CN1655652A - Method of making electric-heating film PTC heating devices - Google Patents

Method of making electric-heating film PTC heating devices Download PDF

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Publication number
CN1655652A
CN1655652A CN 200410015334 CN200410015334A CN1655652A CN 1655652 A CN1655652 A CN 1655652A CN 200410015334 CN200410015334 CN 200410015334 CN 200410015334 A CN200410015334 A CN 200410015334A CN 1655652 A CN1655652 A CN 1655652A
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Prior art keywords
ceramic substrate
radiant heating
heating film
electric radiant
manufacture method
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CN 200410015334
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CN100474983C (en
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郜长福
陈闻杰
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SHENZHEN JINKE SPECIAL MATERIALS CO Ltd
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Individual
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Abstract

This invention relates to electric heating film PTC device process method, which is characterized by comprising the following steps: adopting streamline shaped ceramic green compact as upper ceramic base board and down ceramic base board by use of materials of alumina and aluminium nitride; electric heating film plasm wire net printing, heat rolling and glue drainage with temperature of 60-120 DEG C and pressure of 50-300kg.cm-2,sintering and connection with temperature of 1500-1700 DEG C ; wherein the said plasm is made of tungsten powder or molybdenum and manganese powder of 90%-99% with glass powder of 1%-10% by their proportion of 10:1-1:1.

