CN1669987A - Gemstone ceramic sintering agent and method for manufacturing gemstone ceramic products - Google Patents
Gemstone ceramic sintering agent and method for manufacturing gemstone ceramic products Download PDFInfo
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- CN1669987A CN1669987A CN 200510020205 CN200510020205A CN1669987A CN 1669987 A CN1669987 A CN 1669987A CN 200510020205 CN200510020205 CN 200510020205 CN 200510020205 A CN200510020205 A CN 200510020205A CN 1669987 A CN1669987 A CN 1669987A
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- gemstone
- ceramic
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- sintering agent
- manufacture method
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- C—CHEMISTRY; METALLURGY
- C03—GLASS; MINERAL OR SLAG WOOL
- C03C—CHEMICAL COMPOSITION OF GLASSES, GLAZES OR VITREOUS ENAMELS; SURFACE TREATMENT OF GLASS; SURFACE TREATMENT OF FIBRES OR FILAMENTS MADE FROM GLASS, MINERALS OR SLAGS; JOINING GLASS TO GLASS OR OTHER MATERIALS
- C03C3/00—Glass compositions
- C03C3/04—Glass compositions containing silica
- C03C3/062—Glass compositions containing silica with less than 40% silica by weight
- C03C3/07—Glass compositions containing silica with less than 40% silica by weight containing lead
- C03C3/072—Glass compositions containing silica with less than 40% silica by weight containing lead containing boron
- C03C3/074—Glass compositions containing silica with less than 40% silica by weight containing lead containing boron containing zinc
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- Chemical & Material Sciences (AREA)
- Life Sciences & Earth Sciences (AREA)
- Engineering & Computer Science (AREA)
- Chemical Kinetics & Catalysis (AREA)
- General Chemical & Material Sciences (AREA)
- Geochemistry & Mineralogy (AREA)
- Materials Engineering (AREA)
- Organic Chemistry (AREA)
- Compositions Of Oxide Ceramics (AREA)
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Abstract
The invention discloses a jewel ceramic agglutinant which comprises (by weight ratio) borax 60-75 parts, silicon dioxide 4-8 parts, zinc oxide 5-11 parts, lead oxide 12-20 parts, its preparation process comprises the steps of proportioning, sintering, grinding and blending.
Description
[technical field]
The present invention relates to the ceramic process field, be specifically related to gemstone ceramic sintering agent and with the manufacture method of gemstone ceramic products.
[background technology]
Ceramic process is a traditional manufacturing technology with long history, along with the raising of living standards of the people, also has higher requirement not only to the quality and the performance of ceramic product, and to its aesthetic property.If can produce a kind ofly with hard mass bedecked with jewels and the handicraft that combines together of pottery, will be a much progress of ceramic decoration technical field.
[summary of the invention]
The technical problem to be solved in the present invention provides a kind of gemstone ceramic sintering agent, makes it possible to hard mass and ceramic post sintering are integral and fire the method for gemstone ceramic products.
In order to solve the problems of the technologies described above, the technical solution used in the present invention is: gemstone ceramic sintering agent, comprise borax, silicon-dioxide, zinc oxide and plumbous oxide, the part by weight of each component is 60～75 parts of boraxs, 4～8 parts of silicon-dioxide, 5～11 parts in zinc oxide, 12～20 parts in plumbous oxide.
Preferably, the part by weight of each component is 70 parts of boraxs, 6 parts of silicon-dioxide, 8 parts in zinc oxide, 16 parts in plumbous oxide.
The present invention also provides the manufacture method of above-mentioned gemstone ceramic sintering agent, may further comprise the steps:
1) borax, silicon-dioxide, zinc oxide and plumbous oxide are mixed by aforementioned part by weight;
2) said mixture being sintered into piece pulverizes again;
Preferably, in step 2) also add an amount of water and thickening material furnishing pasty state in the product that makes.
Preferably, described incinerating temperature is 1100～1300 degrees centigrade.
The present invention also provides the manufacture method of gemstone ceramic products, may further comprise the steps:
1) aforementioned/gemstone ceramic sintering agent of making is spread upon respectively on the bond area of hard mass and ceramic;
2) treat after gemstone ceramic sintering agent solidifies the bond area of hard mass and ceramic to be sticked;
3) with step 2) goods that obtain put into kiln and burn to the vitreous of jewel ceramic sintering agent.
Preferably, described hard mass is to be lower than 6*10 by coefficient of linear thermal expansion
-6The silicon boron glass of/C makes.
Preferably, aluminium content is higher than 5% in the porcelain mud of described ceramic.
