CN1703956A - Ant and cockroach killing pesticide formula and production technology - Google Patents
Ant and cockroach killing pesticide formula and production technology Download PDFInfo
- Publication number
- CN1703956A CN1703956A CN 02160097 CN02160097A CN1703956A CN 1703956 A CN1703956 A CN 1703956A CN 02160097 CN02160097 CN 02160097 CN 02160097 A CN02160097 A CN 02160097A CN 1703956 A CN1703956 A CN 1703956A
- Authority
- CN
- China
- Prior art keywords
- content
- auxiliary material
- worm nitrile
- fluorine worm
- meal
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Pending
Links
- 241001674044 Blattodea Species 0.000 title claims abstract description 15
- 238000005516 engineering process Methods 0.000 title claims abstract description 11
- 238000009472 formulation Methods 0.000 title claims abstract description 11
- 238000004519 manufacturing process Methods 0.000 title abstract description 5
- 239000000575 pesticide Substances 0.000 title abstract 2
- 239000000463 material Substances 0.000 claims abstract description 19
- 244000068988 Glycine max Species 0.000 claims abstract description 18
- 235000010469 Glycine max Nutrition 0.000 claims abstract description 18
- 239000000843 powder Substances 0.000 claims abstract description 18
- 235000008331 Pinus X rigitaeda Nutrition 0.000 claims abstract description 16
- 235000011613 Pinus brutia Nutrition 0.000 claims abstract description 16
- 241000018646 Pinus brutia Species 0.000 claims abstract description 16
- 240000008042 Zea mays Species 0.000 claims abstract description 12
- 235000002017 Zea mays subsp mays Nutrition 0.000 claims abstract description 12
- 238000001035 drying Methods 0.000 claims abstract description 12
- YCKRFDGAMUMZLT-UHFFFAOYSA-N Fluorine atom Chemical compound [F] YCKRFDGAMUMZLT-UHFFFAOYSA-N 0.000 claims description 30
- 229910052731 fluorine Inorganic materials 0.000 claims description 30
- 239000011737 fluorine Substances 0.000 claims description 30
- 150000002825 nitriles Chemical class 0.000 claims description 30
- 235000019764 Soybean Meal Nutrition 0.000 claims description 13
- 235000012054 meals Nutrition 0.000 claims description 13
- 239000004455 soybean meal Substances 0.000 claims description 13
- 239000000203 mixture Substances 0.000 claims description 12
- 235000005824 Zea mays ssp. parviglumis Nutrition 0.000 claims description 11
- 235000005822 corn Nutrition 0.000 claims description 11
- 235000013312 flour Nutrition 0.000 claims description 9
- 241000257303 Hymenoptera Species 0.000 claims description 7
- 230000000749 insecticidal effect Effects 0.000 claims description 7
- 238000010298 pulverizing process Methods 0.000 claims description 6
- 239000004615 ingredient Substances 0.000 claims description 3
- 239000012467 final product Substances 0.000 claims description 2
- 235000015895 biscuits Nutrition 0.000 abstract description 6
- ZOCSXAVNDGMNBV-UHFFFAOYSA-N 5-amino-1-[2,6-dichloro-4-(trifluoromethyl)phenyl]-4-[(trifluoromethyl)sulfinyl]-1H-pyrazole-3-carbonitrile Chemical compound NC1=C(S(=O)C(F)(F)F)C(C#N)=NN1C1=C(Cl)C=C(C(F)(F)F)C=C1Cl ZOCSXAVNDGMNBV-UHFFFAOYSA-N 0.000 abstract 2
- 239000005899 Fipronil Substances 0.000 abstract 2
- 229940013764 fipronil Drugs 0.000 abstract 2
- 235000016383 Zea mays subsp huehuetenangensis Nutrition 0.000 abstract 1
- 239000000428 dust Substances 0.000 abstract 1
- 239000002075 main ingredient Substances 0.000 abstract 1
- 235000009973 maize Nutrition 0.000 abstract 1
- 238000003756 stirring Methods 0.000 abstract 1
- 239000002023 wood Substances 0.000 abstract 1
- 239000000047 product Substances 0.000 description 9
- 239000003814 drug Substances 0.000 description 6
