technology can not industrialization. |
Trunk injection | 3~5 | 100~120 | The punching facility | The electric power manpower | Punching facility medicament manpower medicine injecting device | 0.9 ~ 1.1 | Preventive effect is better, and between 70~80%, (aperture 1.5~2cm) has the timber economic worth and to teach large impact but must make a call to the hole of dark approximately a 5~8cm at the tree body during injection to the roundheaded borer preventive effect. Also to seal troublesome poeration after the injection. A whole set of technology |
Can not industrialization. | |||||||
Gravity flow tree trunk injection method | 0.5~ 1.0 | 500~600 | Self-flowing medicine injection device | Transpiration pull | Punching facility medicament manpower | 0.8 ~ 1.2 | Preventive effect is high, and is more than 90%, simple to operate to the roundheaded borer preventive effect, single can finishing. Become miter angle to bore the aperture (aperture 0.5cm) of about a 3~5cm with trunk at butt during use, do not affect the timber economic worth. This technology is not subjected to the restriction of weather, geographical environment. The unification of medicine device does not need special injection machinery and power, but the technology industrialization forms product, is easy to the enterprise-style management operation, can marketization operation. |
The stem brush bandaging strapping | 15~20 | 20~30 | Applicator | - | Applicator wrapper material medicament, manpower | 1.4 ~ 1.6 | Medicament is difficult for infiltrating in the tree body, anti-heterodyne, and it is large to smear dose, wants peeling before the coating, will wrap up troublesome poeration behind the coating. A whole set of technology can not industrialization. |
Poison label method | 15~20 | 20~30 | Poison is signed | - | Bamboo let medicament manpower | 0.8 ~ 1.0 | Drug effect is better, signs but must insert poison in every worm channel, because roundheaded borer is many on trunk top, is difficult to accomplish that can both insert poison in every hole signs, and affect drug effect, and operation is very difficult, time-consuming taking a lot of work. |
The medicament title | The LD-P equation | LD 50(μ g/ head) | Co-toxicity coefficient (CTC) |
Imidacloprid | 8.5989+1.5246x | 4.359×10 -3 | -- |
AVM | 7.0985+1.0757x | 0.0112 | -- |
DDVP | 5.1123+0.8896x | 0.0546 | -- |
Nicotine | 7.6301+2.2581x | 0.0684 | -- |
Quinalphos | 8.8523+3.2122x | 0.0632 | -- |
The desinsection list | 6.7035+1.5002x | 0.0732 | -- |
Acetamiprid | 17.0479+4.809x | 3.124×10 -3 | -- |
Imidacloprid+AVM (4%+0.15%) | 7.7928+1.0987x | 2.871×10 -3 | 153.45 |
Imidacloprid+DDVP (4%+10%) | 6.8482+0.8549x | 6.887×10 -3 | 185.67 |
Imidacloprid+nicotine (2%+7%) | 3.0437-1.0354x | 0.0129 | 124.31 |
Imidacloprid+quinalphos (1%+14%) | 3.1909-1.3765x | 0.0485 | 133.54 |
Imidacloprid+desinsection list (6%+4%) | 7.6974+1.2534x | 7.045×10 -3 | 146.35 |
Imidacloprid+Acetamiprid (3%+8%) | 6.1829+0.7469x | 2.607×10 -3 | 130.21 |
Medicament | Dosage (ml/cm φ) | Roundheaded borer insect population radix | Injection post-equalization death rate % |
5d 15d 30d | |||
The happy liquid formulation for trunk injection of 14% Imidacloprid DDVP 10% Imidacloprid nicotine, 4.15% Imidacloprid AVM 6% Imidacloprid Acetamiprid, 10% Imidacloprid desinsection list liquid formulation for trunk injection 15% Imidacloprid quinalphos, 30% dichlorvos oxygen | 0.8 0.8 0.8 0.8 0.8 0.8 1.2 | 36 47 40 47 43 51 28 | 35.5 75.3 80.5 30.6 45.6 65.3 31.6 51.7 75.3 26.3 35.1 60.5 27.6 41.2 71.8 32.7 50.2 78.6 45.5 72.2 70.8 |