Preferably, the temperature of described gemstone ceramic sintering agent vitreous is 680～800 degrees centigrade.
More preferably, the temperature of described gemstone ceramic sintering agent vitreous is 720～750 degrees centigrade.
Adopt technique scheme, beneficial technical effects of the present invention is: 1) to adopt above-mentioned prescription to have high temperature resistant for agglutinant of the present invention, acid and alkali-resistance, water tolerance, impact-resistant good characteristic, chemical stability and burn till after mechanical property all quite good, hard mass and ceramic can be combined closely, play splendid decorative effect; 2) the agglutinant powder is added into an amount of water and the more convenient use of thickening material furnishing pasty state, and Powdered agglutinant is more convenient for preserving, and can agglutinant powder furnishing pasty state be smeared in use again; 3) manufacture method of agglutinant and gemstone ceramic products is all very simple, and technical process all can be adopted existing installation, and realizing increases additional cost easily hardly; 4) select for use the ceramic of high aluminium content (being higher than 5%) can increase the rigidity of pottery, avoid in sintering process, occurring by the internal stress influence of glass and the situation of explosion improves yield rate; 5) select that coefficient of linear thermal expansion is low (to be lower than 6*10 for use
-6The hard mass that/C) silicon boron glass makes makes its coefficient of expansion and pottery more approaching, more easy-sintering.
[embodiment]
Embodiment one, a kind of gemstone ceramic sintering agent comprise borax, silicon-dioxide, zinc oxide and plumbous oxide, and the part by weight of each component is 70 parts of boraxs, 6 parts of silicon-dioxide, 8 parts in zinc oxide, 16 parts in plumbous oxide.
The manufacture method of gemstone ceramic sintering agent among embodiment two, the embodiment one may further comprise the steps:
1) borax, silicon-dioxide, zinc oxide and the plumbous oxide part by weight by 70 parts, 6 parts, 8 parts, 16 parts is mixed;
2) said mixture being fired to into piece under 1200 degrees centigrade pulverizes again;
3) adding part by weight is 30 parts water and 1～1.5 part sodium carboxymethyl cellulose thickener (being commonly called as cmc sodium), and stirring promptly obtains finished product.
In the above-described embodiments, it is in order to make each component thorough mixing and change its original crystal form on molecular scale that raw mix is carried out high-temperature calcination, and its temperature all is to select preferably between 1100～1300 degrees centigrade.
The manufacture method of embodiment three, a kind of gemstone ceramic products may further comprise the steps:
Material is prepared:
A, employing prior art are with silicon boron glass high temperature die cast, and through making hard mass after the deep processing steps such as polishing, polishing, advance and retreat stove tempering, described silicon boron glass selects for use coefficient of linear thermal expansion to be lower than 6*10 again
-6The kind of/C.
B, with ceramic oven dry, and clean its surface, described ceramic selects that aluminium content is higher than 5% kind in the porcelain mud for use;
Technical process:
1) gemstone ceramic sintering agent that makes among the embodiment two is spread upon respectively on the bond area of hard mass and ceramic;
2) treat that gemstone ceramic sintering agent curing back (under 5～35 degrees centigrade room temperature, approximately needing 3～5 hours) sticks the bond area of hard mass and ceramic;
3) with step 2) goods that obtain put into kiln and burn to the vitreous of jewel ceramic sintering agent, and the temperature of described gemstone ceramic sintering agent vitreous is 750 degrees centigrade; Temperature-rise period can adopt 100 degrees centigrade the speed of per hour raising.750 degrees centigrade of insulations 2 hours, can make the gemstone ceramic sintering agent vitreous, the gemstone ceramic products that obtains burning till.
In the above-described embodiments, the curing of gemstone ceramic sintering agent is preferably under 5～35 degrees centigrade the room temperature range to be carried out, and temperature is spent the end and then is difficult to solidify, and temperature is too high then can the too fast agglutinant density that causes of moisture evaporation to be reduced; The mode of employing stepping heats up and can avoid the destruction of material internal stress as far as possible in sintering process, improves the quality of product; The temperature of burning till all is to select preferably between 680～800 degrees centigrade, and particularly 720～750 degrees centigrade of these scopes can access fabulous sintering effect.
Claims (10)
1, gemstone ceramic sintering agent is characterized in that: contain borax, silicon-dioxide, zinc oxide and plumbous oxide, the part by weight of each component is 60～75 parts of boraxs, 4～8 parts of silicon-dioxide, 5～11 parts in zinc oxide, 12～20 parts in plumbous oxide.