- 239000006071 cream Substances 0.000 description 5
- 239000002994 raw material Substances 0.000 description 5
- 230000000694 effects Effects 0.000 description 4
- LCCNCVORNKJIRZ-UHFFFAOYSA-N parathion Chemical compound CCOP(=S)(OCC)OC1=CC=C([N+]([O-])=O)C=C1 LCCNCVORNKJIRZ-UHFFFAOYSA-N 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- LHHGDZSESBACKH-UHFFFAOYSA-N chlordecone Chemical compound ClC12C3(Cl)C(Cl)(Cl)C4(Cl)C2(Cl)C2(Cl)C4(Cl)C3(Cl)C1(Cl)C2=O LHHGDZSESBACKH-UHFFFAOYSA-N 0.000 description 2
- GVYLCNUFSHDAAW-UHFFFAOYSA-N mirex Chemical compound ClC12C(Cl)(Cl)C3(Cl)C4(Cl)C1(Cl)C1(Cl)C2(Cl)C3(Cl)C4(Cl)C1(Cl)Cl GVYLCNUFSHDAAW-UHFFFAOYSA-N 0.000 description 2
- 239000000126 substance Substances 0.000 description 2
- ZHLKXBJTJHRTTE-UHFFFAOYSA-N Chlorobenside Chemical compound C1=CC(Cl)=CC=C1CSC1=CC=C(Cl)C=C1 ZHLKXBJTJHRTTE-UHFFFAOYSA-N 0.000 description 1
- 241000238631 Hexapoda Species 0.000 description 1
- 241000256602 Isoptera Species 0.000 description 1
- 229910019142 PO4 Inorganic materials 0.000 description 1
- 239000003905 agrochemical Substances 0.000 description 1
- 230000007613 environmental effect Effects 0.000 description 1
- 239000008187 granular material Substances 0.000 description 1
- 239000002917 insecticide Substances 0.000 description 1
- 231100000053 low toxicity Toxicity 0.000 description 1
- 238000012856 packing Methods 0.000 description 1
- 235000021317 phosphate Nutrition 0.000 description 1
- 150000003013 phosphoric acid derivatives Chemical class 0.000 description 1
- 231100000572 poisoning Toxicity 0.000 description 1
- 230000000607 poisoning effect Effects 0.000 description 1
- 238000009366 sericulture Methods 0.000 description 1
- 239000002893 slag Substances 0.000 description 1
- 239000000375 suspending agent Substances 0.000 description 1
Landscapes
- Agricultural Chemicals And Associated Chemicals (AREA)
Abstract
The invention relates to an ant and cockroach killing pesticide formula and production technology, which is prepared through using Fipronil as main ingredient, charging pine wood dust or fried soybean powder or soya bean powder or biscuit powder or maize powder as auxiliary materials, disintegrating one or two of the auxiliary materials, passing through 50 mesh sieve, mixing proportionally, stirring homogeneously, mixing with Fipronil, finally passing through drying treatment.
Description
Technical field
The present invention relates to a kind of insecticide formulation and technology, insecticidal formulation of particularly a kind of killing ants cockroach and technology, it mainly is applicable to the occasion of going out ant in city, the rural environment and killing cockroach.
Background technology
China begins promptly in succession limit production and uses organic chlorbenside ant worm medicament from the seventies, and as mirex, Niran, kepone (KEPONE), up to the present China still has many enterprises this medicament of production and selling ant that is used to go out to kill the cockroach activity.Owing to consider from the angle of environmental protection and reduction pollution, China completely forbids from calendar year 2001 and uses Niran, but present domestic sericulture production is gone up major part and is still being used it to do the ant repellant agent, this is that the ant effect is very good because forbidden mirex and Niran go out, for the moment also can't find better substitute on the market, although the organic phosphates deinsectization medicine also can kill ant, cockroach, because its strong smell, above-mentioned insect is is obviously walked quickly and kept away, and does not bump and does not eat.
