CN1698575A - Reddish brown Chinese traditional medicine dyestuff hair dye using cloves as penetrating agent - Google Patents

Reddish brown Chinese traditional medicine dyestuff hair dye using cloves as penetrating agent Download PDF

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Publication number
CN1698575A
CN1698575A CN 200510026615 CN200510026615A CN1698575A CN 1698575 A CN1698575 A CN 1698575A CN 200510026615 CN200510026615 CN 200510026615 CN 200510026615 A CN200510026615 A CN 200510026615A CN 1698575 A CN1698575 A CN 1698575A
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China
Prior art keywords
agent
deionized water
flos caryophylli
hair dye
add
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CN 200510026615
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Chinese (zh)
Inventor
周飞骏
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Shanghai Jiaotong University
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Shanghai Jiaotong University
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Priority to CN 200510026615 priority Critical patent/CN1698575A/en
Publication of CN1698575A publication Critical patent/CN1698575A/en
Pending legal-status Critical Current

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Abstract

Disclosed is a reddish brown Chinese traditional medicine dyestuff hair dye using cloves as penetrating agent comprising agent No.1 and agent No.2, the agent No. 1 employs nontoxic giant knotweed rhizome as the red brown dyestuff, traditional Chinese medicinal clove as penetrating agent for enhancing color stability, alkalinizing agents ammonium hydroxide and monoethanolamine for adjusting pH, sodium polyacrylate as thickening agent, sodium sulphate as anti-oxidizing agent and disodiumedetate as chelating agent, while the agent 2 employs hydrogen peroxide and belamcanda rhizome as combined oxidation agent, added clove as penetrating agent for improving effect of cooxidant, sodium polyacrylate as thickening agent, 8-hydroxyquinoline sulphate as stabilizing agent for prevention of hydrogen peroxide decomposition.

