CN1627215A - Online optimized method for blending oil products, and system of implementing the method - Google Patents

Online optimized method for blending oil products, and system of implementing the method Download PDF

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Publication number
CN1627215A
CN1627215A CN 200410009191 CN200410009191A CN1627215A CN 1627215 A CN1627215 A CN 1627215A CN 200410009191 CN200410009191 CN 200410009191 CN 200410009191 A CN200410009191 A CN 200410009191A CN 1627215 A CN1627215 A CN 1627215A
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constant temperature
blending
oil
flow
sample
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CN1327306C (en
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李苏安
谢刚
单达彭
林立标
康明强
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ZHONGKE CHUANGYI TECH DEVELOPMENT Co Ltd
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ZHONGKE CHUANGYI TECH DEVELOPMENT Co Ltd
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Abstract

This invention provides an oil-product on-line optimized mixing method including a basic control system controlling flow of each component and an optimized control system with intelligent operation connecting to it via an interface, a sample device and a near infrared on-line analyzer analyzing the sample characterizing in including the following technological steps: before analyzing the sample by the near infrared on-line analyzer, the sample is pre-processed including a constant temperature process and water remove process. The invention also provides an oil-product on-line optimized mixing system.

Description

The method of oil product on-line optimization blending and implement the system of this method
Technical field
The present invention relates to the technology of oil product on-line optimization blending, specifically, oil products such as half-finished gasoline or diesel oil from distillate mouthful flow out after, utilize this technology just can in pipeline, be mixed into the product oil product of the various trades mark.The present invention be more particularly directed to a kind of method of oil product on-line optimization blending, and a kind of oil product on-line optimization blending system of implementing this method.
Background technology
Along with development of technology, both meet the quality standard of optimizing blending in order to reach as far as possible, satisfy the demand of production efficiency and maximizing the benefits again, advanced Blending on Line System is adopted by in the world some Oil Production enterprises.Blending on Line System has been eliminated pot type blending method in the past, has reduced intermediate link, greatly reduces production cost.The device setting of Blending on Line System has changed the old way that block is in the past cut apart, and carries out unified planning by the flow process trend, operates many covering devices with a central control room, reduce construction land, reduce investment, energy-saving and cost-reducing, convenient management has also reduced material loss simultaneously.
Oil product on-line optimization blending system of the prior art mainly comprises two control system, the basic control system of one for the flow of each component is controlled respectively, i.e. and BBC system, it is two for possessing the optimal control system of intelligent computing, i.e. APC system.Optimize and be divided into static optimization and dynamic optimization two parts, when the blending beginning, calculate prescription with static optimization earlier, prescription provides the ratio of each component oil and main flow (if gasoline then is catalytic gasoline), and the flow of catalytic gasoline is controlled by the ramp function of default, the flow that the flow of other each components just draws by its ratio is that BBC control is carried out by basis control.System's operation the time is then undertaken by dynamic optimization, by the NIR analyzer, i.e. and near infrared online analyser, on-line analysis goes out the RON of product oil, alkene, parameters such as aromatic hydrocarbons, the PID_A of APC part, PID_B, three regulating loops of PID_C are calculated RON respectively, alkene, the deviation of aromatic hydrocarbons and setting value according to the value of feedback, the principle of optimality of utilizing these deviations bases to determine is calculated adjusting working value Δ A, Δ B, the Δ C in three loops, and these working values are changed by ratio.The component flow is then regulated according to working value in each loop of BBC part, realizes blending, produces the product oil that meets quality standard.
The oil on-line blending system, advanced near infrared online analyser (being the NIR analyzer) technology and Computer Control Technology have been adopted, online NIR analyzer can provide the multichannel component, the Q factor of multichannel product oil is analyzed data, can be used for FEEDBACK CONTROL, feedforward, fault diagnosis etc., Computer Control Technology can provide open on-line optimization blending platform, can develop related service according to correlation parameter, the real online dynamic control that realizes whole process, adapt to factory's process condition complicated and changeable well, make the on-line optimization blending satisfy the every index on quality standard and the economic benefit.Using online NIR is the important control means of current realization gasoline concoction, has the fast characteristics of analysis speed, the oil product parameter of each sampling channel of timesharing analytical calculation, and compare with the target set-point respectively, as the input variable of dynamic quality controller.
But we carry out finding after the deep development test, if the sample of sending here from sampling apparatus is not carried out the pre-service of standard, just directly enter the near infrared online analyser, and so, can there be bigger error in the analysis data of acquisition.The sample of gathering all can bring influence to the indexs such as penetrance of near infrared light, thereby cause being difficult to keep from start to finish concocting the quality of product oil, and then have influence on production efficiency and economic benefit because of the moisture difference, impurity difference or the temperature difference that contain.
Summary of the invention
The present invention is directed to the technological deficiency or the deficiency that exist in the prior art, a kind of method of oil product on-line optimization blending is provided, this method can obtain the analysis data of the less collected specimens of error, thereby can help keeping from start to finish concocting the quality of product oil, and then enhance productivity and economic benefit.