Summary of the invention
Technical problem to be solved by this invention is a kind of good disinsection effect of design, can eliminate the ant cockroach to the phobotaxis of medicine and allow insecticidal formulation and the technology of the killing ants cockroach of using.
It is to be major ingredient with fluorine worm nitrile that the present invention addresses the above problem the technical scheme that is adopted, add the auxiliary material pine sawdust or fry soybean meal or analysis for soybean powder or cracker meal or corn flour, with standby after pine sawdust or stir-fry soybean meal or analysis for soybean powder or cracker meal or the corn flour pulverizing, again fluorine worm nitrile is sneaked in the auxiliary material after the above-mentioned pulverizing, get final product after handling by drying.
Auxiliary material of the present invention can be two or more also, when auxiliary material is two or more, need mix standby after the pulverizing again.
Fluorine worm nitrile content of the present invention is 0.05～1%, pine sawdust content is greater than zero, less than 99.95%, fry soybean meal content and be greater than zero, less than 99.95%, analysis for soybean powder content is greater than zero, less than 99.95%, cracker meal is greater than zero, less than 99.95%, and corn flour is for greater than zero, less than 99.95% (said content is weight percentage).
Auxiliary material of the present invention pulverizes that the back is standby to be meant that to pulverize 50 orders above standby.
The present invention compared with prior art, have the following advantages and effect: it is effective to use fluorine worm nitrile to make poisoning agent, add a certain proportion of bait (auxiliary material) and can eliminate the phobotaxis of ant cockroach, have low toxicity, efficient, pollution-free, characteristics such as price is low, easy to use and stable in properties medicine.
Embodiment
Major ingredient among the present invention is a fluorine worm nitrile (FRPRONIL), and its chemical name is: (RS)-and 5-amino-1-(2,6-two chloro-4 α-trifluoromethyl)-4-trifluoromethyl sulfinyl pyrazole-3-nitrile.Chemical structural formula is as follows:
When using fluorine worm nitrile, can use the granule of 5% suspending agent or 3% or the fluorine worm nitrile agricultural chemicals of other formulation, also can be the former medicine of fluorine worm nitrile.
The present invention can only use fluorine worm nitrile and pine sawdust (sawmilling slag) in the prescription when killing termite, do not add the auxiliary material of other composition, and adding also can certainly.When killing black ant or cockroach, can not add pine sawdust, only add fry soybean meal and or analysis for soybean powder and or cracker meal and or corn flour, it is also passable to add pine sawdust certainly.
Embodiment 1:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.25 | ??0.5 | ??1 |
| Cracker meal | ??25.5 | ??65.5 | ??75 | ??73.5 |
| Fry soybean meal | ??73 | ??33 | ??23.5 | ??24 |
| Thin pine sawdust | ??1.45 | ??1.25 | ??1 | ??1.5 |
After soybean fried, pulverize, cross 50 mesh sieves with cracker; Biscuit (cream wafer is good especially) is directly broken into fine powder with cracker, cross 50 mesh sieves; Pine sawdust was pulverized 20 mesh sieves, above-mentioned raw materials was mixed in proportion standby.Again fluorine worm nitrile is sneaked in the auxiliary material by prescription, drying handle (as oven dry) back product.
Embodiment 2:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.35 | ??0.55 | ??1 |
| Fry soybean meal | ??60 | ??29.65 | ??25 | ??40 |
| Corn flour | ??9 | ??20 | ??40.45 | ??50 |
| Cracker meal | ??30.95 | ??50 | ??34 | ??9 |
After soybean fried, pulverize, cross 50 mesh sieves with cracker; Biscuit (cream wafer is good especially) is directly broken into fine powder with cracker, cross 50 mesh sieves; Corn was pulverized 50 mesh sieves, above-mentioned raw materials was mixed in proportion standby.Again fluorine worm nitrile is sneaked in the auxiliary material by prescription, drying handle (as oven dry) back product.