Description

The manufacture method of Electric radiant Heating Film PTC heater spare
Technical field:
The present invention relates to a kind of manufacture method of Electric radiant Heating Film PTC heater spare, it belongs to a kind of manufacture method of electric heating device.
Background technology:
At present, the electrothermal film heater spare of making of metal, semiconductor or other composite materials in the prior art is of a great variety.In these electrothermal film heater spares, important composition part Electric radiant Heating Film wherein is because the defective of processing technology, the main problem that exists is that temperature can not be from limit, the energising back is under additional not external temperature control equipment situation, temperature can continue to be elevated to more than 700 degree, use safety inadequately, can not stablize lasting work simultaneously.There is potential safety hazard in the failure phenomenon that particularly is short-circuited easily under oxidizing atmosphere or wet environment." a kind of manufacture method of novel heating original paper " disclosed in No. the 03114238.9th, the Chinese patent, a kind of manufacture method of making electrothermal film heater is provided in this technical scheme, the electrothermal film heater that this method is made, because what adopt in this method is the technical scheme that the ceramic post sintering auxiliary agent bonds together ceramic wafer, therefore, combination under the electrothermal film heater that the manufactures state at high temperature between the ceramic wafer can be easy to destroyed, can not work lastingly, failure phenomenon easily is short-circuited under oxidizing atmosphere or wet environment.
Summary of the invention:
The object of the present invention is to provide a kind of good seal performance, the bond strength height can be worked lastingly, the manufacture method of safe and reliable Electric radiant Heating Film PTC heater spare.
The object of the present invention is achieved like this:
A kind of manufacture method of Electric radiant Heating Film PTC heater spare is characterized in that it comprises following processing step:
A: select to adopt with aluminium oxide or aluminium nitride be ceramic green behind the raw material flow casting molding as ceramic substrate, ceramic substrate divides goes up ceramic substrate and following ceramic substrate;
B: Electric radiant Heating Film slip silk screen printing
Add the raw material of glass powder as the electric heating thick film in tungsten powder, wherein tungsten powder is 90%~99%, and glass powder is 1%~10%, goes into adhesive with 10: 1~1: 1 mixed then and makes the Electric radiant Heating Film slip; Adopt the mode of contact printing to be printed on down on the ceramic substrate green compact in the Electric radiant Heating Film slurry; 150~400 order silk screens are adopted in printing; And from the electric heating thick film, draw the identical electrode of material simultaneously.
C: hot pressing
Last ceramic substrate green compact and the following ceramic substrate green compact that printed the Electric radiant Heating Film slurry are accurately carried out hot pressing behind the location, and hot pressing temperature is generally 60~120 ℃, and pressure is 50~300kgcm -2
D: binder removal
Ceramic green after the hot pressing is put into the stove binder removal, and programming rate is per hour 20 ℃~50 ℃, be raised to 250 ℃~650 ℃ after, be incubated 2~6 hours;
E: sintering
Ceramic green behind the binder removal is put into the stove sintering, and 1500~1700 ℃ of sintering temperatures become as a whole with upper and lower ceramic substrate green sintering.
F: connect
On electrode, connect lead, be connected by soldering, seal silver paste or the method for electroplating the back sintering between lead and the electrode.
Select 50%~90% molybdenum manganese mixed powder as the Electric radiant Heating Film raw material in the silk screen printing of described Electric radiant Heating Film slip, add 10%~50% glass powder, then with 10: 1-1: 1 ratio is mixed with adhesive.
The molybdenum powder in described molybdenum manganese mixed powder and the ratio of manganese powder are 9: 1-3: 1.
Described glass powder is the mixed powder that comprises aluminium oxide, calcium oxide, magnesium oxide, silica, yittrium oxide, and described adhesive is to comprise the contract adhesive of butyl ester, O-phthalic ester dibutyl ester, n-butanol, trichloroethylene, tetrachloro-ethylene, ethanol, nitroglycerine composition of polyvinyl alcohol.
The ceramic green surfacing of flow casting molding, thickness is at 0.2~2.0mm.
The described ceramic substrate of going up leaves two or more breach, and gap position is over against the electrode leads to client of following ceramic substrate;
Described ceramic substrate and the following ceramic substrate gone up is characterized in that described ceramic substrate can be the slab construction of different shapes such as circle is oval or square.
Described as last ceramic substrate and following ceramic substrate raw material aluminium oxide or aluminium nitride at content behind the sintering more than 90%.
The electric heating thick film live width that is printed on down on the ceramic substrate is 0.2~2mm, the spacing 0.2~5mm between line and the line.
Describedly be printed on down electric heating thick film line on the ceramic substrate to be the continuous lines that equally spaced pectination is arranged.
Describedly be printed on down electric heating thick film line on the ceramic substrate to be the continuous lines that density pectination is at interval arranged.
Describedly be printed on down electric heating thick film line on the ceramic substrate to be the continuous lines that parallel concentric circles is arranged.
Described electrode of drawing from Electric radiant Heating Film can be two or more.
Described lead adopts nickel wire or copper cash high temperature wire.
Technological process of the present invention is simple, has solved in the prior art the easy ruined defective of the combination between the ceramic wafer under the existing state at high temperature.The Electric radiant Heating Film PTC heater spare good seal performance of utilizing the present invention to manufacture, the bond strength height can be worked lastingly, and is safe and reliable.
Description of drawings:
Accompanying drawing 1 is one of the wiring form of electric heating thick film on the ceramic substrate under the present invention
Accompanying drawing 2 is the structural representation of ceramic substrate in the present invention