2, gemstone ceramic sintering agent according to claim 1 is characterized in that: the part by weight of each component is 70 parts of boraxs, 6 parts of silicon-dioxide, 8 parts in zinc oxide, 16 parts in plumbous oxide.
3, the manufacture method of claim 1 or 2 described gemstone ceramic sintering agents may further comprise the steps:
1) borax, silicon-dioxide, zinc oxide and plumbous oxide are mixed by described part by weight;
2) said mixture being sintered into piece pulverizes again.
4, the manufacture method of gemstone ceramic sintering agent according to claim 3 is characterized in that: in step 2) also add an amount of water and thickening material furnishing pasty state in the product that makes.
5, the manufacture method of gemstone ceramic sintering agent according to claim 3 is characterized in that: described incinerating temperature is 1100～1300 degrees centigrade.
6, the manufacture method of gemstone ceramic products may further comprise the steps:
1) gemstone ceramic sintering agent is spread upon respectively on the bond area of hard mass and ceramic;
2) treat after gemstone ceramic sintering agent solidifies the bond area of hard mass and ceramic to be sticked;
3) with step 2) goods that obtain put into kiln and burn to the vitreous of jewel ceramic sintering agent.
7, the manufacture method of gemstone ceramic products according to claim 6 is characterized in that: described hard mass is to be lower than 6*10 by coefficient of linear thermal expansion
-6The silicon boron glass of/C makes.
8, the manufacture method of gemstone ceramic products according to claim 6 is characterized in that: aluminium content is higher than 5% in the porcelain mud of described ceramic.
9, according to the manufacture method of any described gemstone ceramic products of claim 6～9, it is characterized in that: the temperature of described gemstone ceramic sintering agent vitreous is 680～800 degrees centigrade.
10, the manufacture method of gemstone ceramic products according to claim 9 is characterized in that: the temperature of described gemstone ceramic sintering agent vitreous is 720～750 degrees centigrade.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100202057A CN1319886C (en) | 2005-01-12 | 2005-01-12 | Gemstone ceramic sintering agent and method for manufacturing gemstone ceramic products |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2005100202057A CN1319886C (en) | 2005-01-12 | 2005-01-12 | Gemstone ceramic sintering agent and method for manufacturing gemstone ceramic products |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1669987A true CN1669987A (en) | 2005-09-21 |
| CN1319886C CN1319886C (en) | 2007-06-06 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2005100202057A Expired - Fee Related CN1319886C (en) | 2005-01-12 | 2005-01-12 | Gemstone ceramic sintering agent and method for manufacturing gemstone ceramic products |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104418585A (en) * | 2013-08-29 | 2015-03-18 | 孙即杰 | High-temperature molding process for ceramic and colored glaze |
| CN106476117A (en) * | 2016-10-10 | 2017-03-08 | 东莞华晶粉末冶金有限公司 | A kind of method inlaying sapphire glass in zirconia ceramicss |
| CN108623321A (en) * | 2017-03-15 | 2018-10-09 | 东莞华晶粉末冶金有限公司 | The preparation method of ceramics-glass multiple device |
| CN109422542A (en) * | 2017-08-23 | 2019-03-05 | 金宇 | Glass and Ceramic bond product manufacture |
Family Cites Families (2)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1014202B (en) * | 1987-06-25 | 1991-10-09 | 亚历山大·西门诺维奇·布卡托夫 | Artificial heart valves |
| CN1013624B (en) * | 1989-11-11 | 1991-08-21 | 复旦大学 | Prodn. method of high-efficiency vacuum ultraviolet source |
-
2005
- 2005-01-12 CN CNB2005100202057A patent/CN1319886C/en not_active Expired - Fee Related
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN104418585A (en) * | 2013-08-29 | 2015-03-18 | 孙即杰 | High-temperature molding process for ceramic and colored glaze |
| CN106476117A (en) * | 2016-10-10 | 2017-03-08 | 东莞华晶粉末冶金有限公司 | A kind of method inlaying sapphire glass in zirconia ceramicss |
| CN108623321A (en) * | 2017-03-15 | 2018-10-09 | 东莞华晶粉末冶金有限公司 | The preparation method of ceramics-glass multiple device |
| CN109422542A (en) * | 2017-08-23 | 2019-03-05 | 金宇 | Glass and Ceramic bond product manufacture |
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| Publication number | Publication date |
|---|---|
| CN1319886C (en) | 2007-06-06 |
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Granted publication date: 20070606 Termination date: 20120112 |