Embodiment 3:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.3 | ??0.7 | ??1 |
| Thin pine sawdust | ??99.95 | ??99.7 | ??99.3 | ??99 |
Pine sawdust is pulverized, and it is standby to cross 20 mesh sieves, again fluorine worm nitrile is sneaked in the pine sawdust by formula rate, drying handle the back product.
Embodiment 4:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.6 | ??0.75 | ??1 |
| Fry soybean meal | ??15.95 | ??10 | ??25 | ??30 |
| Cracker meal | ??84 | ??89.4 | ??74.25 | ??69 |
After soybean fried, pulverize, cross 50 mesh sieves with cracker; Biscuit (cream wafer is good especially) is directly broken into fine powder with cracker, cross 50 mesh sieves; Above-mentioned raw materials is mixed in proportion standby.Again fluorine worm nitrile is sneaked in the auxiliary material by prescription, drying handle (as oven dry) product.
Embodiment 5:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.3 | ??0.8 | ??1 |
| Fry soybean meal | ??70.95 | ??29.7 | ??20.2 | ??30 |
| Corn flour | ??29 | ??70 | ??79 | ??69 |
After soybean fried, pulverize, cross 50 mesh sieves with cracker; Corn was pulverized 50 mesh sieves, above-mentioned raw materials was mixed in proportion standby.Again fluorine worm nitrile is sneaked in the auxiliary material by prescription, drying handle (as oven dry) back product.
Embodiment 6:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.09 | ??0.5 | ??1 |
| Cracker meal | ??99.95 | ??99.91 | ??99.5 | ??99 |
Biscuit (cream wafer is good especially) is directly broken into fine powder with cracker, and it is standby to cross 50 mesh sieves; Again fluorine worm nitrile is sneaked in the cracker meal by prescription, drying handle (as oven dry) back product.
Embodiment 7:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.2 | ??0.8 | ??1 |
| Fry soybean meal | ??99.95 | ??99.8 | ??99.2 | ??99 |
After soybean fried, pulverize with cracker, it is standby to cross 50 mesh sieves; Again fluorine worm nitrile is sneaked into by prescription and fries in the soybean meal, drying handle (as oven dry) back product.
Embodiment 8:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.08 | ??0.4 | ??1 |
| Analysis for soybean powder | ??99.95 | ??99.92 | ??99.6 | ??99 |
After soya bean fried, pulverize with cracker, it is standby to cross 50 mesh sieves, again fluorine worm nitrile is sneaked in the pine sawdust by formula rate, drying handle the back product, just can put on market by packing.
Embodiment 9:
| Title | Content % (percentage by weight) | |||
| Fluorine worm nitrile | ??0.05 | ??0.25 | ??0.75 | ??1 |
| Cracker meal | ??80 | ??35.5 | ??10.25 | ??94 |
| Analysis for soybean powder | ??19.95 | ??64.25 | ??89 | ??5 |
Biscuit (cream wafer is good especially) is directly broken into fine powder with cracker, cross 50 mesh sieves, after soya bean is fried, pulverize, cross 50 mesh sieves with cracker; Again above-mentioned raw materials is mixed in proportion standby.Fluorine worm nitrile is sneaked in the auxiliary material by formula rate, drying handle (as oven dry) back product.
Claims (4)
1. insecticidal formulation of a killing ants cockroach and technology, it is characterized in that: with fluorine worm nitrile is major ingredient, add the auxiliary material pine sawdust or fry soybean meal or analysis for soybean powder or cracker meal or corn flour, with standby after pine sawdust or stir-fry soybean meal or analysis for soybean powder or cracker meal or the corn flour pulverizing, again fluorine worm nitrile is sneaked in the auxiliary material after the above-mentioned pulverizing, get final product after handling by drying.