Accompanying drawing 3 is two of the wiring form of electric heating thick film on the ceramic substrate under the present invention
Accompanying drawing 4 is two of the structural representation of ceramic substrate in the present invention
Accompanying drawing 5 is three of the wiring form of electric heating thick film on the ceramic substrate under the present invention
Accompanying drawing 6 is three of the structural representation of ceramic substrate in the present invention
Embodiment:
Embodiment 1:
At first utilize the green compact casting technique to make the ceramic substrate green compact: in the aluminium oxide ceramics powder, add suitable adhesive, as the employed aluminium oxide requirement of last ceramic substrate and following ceramic substrate raw material behind sintering content 96%.Form highly viscous slurry through behind the ball mill mixing.With the thickness of the scraper control cast layer that is positioned at the conveyer belt top, certain thickness slurry just was evenly distributed on the carrier band when conveyer belt moved.After oven dry under 100 ℃ of temperature, can be standby.This technology is prior art.The surfacing of described ceramic substrate green compact, thickness are 0.8mm.As shown in attached Fig. 1 and 2, ceramic substrate green compact in the present embodiment are rectangle structure, leave three breach 6 or leave two breach at last ceramic substrate 4, gap position can expose electrode leads to client over against the exit of the electrode 2 of following ceramic substrate 3 after upper and lower ceramic substrate sinters integral body into.As shown in accompanying drawing 2 and accompanying drawing 4.
The silk screen printing of Electric radiant Heating Film slip:
At first make the Electric radiant Heating Film slip: in tungsten powder, add the raw material of glass powder as the electric heating thick film, wherein tungsten powder is 95%, and glass powder is 5%, is mixed into adhesive then in raw material, the raw material of electric heating thick film and the ratio of adhesive are 2: 1, make the Electric radiant Heating Film slip.Described glass powder is the mixed powder that comprises aluminium oxide, calcium oxide, magnesium oxide, silica, yittrium oxide, described adhesive be comprise polyvinyl alcohol contract butyl ester, O-phthalic ester dibutyl ester, n-butanol, trichloroethylene, tetrachloro-ethylene, ethanol, nitroglycerine composition solvent type adhesive or add water-soluble binder.Glass powder and adhesive constitute prior art.
Adopt the mode of contact printing to be printed on down on the ceramic substrate green compact in the Electric radiant Heating Film slurry then; 300 order silk screens are adopted in printing; And from the electric heating thick film, draw the identical electrode of material simultaneously.Electric heating thick film 5 live widths that are printed on down on the ceramic substrate are 0.5mm, the spacing 2mm between line and the line.The described electric heating thick film line 5 that is printed on down on the ceramic substrate 3 is continuous lines that equally spaced pectination is arranged, as shown in accompanying drawing 1, or the continuous lines 7 of density pectination arrangement at interval, as shown in accompanying drawing 3.Also from the electric heating thick film, draw the identical electrode of material 2 simultaneously simultaneously.The electrode of drawing from Electric radiant Heating Film can be three, as shown in accompanying drawing 1, includes zero line and live wire.The electrode of drawing from Electric radiant Heating Film can be two, as shown in accompanying drawing 3
Hot pressing: the following ceramic substrate green compact that will go up the ceramic substrate green compact and print the electric heating slurry accurately carry out hot pressing behind the location, and hot pressing temperature is generally 100 ℃, and pressure is 100kgcm -2
Binder removal: the ceramic substrate green compact after the hot pressing are put into the stove binder removal, and programming rate is per hour 30 ℃, be raised to 600 ℃ after, be incubated 2 hours.
Sintering: the ceramic green behind the binder removal is put into the stove sintering, and 1600 ℃ of sintering temperatures become as a whole with upper and lower ceramic substrate green sintering.
Connect: connect lead 1 on electrode, the method by sintering after soldering, seal silver paste or the plating between lead 1 and the electrode 2 is connected.Described lead can adopt nickel wire or copper cash high temperature wire.
The Electric radiant Heating Film PTC heater spare that uses above-mentioned technology to make has ptc characteristics, and promptly when temperature raise, its resistance can increase.
Embodiment 2:
At first select to adopt with the aluminium nitride be ceramic green behind the raw material flow casting molding as ceramic substrate, as last ceramic substrate and the employed aluminium nitride requirement of following ceramic substrate raw material behind sintering content 94%.Ceramic substrate green compact in the present embodiment are circular slab construction, leave two breach at last ceramic substrate 4, and gap position is over against the exit of the electrode 2 of following ceramic substrate 3, as shown in accompanying drawing 5 and accompanying drawing 6.The surfacing of described ceramic substrate green compact, thickness are 1.0mm
In the present embodiment, in the silk screen printing of described Electric radiant Heating Film slip, select 60% molybdenum manganese mixed powder, add 40% glass powder, mix with adhesive with 4: 1 ratio then as the Electric radiant Heating Film raw material.The molybdenum powder in described molybdenum manganese mixed powder and the ratio of manganese powder are 5: 1.The described electric heating thick film line 8 that is printed on down on the ceramic substrate is continuous lines of arranging with parallel concentric circles, and electric heating thick film 8 live widths are 0.9mm.250 order silk screens are adopted in printing.
Hot pressing: the following ceramic substrate green compact that will go up the ceramic substrate green compact and print the Electric radiant Heating Film slurry accurately carry out hot pressing behind the location, and hot pressing temperature is generally 120 ℃, and pressure is 300kgcm -2
Binder removal: the ceramic green after the hot pressing is put into the stove binder removal, and programming rate is per hour 50 ℃, after 650 ℃, is incubated 5 hours.
Sintering: the ceramic green behind the binder removal is put into the stove sintering, and 1500 ℃ of sintering temperatures become as a whole with upper and lower ceramic substrate green sintering.
Other processing steps of present embodiment are identical with embodiment 1 with parameter.