Description

With the Flos Caryophylli is the rufous Chinese medicine dyestuff hair dye of penetrating agent
Technical field
The present invention relates to a kind of colored hair dye, relating in particular to a kind of is the rufous Chinese medicine dyestuff hair dye of penetrating agent with the Flos Caryophylli, belongs to the cosmetics industry technical field.
Background technology
Along with people's living standard improves constantly, to healthy, the pursuit of U.S. has been become increasing people's yearning, ecological idea also is rooted in the hearts of the people day by day simultaneously, therefore, dyes the color favor that will be subjected to consumer of sending out with Chinese medicine dyestuff instead of chemical dyestuff.
But, use at present, or the Chinese medicine dyestuff of reported in literature dyes agent for dying hair coloured and still has place not as people's will.The problem that has the safety aspect that has, for example application number is 00128128.3 Chinese invention patent " a kind of rinse and preparation method thereof ", use be Chinese medicine Flos Impatientis water, because of Ministry of Public Health Flos Impatientis is listed in banned substance and stops to promote listing.The performance that has can not satisfy the demands of consumers, and for example the retention time is short.JP02,166,716 (1990) contain natural dye (berberine chloride, alkermes etc.) hair dye, belong to semi-permanent hairdye, hair dyeing effect can only keep about three weeks, and the color dullness, can not satisfy the Chinese medicine dyestuff and dye the color growth requirement of sending out.
Summary of the invention
The objective of the invention is at the deficiencies in the prior art and real life demand, a kind of novel rufous Chinese medicine dyestuff hair dye is provided, safe in utilization nontoxic, can not only improve hair dyeing effect, and can reduce the infringement of hair dye to hair quality, promote the development of the colored hair dye of Chinese medicine.
For realizing this purpose, Chinese medicine dyestuff hair dye provided by the invention comprises No. 1 agent and No. 2 agent, wherein to select nontoxic Rhizoma Polygoni Cuspidati for use be brick-red dye in No. 1 agent, adding with the Chinese medicine Flos Caryophylli is that penetrating agent strengthens dyefastness, regulate pH value with basifier ammonium hydroxide, monoethanolamine, and be equipped with thickening agent sodium polyacrylate, antioxidant sodium sulfite and chelating agen disodiumedetate.No. 2 agent adopt hydrogen peroxide and Rhizoma Belamcandae to be the combination oxidant, add the Flos Caryophylli penetrating agent to improve the usefulness of cooxidant, are equipped with the thickening agent sodium polyacrylate again, are equipped with the stabilizing agent oxine sulfate that prevents hydrogen peroxide decomposes.
Chinese medicine dyestuff hair dye particular content of the present invention is:
The mass percent of No. 1 each constituent of agent:
Brick-red dye Rhizoma Polygoni Cuspidati 3-15%, penetrating agent Flos Caryophylli 1-10%, basifier ammonium hydroxide and monoethanolamine, it is 9-10 that its consumption makes No. 1 agent keep pH value, thickening agent sodium polyacrylate 0.2%, antioxidant sodium sulfite 0.1-0.5%, chelating agen disodiumedetate 0.2%, all the other are deionized water.
The mass percent of No. 2 each constituent of agent:
The combination oxidant: hydrogen peroxide (by 100%) 2-4% and Rhizoma Belamcandae 1-15%, penetrating agent Flos Caryophylli 1-10%, thickening agent sodium polyacrylate 0.2%, stabilizing agent oxine sulfate 0.2%, all the other are deionized water.
The concrete compound method of No. 1 agent is as follows among the present invention:
After sodium polyacrylate adds deionized water (1: 20) and soaks 12 hours, add residue deionized water, Rhizoma Polygoni Cuspidati, Flos Caryophylli, monoethanolamine, disodiumedetate, sodium sulfite, stir and heat to 70 ℃, kept 20 minutes, be cooled to room temperature, repeated hydrogenation amine-oxides, check, fill.
The concrete compound method of No. 2 agent is as follows among the present invention:
In a container, add earlier 60% deionized water, addition polymerization acrylic acid sodium, Rhizoma Belamcandae, Flos Caryophylli, heat, be incubated 15 minutes, be cooled to 40 ℃ to 70 ℃.In No. two containers, add the deionized water of residue 40% then, be heated to 40 ℃, oxine sulfate is added, be stirred to dissolving fully, slowly add in container, be cooled to 30 ℃, add hydrogen peroxide again.Stirring, check, fill.
Using method: hair washing earlier before the hair dyeing dries up.Then No. 1 agent and No. 2 agent are mixed well with one to one, be coated on the hair.40 ℃ are incubated about 20 minutes, cooled off ten minutes.With shampoo hair washing, dry up and get final product.
Chinese medicine dyestuff hair dye of the present invention has unique advantage.The present invention is directed to existing Chinese medicine dyestuff and have safety issue, selecting nontoxic Rhizoma Polygoni Cuspidati for use is raw material, relatively big at Chinese medicine dye molecule quality, be difficult for entering hair hair small pieces gap, the problem that color fastness is not enough, adding with the Chinese medicine Flos Caryophylli is penetrating agent, helps the Chinese medicine dyestuff to enter hair hair small pieces gap, strengthens dyefastness.The Rhizoma Polygoni Cuspidati rufous Chinese medicine dyestuff hair dye that the present invention innovates preparation has overcome the shortcoming of Chinese medicine dyeing dullness, has enriched the treasure-house of Chinese medicine hair dye.
Chinese medicine dyestuff hair dye of the present invention does not contain any chemical pigment, and is nontoxic after testing, can not cause the mammalian cell chromosome mutation, can not cause the salmonella typhimurium cell sudden change, safe in utilization.Content of hydrogen peroxide is low, thereby can reduce the infringement of hair dye to hair quality largely, and institute's dyeing hair is a rufous, and gloss is flexible, can keep three months colour-fast.
The specific embodiment
Below in conjunction with specific embodiment technical scheme of the present invention is further described.
Embodiment 1
The mass percent of No. 1 each constituent of agent: Rhizoma Polygoni Cuspidati 3%, Flos Caryophylli 10%, ammonium hydroxide (28%) 10%, monoethanolamine (99.0%) 2%, sodium sulfite 0.1%, sodium polyacrylate 0.2%, disodiumedetate 0.2%, deionized water adds to 100%.
The mass percent of No. 2 each constituent of agent: hydrogen peroxide (by 100%) 4%, Rhizoma Belamcandae 1%, Flos Caryophylli 1%, sodium polyacrylate 0.2%, oxine sulfate 0.2%, deionized water adds to 100%.
The concrete compound method of No. 1 agent is as follows among the present invention:
After sodium polyacrylate adds deionized water (1: 20) and soaks 12 hours, add residue deionized water, Rhizoma Polygoni Cuspidati, Flos Caryophylli, monoethanolamine, disodiumedetate, sodium sulfite, stir and heat to 70 ℃, kept 20 minutes, be cooled to room temperature, repeated hydrogenation amine-oxides, check, fill.
The concrete compound method of No. 2 agent is as follows among the present invention:
In a container, add earlier 60% deionized water, addition polymerization acrylic acid sodium, Rhizoma Belamcandae, Flos Caryophylli, heat, be incubated 15 minutes, be cooled to 40 ℃ to 70 ℃.In No. two containers, add the deionized water of residue 40% then, be heated to 40 ℃, oxine sulfate is added, be stirred to dissolving fully, slowly add in container, be cooled to 30 ℃, add hydrogen peroxide again.Stirring, check, fill.
Using method: hair washing earlier before the hair dyeing dries up.Then No. 1 agent and No. 2 agent are mixed well with one to one, be coated on the hair.40 ℃ are incubated about 20 minutes, cooled off ten minutes.With shampoo hair washing, dry up and get final product.
Embodiment 2
The mass percent of No. 1 each constituent of agent: Rhizoma Polygoni Cuspidati 8%, Flos Caryophylli 5%, ammonium hydroxide (28%) 10%, monoethanolamine (99.0%) 2%, sodium sulfite 0.3%, sodium polyacrylate 0.2%, disodiumedetate 0.2%, deionized water adds to 100%.
The mass percent of No. 2 each constituent of agent: hydrogen peroxide (by 100%) 3%, Rhizoma Belamcandae 10%, Flos Caryophylli 5%, sodium polyacrylate 0.2%, oxine sulfate 0.2%, deionized water adds to 100%.
The compound method of No. 1 agent and No. 2 agent and using method are with embodiment 1.
Embodiment 3
The mass percent of No. 1 each constituent of agent: Rhizoma Polygoni Cuspidati 15%, Flos Caryophylli 1%, ammonium hydroxide (28%) 10%, monoethanolamine (99.0%) 2%, sodium sulfite 0.5%, sodium polyacrylate 0.2%, disodiumedetate 0.2%, deionized water adds to 100%.
The mass percent of No. 2 each constituent of agent: hydrogen peroxide (by 100%) 2%, Rhizoma Belamcandae 15%, Flos Caryophylli 10%, sodium polyacrylate 0.2%, oxine sulfate 0.2%, deionized water adds to 100%.
The compound method of No. 1 agent and No. 2 agent and using method are with embodiment 1.
The Chinese medicine dyestuff hair dye of above-mentioned three embodiment is nontoxic after testing, safe in utilization, significantly reduces the infringement of hair dye to hair quality, and institute's dyeing hair is a rufous, and gloss is flexible, can keep three months colour-fast.