The present invention also provides a kind of oil product on-line optimization blending system of implementing said method.
Technical solution of the present invention is as follows:
The method of oil product on-line optimization blending, comprise basic control system that the flow of each component is controlled respectively and by the connected optimal control system that possesses intelligent computing of interface, and sampling apparatus and near infrared online analyser that sample is analyzed, it is characterized in that comprising following processing step: enter before the near infrared online analyser analyzes at sample, described sample is carried out pre-service.
The described pre-service that sample is carried out comprises the constant temperature processing and removes water treatment.
Described constant temperature is handled and is comprised one-level constant temperature and secondary constant temperature, and described one-level constant temperature adopts 25 ℃ of constant temperature water bath devices, and described secondary constant temperature adopts the electrical heating thermostat that sample temperature is controlled to be 30 ℃.
Describedly remove water treatment and between one-level constant temperature and secondary constant temperature, carry out, comprise also that between one-level constant temperature and secondary constant temperature the removal of impurity handles.
The described optimal control system that possesses intelligent computing carries out following running program: calculate prescription with static optimization earlier when the blending beginning, prescription provides the ratio of each component oil and main flow, and main flow is controlled by the ramp function of default, and the flow of other each components is just carried out by basic control system by the flow that its ratio draws; When operation, then undertaken by dynamic optimization, by the near infrared online analyser, on-line analysis goes out the RON of product oil, alkene, the aromatic hydrocarbons parameter is calculated RON by regulating loop respectively according to the value of feedback, alkene, the deviation of aromatic hydrocarbons and setting value is utilized the adjusting working value of these deviations according to the principle of optimality calculating circuit of determining, these working values are changed by ratio; The component flow is then regulated according to working value in each loop of basis control system, realizes blending.
Described regulating loop is three, be PID_A, PID_B, three regulating loops of PID_C, the adjusting working value in corresponding three loops is Δ A, Δ B, Δ C, initial ratio A, B, the C addition of regulating working value and static optimization obtain ratio set-point A-SP, B-SP, the C-SP of new ratio as basic control system regulating loop, and the flow that the product of loop ratio set-point and main flow F-O draws is as the flow setting value in basic control system flow control circuit FIC-REF, loops such as FIC-MTBE, FIC-CYY.The basic control system of blending control system is carried out each component oil flow control according to these setting values, to reach the purpose of on-line optimization blending.
The controlled variable of described dynamic optimization comprises the tank farm stock size parameter of price parameter, each component oil properties parameter and the each component oil of each component oil.
The phylogenetic relationship between the regulated value is respectively exported in the price parameter decision of described each component oil; The size of described each component oil properties parameter decision output regulated value; The tank farm stock size parameter of described each component oil determines the output regulated value of each component.
In the described basic control system that the flow of each component is controlled respectively, every road is provided with distant place setter and local setter.
A kind of oil product on-line optimization blending system, comprise basic control system that the flow of each component is controlled respectively and by the connected optimal control system that possesses intelligent computing of interface, and sampling apparatus and near infrared online analyser that sample is analyzed, it is characterized in that: also comprise pretreatment system, this pretreatment system is provided with the constant temperature treating apparatus and removes water disposal facility, enter before the near infrared online analyser analyzes at sample, described sample is carried out pre-service.
The technology of the present invention effect is as follows:
Because the method for oil product on-line optimization blending of the present invention, entering before the near infrared online analyser analyzes, described sample is carried out pre-service, this pre-treatment step just can make sample eliminate the influence of near infrared ray being analyzed data aspect certain or some, can obtain the analysis data of the less collected specimens of error, thereby can help keeping from start to finish concocting the quality of product oil, and then enhance productivity and economic benefit.Also help simultaneously basic control system that the flow of each component is controlled respectively and by the connected normal stabilizing effective operation of optimal control system that possesses intelligent computing of interface.
Because the pre-service that sample is carried out comprises the constant temperature processing and removes water treatment, this sample of just having eliminated collection is because the influence that moisture difference that contains or temperature difference are brought the indexs such as penetrance of near infrared light, thereby help keeping from start to finish concocting the quality of product oil, the normal stabilizing effective operation of maintenance system, and then enhance productivity and economic benefit.
Comprise one-level constant temperature and secondary constant temperature because constant temperature is handled, described one-level constant temperature adopts 25 ℃ of constant temperature water bath devices, and described secondary constant temperature adopts the electrical heating thermostat that sample temperature is controlled to be 30 ℃; Describedly remove water treatment and between one-level constant temperature and secondary constant temperature, carry out, comprise also that between one-level constant temperature and secondary constant temperature the removal of impurity handles; This just helps the rational deployment of process equipment, guarantees simultaneously conscientiously sample dewatering and temperature constant state when entering the near infrared online analyser, and the state that is controlled of impurity content.