2. insecticidal formulation of killing ants cockroach according to claim 1 and technology is characterized in that: described auxiliary material can be two or more also, when auxiliary material is two or more, need mix standby after the pulverizing again.
3. insecticidal formulation of killing ants cockroach according to claim 1 and 2 and technology, it is characterized in that: described fluorine worm nitrile content is 0.05～1%, pine sawdust content is greater than zero, less than 99.95%, fry soybean meal content and be greater than zero, less than 99.95%, analysis for soybean powder content is greater than zero, less than 99.95%, cracker meal content is greater than zero, less than 99.95%, and corn flour content is for greater than zero, less than 99.95% (said content is weight percentage).
4. insecticidal formulation of killing ants cockroach according to claim 1 and 2 and technology is characterized in that: described auxiliary material pulverizes that the back is standby to be meant that to pulverize 50 orders above standby.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02160097 CN1703956A (en) | 2002-12-31 | 2002-12-31 | Ant and cockroach killing pesticide formula and production technology |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 02160097 CN1703956A (en) | 2002-12-31 | 2002-12-31 | Ant and cockroach killing pesticide formula and production technology |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1703956A true CN1703956A (en) | 2005-12-07 |
Family
ID=35575604
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 02160097 Pending CN1703956A (en) | 2002-12-31 | 2002-12-31 | Ant and cockroach killing pesticide formula and production technology |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1703956A (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102458126A (en) * | 2009-04-28 | 2012-05-16 | 巴斯夫公司 | Foamable pesticide compositions |
| CN102726425A (en) * | 2011-04-08 | 2012-10-17 | 富荣龙 | Cockroach killer |
| CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
| CN105309453A (en) * | 2014-05-31 | 2016-02-10 | 尹连花 | Formula and process of insecticide for killing ants and blattodea |
| CN106665627A (en) * | 2016-12-28 | 2017-05-17 | 北京贝达化工股份有限公司 | Cockroach attractant, preparation method of cockroach attractant and cockroach bait |
| CN106818889A (en) * | 2017-01-18 | 2017-06-13 | 华中农业大学 | A kind of particle bait formulation of trapping and killing termites and preparation method thereof |
| CN107821415A (en) * | 2017-11-23 | 2018-03-23 | 杨锡奇 | A kind of Cockroach killing bait agent and preparation method thereof |
-
2002
- 2002-12-31 CN CN 02160097 patent/CN1703956A/en active Pending
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102458126A (en) * | 2009-04-28 | 2012-05-16 | 巴斯夫公司 | Foamable pesticide compositions |
| CN102458126B (en) * | 2009-04-28 | 2014-07-02 | 巴斯夫公司 | Foamable pesticide compositions |
| CN104082289A (en) * | 2009-04-28 | 2014-10-08 | 巴斯夫公司 | Foamable Pesticide Compositions |
| CN102726425A (en) * | 2011-04-08 | 2012-10-17 | 富荣龙 | Cockroach killer |
| CN102845466A (en) * | 2012-08-13 | 2013-01-02 | 北京绿叶世纪日化用品有限公司 | High-efficiency cockroach-killing bait and preparation method thereof |
| CN105309453A (en) * | 2014-05-31 | 2016-02-10 | 尹连花 | Formula and process of insecticide for killing ants and blattodea |
| CN106665627A (en) * | 2016-12-28 | 2017-05-17 | 北京贝达化工股份有限公司 | Cockroach attractant, preparation method of cockroach attractant and cockroach bait |
| CN106818889A (en) * | 2017-01-18 | 2017-06-13 | 华中农业大学 | A kind of particle bait formulation of trapping and killing termites and preparation method thereof |
| CN107821415A (en) * | 2017-11-23 | 2018-03-23 | 杨锡奇 | A kind of Cockroach killing bait agent and preparation method thereof |
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| C12 | Rejection of a patent application after its publication | ||
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