Medicament | Dosage (ml/cm φ) | Insect population radix (defecation hole count) | Insect population number (defecation hole count) | Death rate % | ||||
5d | 15d | 30d | 5d | 15d | 30d | |||
14% Imidacloprid enemy enemy is blunt | 1 | 56 | 37 | 32 | 5 | 34 | 42.8 | 91.1 |
10% Imidacloprid nicotine | 1 | 49 | 47 | 40 | 17 | 4.1 | 14.2 | 65.3 |
4.15% Imidacloprid AVM | 1 | 51 | 40 | 27 | 8 | 21.6 | 47.1 | 84.3 |
15% Imidacloprid quinalphos | 1 | 45 | 37 | 25 | 6 | 17.7 | 44.4 | 86.6 |
The happy liquid formulation for trunk injection of 30% dichlorvos oxygen | 1.2 | 51 | 31 | 18 | 5 | 39.2 | 64.7 | 90.2 |
Contrast | 61 | 57 | 58 | 53 |
Medicament | Dosage (ml/cm φ) | Wood louse insect population radix | Wood louse corrected mortality after the injection |
1d 3d 7d | |||
14% Imidacloprid DDVP | 0.8 | 115 | 21.5 58.9 92.5 |
The happy liquid formulation for trunk injection of 10% Imidacloprid nicotine, 30% dichlorvos oxygen | 1.2 0.8 1.2 0.8 1.2 | 102 165 110 146 135 | 30.3 57.3 93.7 17.6 42.6 90.1 16.8 48.3 88.2 66.5 82.2 95.8 63.8 91.2 96.2 |
Medicament | Dosage (ml/cm φ) | Wood louse corrected mortality (%) after the injection |
1d 3d 7d | ||
The happy liquid formulation for trunk injection of 4.5% Imidacloprid liquid formulation for trunk injection 14% Imidacloprid DDVP liquid formulation for trunk injection, 10% Imidacloprid nicotine liquid formulation for trunk injection 3% acetamiprid EC, 10% Imidacloprid desinsection list liquid formulation for trunk injection 30% dichlorvos oxygen | 0.5 0.5 0.5 0.5 0.5 0.5 | 20 35 91 45 65 93 21 34 85 18 32 65 20 37 78 56 80 95 |
Process | Injection amount (milliliter/diameter of a cross-section of a tree trunk 1.3 meters above the ground) | Insect population number (only) before the injection | The 2d 4d 6d 10d 10d death rate (%) |
The happy liquid formulation for trunk injection contrast of 14% Imidacloprid DDVP, 10% Imidacloprid nicotine, 30% dichlorvos oxygen | 0.8 0.8 0.8 | 413 362 296 199 | 189 220 81 3 99.27 218 163 96 38 89.5 168 209 119 1 99.66 157 187 180 162 |
Medicament | Dosage (ml/cm φ) | Preventive effect % |
2d 5d | ||
The happy liquid formulation for trunk injection of 4.15% Imidacloprid AVM 6% Imidacloprid Acetamiprid, 10% Imidacloprid desinsection list 15% Imidacloprid quinalphos, 30% dichlorvos oxygen | 0.8 0.8 0.8 0.8 0.8 | 70.5 95 37.5 83 32.7 78.2 45.8 91.3 48.6 87 |
Medicament/dosage (ml/ Ф cm) | Land chrysomelid number (head) | Add up to a number |
6h 1d 2d 3d 4d 5d 6d 7d 8d | ||
A/0.4 A/0.7 A/1.0 B/0.4 B/0.7 B/1.0 | 6 12 20 16 20 32 3 0 1 6 27 33 30 28 61 10 0 0 4 33 40 41 39 80 13 3 0 3 14 41 20 19 20 5 6 1 4 13 77 22 20 31 8 1 0 3 12 43 28 19 21 4 0 1 | 110 195 253 129 176 131 |
C/0.4 C/0.7 D/0.4 D/0.7 CK | 0 20 33 11 9 43 0 1 1 0 16 20 8 2 28 3 0 2 0 4 12 9 2 10 0 0 1 2 3 7 3 8 12 8 0 1 0 0 2 0 3 1 0 0 0 | 118 79 38 44 7 |
Medicament/dosage (ml/ Φ cm) | Aphed population (head) |
4.24 4.28 5.2 5.8 5.15 5.20 5.23 | |
A/0.4 A/0.7 A/1.0 B/0.4 B/0.7 | 28 75 12 6 28 12 6 51 75 0 5 15 5 0 31 165 16 0 7 0 2 25 211 78 38 10 25 12 52 182 61 12 0 12 5 |