In addition, provide a series of algorithm routines that meet working condition to the optimal control system that possesses intelligent computing, this has improved the intelligent level of optimal control system widely.
Description of drawings
Fig. 1 is the online pre-service loop synoptic diagram among the present invention;
Fig. 2 is the control principle figure of oil product on-line optimization blending system of the present invention.
Embodiment
The present invention is described in further detail below in conjunction with accompanying drawing.
As shown in Figure 1, sample through the quick loop of over-sampling, is diverted to pretreatment system from quick loop from the component loop.
Through reduction valve,, uses safely oil sample pressure behind the sample inflow pretreatment system so that reducing for pretreatment system.
What the first road constant temperature used in the thermostat is a waters, and sample inlet can fully be carried out heat interchange through behind this waters, makes sample temperature can reach certain value substantially, makes the secondary thermostat can make sample reach predetermined temperature fast.Through behind the constant temperature, the result's of sample analysis stability and degree of accuracy improve, and the octane value precision that the interaction energy of constant temperature makes gasoline reaches in 0.1 from 0.3, and other majority parameters analysis precisions of oil product also can improve two to three times.
Water also has very big influence to the measuring accuracy of near-infrared analyzer, therefore sample passes through dehydrator behind one-level constant temperature, sample moisture content after the performance requirement of dehydrator is handled is lower than 5ppm, place to go water also is the assurance that guarantees the near-infrared analyzer precision to the influence of sample, because the state when the more approaching oil refining of the oil product after dehydration factory analyzes, thereby make analysis result more near actual value.The design of dehydrator is the using and the reserved, realizes two switchings between filtrator by T-valve.The post analysis result that dewaters can improve about 5% precision.
The effect of filtrator is the impurity in the oil product of place to go, to reduce absorbing the influence of near infrared spectrum to analysis result in a large number because of impurity.The design of filtrator also is the using and the reserved, switches by T-valve.
Sample is CELL among Fig. 1 through the analysis cell of having arrived behind the filtrator, analysis cell is in the constant temperature oven of secondary constant temperature, this constant temperature oven uses electrical heating to heat, and lowers the temperature by chilled water, makes the temperature of sample reach 30 ± 0.1 ℃ by the electric current of control heating apparatus and the flow of chilled water.
Outlet at analysis cell is equipped with a spinner-type flowmeter, and in order to the speed of the treated device of control sample flow, the flow velocity size should be moderate, is advisable with 60CC/Min.
Final sample flows to retracting device and finishes pre-treatment step.
Nitrogen among Fig. 1 is used for the function that pipeline cleans.
As shown in Figure 2, oil product on-line optimization blending system of the present invention is divided into APC and BBC two parts, and APC is that advanced control section is promptly optimized, and BBC is basic control section.
Optimize and be divided into static optimization and dynamic optimization two parts, when the blending beginning, calculate prescription with static optimization earlier, prescription provides the ratio of each component oil and main flow (catalytic gasoline), and the flow of catalytic gasoline is controlled by the ramp function of default, and the flow of other each components is just controlled the BBC Control Flow by the flow that its ratio draws by the basis.
System is then undertaken by dynamic optimization during operation, go out the RON of product oil by the on-line analysis of NIR analyzer, alkene, parameters such as aromatic hydrocarbons, the PID_A of APC part, PID_B, three regulating loops of PID_C are calculated RON respectively, alkene, the deviation of aromatic hydrocarbons and setting value according to the value of feedback, utilize these deviations to calculate adjusting working value Δ A, Δ B, the Δ C in three loops according to the following principle of optimality, these working values are changed by ratio.Each loop of BBC part is then regulated flow according to working value and is realized the blending process.
The dynamic optimization rule:
1. respectively export relation between the regulated value according to the price decision of each component oil.
2. export the size of regulated value by each component oil properties decision.
3. also can determine the output regulated value of each component as required by the size of tank farm stock.
This scheme has solved the multi-input multi-output system parameter, can add new argument easily according to system's needs, has very strong easy extendability, then only need add a pid loop just as many controlled variable.
All add a distant place, local given function (L represents that this loop adopts manually given on the every road of BBC part, R represents that a distant place promptly automatically), when there is fault in system or feeds back workman when malfunctioning can rule of thumb manual given this component and the ratio of main flow component (catalytic gasoline), this part has substituted the method for traditional artificial this composition flow rate of input.If take traditional method meeting make this component can not follow variation and influence the final finished quality because of the fluctuation of main flow, and no matter the method is the variation of main flow.Handoff functionality can switch simultaneously between each loop or switch separately in certain loop.The no disturbance of this switching is carried out, and therefore can make the operation of system stability ground.
Have more dirigibility by this prioritization scheme of system trial run than classical control method, can adapt to factory's process condition complicated and changeable well.
Should be pointed out that the above embodiment can make those skilled in the art more fully understand the present invention, but do not limit the present invention in any way.