Claims (2)

1, a kind of is the rufous Chinese medicine dyestuff hair dye of penetrating agent with the Flos Caryophylli, comprise No. 1 agent and No. 2 agent, the mass percent that it is characterized in that No. 1 each constituent of agent is: Rhizoma Polygoni Cuspidati 3-15%, Flos Caryophylli 1-10%, ammonium hydroxide and monoethanolamine, it is 9-10 that its consumption makes No. 1 agent keep pH value, sodium polyacrylate 0.2%, sodium sulfite 0.1-0.5%, disodiumedetate 0.2%, all the other are deionized water; The mass percent of No. 2 each constituent of agent is: hydrogen peroxide 2-4%, and Rhizoma Belamcandae 1-15%, Flos Caryophylli 1-10%, sodium polyacrylate 0.2%, oxine sulfate 0.2%, all the other are deionized water.
2, a kind of preparation method of Chinese medicine dyestuff hair dye of claim 1, it is characterized in that being formulated as of No. 1 agent: sodium polyacrylate is added deionized water with 1: 20 mixed, after soaking 12 hours, add residue deionized water, Rhizoma Polygoni Cuspidati, Flos Caryophylli, monoethanolamine, disodiumedetate, sodium sulfite, stirring is heated to 70 ℃, keeps 20 minutes, is cooled to room temperature, the repeated hydrogenation amine-oxides gets No. 1 agent after check, the fill; Being formulated as of No. 2 agent: in a container, add earlier 60% deionized water, addition polymerization acrylic acid sodium, Rhizoma Belamcandae, Flos Caryophylli, heat, be incubated 15 minutes to 70 ℃, be cooled to 40 ℃, in No. two containers, add the deionized water of residue 40% then, be heated to 40 ℃, oxine sulfate is added, be stirred to fully dissolving, slowly add in container, be cooled to 30 ℃, add hydrogen peroxide again, get No. 2 agent after stirring, check, the fill.
CN 200510026615 2005-06-09 2005-06-09 Reddish brown Chinese traditional medicine dyestuff hair dye using cloves as penetrating agent Pending CN1698575A (en)

Priority Applications (1)

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CN 200510026615 CN1698575A (en) 2005-06-09 2005-06-09 Reddish brown Chinese traditional medicine dyestuff hair dye using cloves as penetrating agent

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN 200510026615 CN1698575A (en) 2005-06-09 2005-06-09 Reddish brown Chinese traditional medicine dyestuff hair dye using cloves as penetrating agent

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CN1698575A true CN1698575A (en) 2005-11-23

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Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103006514A (en) * 2012-12-31 2013-04-03 周垂虎 Rapid vegetal hair dyeing agent integrating washing with dyeing
CN105769660A (en) * 2016-03-10 2016-07-20 蚌埠团结日用化学有限公司 Chinese herbal hair dye and preparation method thereof

Cited By (2)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN103006514A (en) * 2012-12-31 2013-04-03 周垂虎 Rapid vegetal hair dyeing agent integrating washing with dyeing
CN105769660A (en) * 2016-03-10 2016-07-20 蚌埠团结日用化学有限公司 Chinese herbal hair dye and preparation method thereof

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