Claims (13)

1, a kind of manufacture method of Electric radiant Heating Film PTC heater spare is characterized in that it comprises following processing step:
A: select to adopt with aluminium oxide or aluminium nitride be ceramic green behind the raw material flow casting molding as ceramic substrate, ceramic substrate divides goes up ceramic substrate and following ceramic substrate;
B: Electric radiant Heating Film slip silk screen printing
Add the raw material of glass powder as the electric heating thick film in tungsten powder, wherein tungsten powder is 90%~99%, and glass powder is 1%~10%, goes into adhesive with 10: 1~1: 1 mixed then and makes the Electric radiant Heating Film slip; Adopt the mode of contact printing to be printed on down on the ceramic substrate green compact in the Electric radiant Heating Film slurry; 150~400 order silk screens are adopted in printing; And from the electric heating thick film, draw the identical electrode of material simultaneously.
C: hot pressing
Last ceramic substrate green compact and the following ceramic substrate green compact that printed the Electric radiant Heating Film slurry are accurately carried out hot pressing behind the location, and hot pressing temperature is generally 60~120 ℃, and pressure is 50~300kgcm -2
D: binder removal
Ceramic green after the hot pressing is put into the stove binder removal, and programming rate is per hour 20 ℃~50 ℃, be raised to 250 ℃~650 ℃ after, be incubated 2~6 hours;
E: sintering
Ceramic green behind the binder removal is put into the stove sintering, and 1500~1700 ℃ of sintering temperatures become as a whole with upper and lower ceramic substrate green sintering.
F: connect
On electrode, connect lead, be connected by soldering, seal silver paste or the method for electroplating the back sintering between lead and the electrode.
2, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 1, it is characterized in that in the silk screen printing of described Electric radiant Heating Film slip, selecting 50%~90% molybdenum manganese mixed powder as the Electric radiant Heating Film raw material, the glass powder of adding 10%~50%, then with 10: 1-1: 1 ratio is mixed with adhesive.
3, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 2 is characterized in that the molybdenum powder in described molybdenum manganese mixed powder and the ratio of manganese powder are 9: 1-3: 1.
4, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 1 or 2, it is characterized in that described glass powder is the mixed powder that comprises aluminium oxide, calcium oxide, magnesium oxide, silica, yittrium oxide, described adhesive is to comprise the contract adhesive of butyl ester, O-phthalic ester dibutyl ester, n-butanol, trichloroethylene, tetrachloro-ethylene, ethanol, nitroglycerine composition of polyvinyl alcohol.
5, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 1 or 2 is characterized in that the ceramic green surfacing of flow casting molding, and thickness is at 0.2~2.0mm; The described ceramic substrate of going up leaves two or more breach, and gap position is over against the electrode leads to client of following ceramic substrate;
6, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 5 is characterized in that described ceramic substrate and the following ceramic substrate gone up, and it is characterized in that described ceramic substrate can be the slab construction of different shapes such as circle is oval or square.
7, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 1 or 2, it is characterized in that described as last ceramic substrate and following ceramic substrate raw material aluminium oxide or aluminium nitride at content behind the sintering more than 90%.
8, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 1 or 2, the electric heating thick film live width that it is characterized in that being printed on down on the ceramic substrate is 0.2~2mm, the spacing 0.2~5mm between line and the line.
9, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 8 is characterized in that describedly being printed on down electric heating thick film line on the ceramic substrate to be the continuous lines that equally spaced pectination is arranged.
10, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 8 is characterized in that describedly being printed on down electric heating thick film line on the ceramic substrate to be the continuous lines that density pectination is at interval arranged.
11, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 8 is characterized in that describedly being printed on down electric heating thick film line on the ceramic substrate to be the continuous lines that parallel concentric circles is arranged.
12, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 1 or 2 is characterized in that described electrode of drawing can be two or more from Electric radiant Heating Film.
13, the manufacture method of the Electric radiant Heating Film PTC heater spare described in claim 1 or 2 is characterized in that described lead adopts nickel wire or copper cash high temperature wire.
CNB2004100153342A 2004-02-13 2004-02-13 Method for fabricating electric-heating film PTC heating devices Expired - Fee Related CN100474983C (en)