Claims (10)

1. the method for oil product on-line optimization blending, comprise basic control system that the flow of each component is controlled respectively and by the connected optimal control system that possesses intelligent computing of interface, and sampling apparatus and near infrared online analyser that sample is analyzed, it is characterized in that comprising following processing step: enter before the near infrared online analyser analyzes at sample, described sample is carried out pre-service.
2. the method for oil product on-line optimization blending according to claim 1 is characterized in that: the described pre-service that sample is carried out comprises the constant temperature processing and removes water treatment.
3. the method for oil product on-line optimization blending according to claim 2, it is characterized in that: described constant temperature is handled and is comprised one-level constant temperature and secondary constant temperature, described one-level constant temperature adopts 25 ℃ of constant temperature water bath devices, and described secondary constant temperature adopts the electrical heating thermostat that sample temperature is controlled to be 30 ℃.
4. the method for oil product on-line optimization according to claim 3 blending is characterized in that: describedly remove water treatment and carry out between one-level constant temperature and secondary constant temperature, comprise also that between one-level constant temperature and secondary constant temperature the removal of impurity handles.
5. the method for oil product on-line optimization blending according to claim 1, it is characterized in that: the described optimal control system that possesses intelligent computing carries out following running program: calculate prescription with static optimization earlier when the blending beginning, prescription provides the ratio of each component oil and main flow, and main flow is controlled by the ramp function of default, and the flow of other each components is just carried out by basic control system by the flow that its ratio draws; When operation, then undertaken by dynamic optimization, by the near infrared online analyser, on-line analysis goes out the RON of product oil, alkene, the aromatic hydrocarbons parameter is calculated RON by regulating loop respectively according to the value of feedback, alkene, the deviation of aromatic hydrocarbons and setting value is utilized the adjusting working value of these deviations according to the principle of optimality calculating circuit of determining, these working values are changed by ratio; The component flow is then regulated according to working value in each loop of basis control system, realizes blending.
6. the method for oil product on-line optimization blending according to claim 1, it is characterized in that: described regulating loop is three, be PID_A, PID_B, three regulating loops of PID_C, the adjusting working value in corresponding three loops is Δ A, Δ B, Δ C, regulate the initial ratio A of working value and static optimization, B, the C addition obtains the ratio set-point A-SP of new ratio as the BBC regulating loop, B-SP, C-SP, the flow that the product of loop ratio set-point and main flow F-0 draws is as BBC flow control circuit FIC-REF, FIC-MTBE, the flow setting value in loops such as FIC-CYY.Blending control system BBC carries out each component oil flow control according to these setting values, to reach the purpose of on-line optimization blending.
7. the method for oil product on-line optimization blending according to claim 5, it is characterized in that: the controlled variable of described dynamic optimization comprises the tank farm stock size parameter of price parameter, each component oil properties parameter and the each component oil of each component oil.
8. the method for oil product on-line optimization blending according to claim 7 is characterized in that: the phylogenetic relationship between the regulated value is respectively exported in the price parameter decision of described each component oil; The size of described each component oil properties parameter decision output regulated value; The tank farm stock size parameter of described each component oil determines the output regulated value of each component.
9. the method for oil product on-line optimization according to claim 1 blending is characterized in that: in the described basic control system that the flow of each component is controlled respectively, every road is provided with a distant place and local setter.
10. oil product on-line optimization blending system, comprise basic control system that the flow of each component is controlled respectively and by the connected optimal control system that possesses intelligent computing of interface, and sampling apparatus and near infrared online analyser that sample is analyzed, it is characterized in that: also comprise pretreatment system, this pretreatment system is provided with the constant temperature treating apparatus and removes water disposal facility, enter before the near infrared online analyser analyzes at sample, described sample is carried out pre-service.
CNB2004100091914A 2004-06-09 2004-06-09 Online optimized method for blending oil products, and system of implementing the method Expired - Fee Related CN1327306C (en)