B/1.0 C/0.4 C/0.7 D/0.4 D/0.7 CK | 25 130 128 0 7 13 2 142 223 228 251 357 985 1654 55 86 17 78 105 704 1426 364 831 942 1780 1367 1142 1567 151 564 732 966 1123 1307 1059 417 1108 1736 2521 2074 1634 1958 |
Medicament/dosage (ml/ Φ cm) | Land borer population (head) | Add up to a number |
6.25 6.26 6.27 6.28 7.2 7.9 7.14 7.19 7.22 7.26 | ||
A/0.4 A/0.4 A/1.0 B/0.4 B/0.7 B/1.0 D/0.4 D/0.7 ck E/0.4 F/0.4 | 16 28 34 27 11 35 19 8 0 0 18 21 30 16 15 37 22 13 1 1 20 14 45 27 35 47 23 14 0 2 11 7 21 12 12 8 30 7 1 0 18 13 25 16 2 15 9 6 3 0 21 12 31 13 24 33 18 12 6 0 26 14 41 31 40 38 7 12 4 6 5 37 30 24 10 5 7 6 3 6 0 2 2 0 0 1 0 0 0 0 - - - - - - - 0 8 4 - - - - - - - 0 10 3 | 178 174 227 109 107 173 219 133 0 12 13 |
Medicament | Dosage (milliliter/centimetre leading thread) | Process the strain number | The death rate (%) |
15d 30d | |||
14% Imidacloprid DDVP, 4.15% Imidacloprid AVM | 0.7 1.0 0.7 1.0 | 20 20 20 20 | 73.42 93.91 90.52 98.75 26.51 65.26 37.48 68.54 |
Claims (3)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 200510043092 CN1291651C (en) | 2005-08-11 | 2005-08-11 | Imidacloprid-containing liquid formulation for trunk injection of trees |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CN 200510043092 CN1291651C (en) | 2005-08-11 | 2005-08-11 | Imidacloprid-containing liquid formulation for trunk injection of trees |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1729777A true CN1729777A (en) | 2006-02-08 |
CN1291651C CN1291651C (en) | 2006-12-27 |
Family
ID=35962223
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CN 200510043092 Expired - Fee Related CN1291651C (en) | 2005-08-11 | 2005-08-11 | Imidacloprid-containing liquid formulation for trunk injection of trees |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN1291651C (en) |
Cited By (19)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101810189A (en) * | 2010-04-01 | 2010-08-25 | 中国热带农业科学院环境与植物保护研究所 | Pesticide composite of imidacloprid and acetamiprid water dispersible granules |
CN101836657A (en) * | 2010-04-01 | 2010-09-22 | 海南大学 | Pesticide composition of imidacloprid and acetamiprid aqueous emulsion |
CN101919387A (en) * | 2010-03-05 | 2010-12-22 | 江西盛林科技发展有限公司 | Compounded preparation of pesticide for preventing and curing forest defoliator by trunk injection |
CN101366375B (en) * | 2008-08-25 | 2011-07-20 | 西北农林科技大学无公害农药研究服务中心 | Liquid formulation for trunk injection containing tebuconazole |
CN102217611A (en) * | 2011-04-19 | 2011-10-19 | 浙江农林大学 | Milbemycins tree trunk injection liquid and application thereof |
CN102246808A (en) * | 2011-07-22 | 2011-11-23 | 天津市绿亨化工有限公司 | Imidacloprid and dichlorvos compound preparation |
CN102578137A (en) * | 2012-02-13 | 2012-07-18 | 中国水稻研究所 | Nitenpyram and quintiofos compound pesticide |
CN102696667A (en) * | 2011-12-19 | 2012-10-03 | 连云港市农业科学院 | Pesticide for controlling corythucha ciliate and use method thereof |
CN101755741B (en) * | 2009-12-30 | 2013-11-13 | 北京富力特农业科技有限责任公司 | Thiacloprid injecta |
CN103875703A (en) * | 2014-03-27 | 2014-06-25 | 上海市绿化管理指导站 | Pesticide paste for controlling longicorn beetles |
CN103918700A (en) * | 2014-03-28 | 2014-07-16 | 海南力智生物工程有限责任公司 | Insecticidal granules and preparation method and application thereof |
CN103960275A (en) * | 2013-01-31 | 2014-08-06 | 浙江农林大学 | Tree trunk injection liquid containing emamectin benzoate and thiacloprid, and preparation method thereof |