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Cited By (20)

* Cited by examiner, † Cited by third party
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CN100499944C (en) * 2007-10-01 2009-06-10 卫民 A making technology for thick film electric heater
CN100544525C (en) * 2006-01-09 2009-09-23 潘国章 A kind of electro-thermal film ceramic heating element of hot-air fan and preparation method thereof
CN101871635A (en) * 2010-06-23 2010-10-27 浙江晶皓光电科技有限公司 Heat-conducting medium for LED lamps and manufacturing method thereof
CN102065588A (en) * 2010-11-15 2011-05-18 中山市格普斯纳米电热科技有限公司 Ceramic heating plate and manufacturing method thereof
CN102155750A (en) * 2011-04-21 2011-08-17 浙江苏泊尔家电制造有限公司 Electromagnetic oven and manufacturing method thereof
CN102215609A (en) * 2011-04-21 2011-10-12 王亚奇 Internal heating reinforced composite board connected through hot-melt dry film
CN101118089B (en) * 2007-07-17 2011-12-14 巫嘉雄 Combining method of heaters and structure thereof
CN101321415B (en) * 2008-07-14 2011-12-21 佛山市海辰科技有限公司 Rare earth thick film circuit electrical heating element based on aluminum nitride minicrystal ceramic substrates and its preparation technique
CN101616511B (en) * 2009-04-16 2012-05-23 珠海粤科京华电子陶瓷有限公司 Preparation method of ceramic heating element
CN103077780A (en) * 2013-01-11 2013-05-01 深圳顺络电子股份有限公司 Production method of a thick-electrode conductor device
CN103604157A (en) * 2013-11-19 2014-02-26 浙江荣荣实业有限公司 Heat conducting plate of heating radiator
CN103874244A (en) * 2014-03-27 2014-06-18 福建闽航电子有限公司 Ceramic heating plate
CN103874245A (en) * 2014-03-27 2014-06-18 福建闽航电子有限公司 Bonding pad structure of ceramic heating piece with temperature control
CN103874243A (en) * 2014-03-27 2014-06-18 福建闽航电子有限公司 Temperature-control ceramic heating piece
CN103957613A (en) * 2014-03-27 2014-07-30 西安理工大学 Preparing method for high-temperature resistant metal/ceramic composite heating unit material
CN104245262A (en) * 2011-11-30 2014-12-24 部件再设计股份有限公司 Method for joining materials and plate and shaft device and multi-layer plate formed therewith
CN106882967A (en) * 2017-02-16 2017-06-23 北京钢研新冶精特科技有限公司 A kind of hot-pressing sintering method of the ceramic body containing built-in electrode
CN108263080A (en) * 2016-12-30 2018-07-10 上海烟草集团有限责任公司 The processing unit (plant) and processing method of calandria
CN108658605A (en) * 2018-05-24 2018-10-16 深圳市商德先进陶瓷股份有限公司 Heating device and its preparation method and application
CN110740532A (en) * 2019-11-12 2020-01-31 珠海格力电器股份有限公司 heating assembly, preparation method thereof and kitchen appliance

Cited By (25)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN100544525C (en) * 2006-01-09 2009-09-23 潘国章 A kind of electro-thermal film ceramic heating element of hot-air fan and preparation method thereof
CN101118089B (en) * 2007-07-17 2011-12-14 巫嘉雄 Combining method of heaters and structure thereof
CN100499944C (en) * 2007-10-01 2009-06-10 卫民 A making technology for thick film electric heater
CN101321415B (en) * 2008-07-14 2011-12-21 佛山市海辰科技有限公司 Rare earth thick film circuit electrical heating element based on aluminum nitride minicrystal ceramic substrates and its preparation technique
CN101616511B (en) * 2009-04-16 2012-05-23 珠海粤科京华电子陶瓷有限公司 Preparation method of ceramic heating element
CN101871635A (en) * 2010-06-23 2010-10-27 浙江晶皓光电科技有限公司 Heat-conducting medium for LED lamps and manufacturing method thereof
CN102065588A (en) * 2010-11-15 2011-05-18 中山市格普斯纳米电热科技有限公司 Ceramic heating plate and manufacturing method thereof
CN102155750A (en) * 2011-04-21 2011-08-17 浙江苏泊尔家电制造有限公司 Electromagnetic oven and manufacturing method thereof
CN102215609A (en) * 2011-04-21 2011-10-12 王亚奇 Internal heating reinforced composite board connected through hot-melt dry film
CN102155750B (en) * 2011-04-21 2015-09-09 浙江苏泊尔家电制造有限公司 A kind of electromagnetic oven and this electromagnetic oven manufacture method
CN104245262A (en) * 2011-11-30 2014-12-24 部件再设计股份有限公司 Method for joining materials and plate and shaft device and multi-layer plate formed therewith
CN103077780A (en) * 2013-01-11 2013-05-01 深圳顺络电子股份有限公司 Production method of a thick-electrode conductor device
CN103604157B (en) * 2013-11-19 2016-08-17 浙江荣荣实业有限公司 A kind of radiator heat-conducting plate
CN103604157A (en) * 2013-11-19 2014-02-26 浙江荣荣实业有限公司 Heat conducting plate of heating radiator
CN103874243A (en) * 2014-03-27 2014-06-18 福建闽航电子有限公司 Temperature-control ceramic heating piece
CN103957613A (en) * 2014-03-27 2014-07-30 西安理工大学 Preparing method for high-temperature resistant metal/ceramic composite heating unit material
CN103874245A (en) * 2014-03-27 2014-06-18 福建闽航电子有限公司 Bonding pad structure of ceramic heating piece with temperature control
CN103874244A (en) * 2014-03-27 2014-06-18 福建闽航电子有限公司 Ceramic heating plate
CN103874243B (en) * 2014-03-27 2016-06-01 福建闽航电子有限公司 The ceramic heating plate of a kind of band temperature control
CN108263080A (en) * 2016-12-30 2018-07-10 上海烟草集团有限责任公司 The processing unit (plant) and processing method of calandria
CN106882967A (en) * 2017-02-16 2017-06-23 北京钢研新冶精特科技有限公司 A kind of hot-pressing sintering method of the ceramic body containing built-in electrode
CN106882967B (en) * 2017-02-16 2019-08-23 北京钢研新冶精特科技有限公司 A kind of hot-pressing sintering method of the ceramic body containing built-in electrode
CN108658605A (en) * 2018-05-24 2018-10-16 深圳市商德先进陶瓷股份有限公司 Heating device and its preparation method and application
CN110740532A (en) * 2019-11-12 2020-01-31 珠海格力电器股份有限公司 heating assembly, preparation method thereof and kitchen appliance
CN110740532B (en) * 2019-11-12 2024-08-16 珠海格力电器股份有限公司 Heating assembly, manufacturing method thereof and kitchen appliance

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