CN104170834A (en) * | 2014-07-28 | 2014-12-03 | 浙江天一农化有限公司 | Abamectin.imidacloprid granules for preventing and treating insect pests |
CN105284864A (en) * | 2015-12-04 | 2016-02-03 | 李开森 | Forest fruit trunk-injection insecticide and preparation method and application thereof |
CN109819991A (en) * | 2018-12-21 | 2019-05-31 | 田珍姣 | A kind of soluble concentrate for preventing and treating forest disease and pest by trunk injection apparatus |
CN110477000A (en) * | 2019-09-19 | 2019-11-22 | 山东省林业科学研究院 | A kind of liquid formulation for trunk injection and its preparation method and application of Japanese red pine limb portion pest |
CN112136817A (en) * | 2020-10-16 | 2020-12-29 | 福建农林大学 | A drying injection for preventing and controlling pine wood nematode disease and Monochamus alternatus |
CN115053736A (en) * | 2022-06-27 | 2022-09-16 | 赵卫华 | Novel aphid control method for goldenrain tree by micropore drying injection |
CN116250541A (en) * | 2023-03-16 | 2023-06-13 | 海南利蒙特生物科技有限公司 | Medicament for preventing and treating areca-nut coconut leaf beetles and application thereof |
Families Citing this family (1)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN103039310B (en) * | 2013-01-12 | 2014-04-09 | 昆明钢铁集团有限责任公司 | Perfusion method for preventing diseases and insect pests in tree |
-
2005
- 2005-08-11 CN CN 200510043092 patent/CN1291651C/en not_active Expired - Fee Related
Cited By (26)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN101366375B (en) * | 2008-08-25 | 2011-07-20 | 西北农林科技大学无公害农药研究服务中心 | Liquid formulation for trunk injection containing tebuconazole |
CN101755741B (en) * | 2009-12-30 | 2013-11-13 | 北京富力特农业科技有限责任公司 | Thiacloprid injecta |
CN101919387A (en) * | 2010-03-05 | 2010-12-22 | 江西盛林科技发展有限公司 | Compounded preparation of pesticide for preventing and curing forest defoliator by trunk injection |
CN101810189B (en) * | 2010-04-01 | 2013-10-09 | 中国热带农业科学院环境与植物保护研究所 | Pesticide composite of imidacloprid and acetamiprid water dispersible granules |
CN101836657B (en) * | 2010-04-01 | 2013-06-19 | 中国热带农业科学院环境与植物保护研究所 | Pesticide composition of imidacloprid and acetamiprid aqueous emulsion |
CN101836657A (en) * | 2010-04-01 | 2010-09-22 | 海南大学 | Pesticide composition of imidacloprid and acetamiprid aqueous emulsion |
CN101810189A (en) * | 2010-04-01 | 2010-08-25 | 中国热带农业科学院环境与植物保护研究所 | Pesticide composite of imidacloprid and acetamiprid water dispersible granules |
CN102217611A (en) * | 2011-04-19 | 2011-10-19 | 浙江农林大学 | Milbemycins tree trunk injection liquid and application thereof |
CN102246808A (en) * | 2011-07-22 | 2011-11-23 | 天津市绿亨化工有限公司 | Imidacloprid and dichlorvos compound preparation |
CN102696667A (en) * | 2011-12-19 | 2012-10-03 | 连云港市农业科学院 | Pesticide for controlling corythucha ciliate and use method thereof |
CN102578137A (en) * | 2012-02-13 | 2012-07-18 | 中国水稻研究所 | Nitenpyram and quintiofos compound pesticide |
CN102578137B (en) * | 2012-02-13 | 2013-11-06 | 中国水稻研究所 | Nitenpyram and quintiofos compound pesticide |
CN103960275A (en) * | 2013-01-31 | 2014-08-06 | 浙江农林大学 | Tree trunk injection liquid containing emamectin benzoate and thiacloprid, and preparation method thereof |
CN103960275B (en) * | 2013-01-31 | 2016-05-11 | 浙江农林大学 | Tie up trunk injection liquor of salt and thiacloprid and preparation method thereof containing first |
CN103875703A (en) * | 2014-03-27 | 2014-06-25 | 上海市绿化管理指导站 | Pesticide paste for controlling longicorn beetles |
CN103875703B (en) * | 2014-03-27 | 2015-09-23 | 上海市绿化管理指导站 | A kind of agricultural chemicals paste preventing and treating longicorn |
CN103918700B (en) * | 2014-03-28 | 2016-02-24 | 海南力智生物工程有限责任公司 | A kind of desinsection particle and its preparation method and application |
CN103918700A (en) * | 2014-03-28 | 2014-07-16 | 海南力智生物工程有限责任公司 | Insecticidal granules and preparation method and application thereof |
CN104170834A (en) * | 2014-07-28 | 2014-12-03 | 浙江天一农化有限公司 | Abamectin.imidacloprid granules for preventing and treating insect pests |
CN105284864A (en) * | 2015-12-04 | 2016-02-03 | 李开森 | Forest fruit trunk-injection insecticide and preparation method and application thereof |
CN105284864B (en) * | 2015-12-04 | 2017-03-15 | 李开森 | Woods fruit notes dry insecticide and its preparation method and application |
CN109819991A (en) * | 2018-12-21 | 2019-05-31 | 田珍姣 | A kind of soluble concentrate for preventing and treating forest disease and pest by trunk injection apparatus |
CN110477000A (en) * | 2019-09-19 | 2019-11-22 | 山东省林业科学研究院 | A kind of liquid formulation for trunk injection and its preparation method and application of Japanese red pine limb portion pest |
CN112136817A (en) * | 2020-10-16 | 2020-12-29 | 福建农林大学 | A drying injection for preventing and controlling pine wood nematode disease and Monochamus alternatus |
CN115053736A (en) * | 2022-06-27 | 2022-09-16 | 赵卫华 | Novel aphid control method for goldenrain tree by micropore drying injection |
CN116250541A (en) * | 2023-03-16 | 2023-06-13 | 海南利蒙特生物科技有限公司 | Medicament for preventing and treating areca-nut coconut leaf beetles and application thereof |
Also Published As
Publication number | Publication date |
---|---|
CN1291651C (en) | 2006-12-27 |
Similar Documents
Publication | Publication Date | Title |
---|---|---|
CN1291651C (en) | Imidacloprid-containing liquid formulation for trunk injection of trees | |
KR101451978B1 (en) | Pesticidal Composition for Tree Parastic Pests | |
CN107779408B (en) | Beauveria bassiana for preventing and treating scarab beetles and microbial agent thereof | |
CN101073324A (en) | Synergistic insect-killing composition | |
KR20110033691A (en) | Environment-friendly organic agricultural products for soil insect pest control | |
CN1759675A (en) | Pesticide containing comptothecin or dreivates of camptothecin, and preparation method | |
CN1802912A (en) | Mixed herbicide for dry land | |
CN1297196C (en) | Insecticide composition containing methylamino Avermectin and matrine | |
CN104081977A (en) | Method for planting magnolia officinalis | |
CN105874997A (en) | Method for increasing soil carbon-nitrogen ratio for direct returning to field by adding urea after crushing corn straws | |
CN1524420A (en) | Insecticidal composition containing methylamino abamectin and pyrethroid compound | |
CN1647652A (en) | Pesticide composition containing methyl amino abamectin and bacillus thuringiensis | |
CN108902139B (en) | Yunnan longicorn attractant and application thereof | |
Pohan et al. | The use of bokashi compost as a soil fertility amendment in increasing vegetative growth of organic tomato (Lycopersicum esculentum Mill.) | |
Ingham | Soil biology | |
CN100342787C (en) | Combination of insect disinfectations containing benzoate of Avermectin in methylamine group and azadirachtin | |
CN105746566B (en) | A kind of trunk injection liquor containing dinotefuran | |
CN109258683B (en) | Ointment with internal absorption and conduction functions for preventing and treating longhorn beetles and using method thereof | |
CN1736194A (en) | Application of alpha-trithiophene in control of pine wood nematode disease | |
CN109168905B (en) | Roxburgh rose planting method | |
CN105767011A (en) | Nematode granules capable of promoting recovery of diseased plants | |
CN1943354A (en) | Novel pesticide for preventing corn core losing | |
CN1593142A (en) | Mixed herbicide | |
WO2011152700A1 (en) | A palm growth underground formulation | |
CN110495388B (en) | Application of lauric acid in preparation of plant resistance activator |
Legal Events
Date | Code | Title | Description |
---|---|---|---|
C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
ASS | Succession or assignment of patent right |
Owner name: FUJI BIOTECH. (SHANGHAI) CO., LTD. Free format text: FORMER OWNER: YANGLING NWSUAF RESEARCH + DEVELOPMENT CENTER OF BIORATIONAL PESTICIDE Effective date: 20110929 |
|
C41 | Transfer of patent application or patent right or utility model | ||
C56 | Change in the name or address of the patentee |
Owner name: YANGLING NWSUAF RESEARCH + DEVELOPMENT CENTER OF B Free format text: FORMER NAME: NUISANCELESS PESTICIDE RESEARCH SERVICE CENTER, XIBEI AGROFORESTRY SCIENCE AND T |
|
COR | Change of bibliographic data |
Free format text: CORRECT: ADDRESS; FROM: 712100 XIANYANG, SHAANXI PROVINCE TO: 200443 BAOSHAN, SHANGHAI |
|
CP03 | Change of name, title or address |
Address after: 712100 Yangling District, Shaanxi Province Patentee after: RESEARCH & DEVELOPMENT CENTER OF BIORATIONAL PESTICIDE YANGLING NONGKEDA Address before: 712100 Shaanxi Province Tai Road No. 3 in Yangling demonstration zone Patentee before: Pollution free pesticide research and service center of northwest agricultural and Forestry University |
|
TR01 | Transfer of patent right |
Effective date of registration: 20110929 Address after: 200443 Shanghai City, Baoshan District No. 588 South Building 10C Yunlu Ji Patentee after: FUJI BIOLOGICAL TECHNOLOGY DEVELOPMENT (SHANGHAI) CO.,LTD. Address before: 712100 Yangling District, Shaanxi Province Patentee before: RESEARCH & DEVELOPMENT CENTER OF BIORATIONAL PESTICIDE YANGLING NONGKEDA |
|
PE01 | Entry into force of the registration of the contract for pledge of patent right |
Denomination of invention: Liquid formulation containing imidacloprid for trunk injection Effective date of registration: 20120321 Granted publication date: 20061227 Pledgee: Shanghai Sino Investment Group Co.,Ltd. Pledgor: FUJI BIOLOGICAL TECHNOLOGY DEVELOPMENT (SHANGHAI) CO.,LTD. Registration number: 2012990000095 |
|
PC01 | Cancellation of the registration of the contract for pledge of patent right |
Date of cancellation: 20160901 Granted publication date: 20061227 Pledgee: Shanghai Sino Investment Group Co.,Ltd. Pledgor: FUJI BIOLOGICAL TECHNOLOGY DEVELOPMENT (SHANGHAI) CO.,LTD. Registration number: 2012990000095 |
|
PLDC | Enforcement, change and cancellation of contracts on pledge of patent right or utility model | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20061227 Termination date: 20180811 |
|
CF01 | Termination of patent right due to non-payment of annual fee |