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Cited By (10)

* Cited by examiner, † Cited by third party
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CN101286065B (en) * 2008-05-23 2010-06-02 清华大学 Crude oil blending multi-period optimized crude oil concocting and scheduling method
CN102375411A (en) * 2010-08-21 2012-03-14 中国石油化工股份有限公司 Online oil product blending method and device
CN102393636A (en) * 2011-09-22 2012-03-28 任季明 Control system and method for petroleum refining process
CN101887255B (en) * 2009-05-14 2012-07-04 宝山钢铁股份有限公司 Real-time data transmission device and method thereof
CN103941760A (en) * 2014-04-30 2014-07-23 浙江中控软件技术有限公司 Method and device for blending product oil and data integration optimal control server
CN104515861A (en) * 2013-09-28 2015-04-15 中国石油化工股份有限公司 Integrated on-line measurement system for gasoline and diesel oil
CN108333943A (en) * 2018-02-26 2018-07-27 华东理工大学 Crude oil based on incremental mode concocts method for on-line optimization
CN108931496A (en) * 2018-02-05 2018-12-04 北京航程迈进科技发展有限公司 A kind of modeling and method of gasoline sample
CN111359523A (en) * 2020-02-17 2020-07-03 上海华理自动化系统工程有限公司 Advanced control system for oil blending
CN113760002A (en) * 2021-09-01 2021-12-07 南京富岛信息工程有限公司 Heavy oil preheating device and method for near infrared spectrum analysis

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US5712481A (en) * 1990-04-09 1998-01-27 Ashland Inc Process and apparatus for analysis of hydrocarbon species by near infrared spectroscopy
US6395228B1 (en) * 1991-11-27 2002-05-28 Marathon Ashland Petroleum Llc Sampling and analysis system
US5939717A (en) * 1998-01-29 1999-08-17 Schlumberger Technology Corporation Methods and apparatus for determining gas-oil ratio in a geological formation through the use of spectroscopy
CN2468053Y (en) * 2000-11-08 2001-12-26 中国石油天然气股份有限公司兰州炼化分公司 On-line petroleum products blending apparatus
US6897071B2 (en) * 2002-08-13 2005-05-24 Saudi Arabian Oil Company Topological near infrared analysis modeling of petroleum refinery products

Cited By (16)

* Cited by examiner, † Cited by third party
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CN101286065B (en) * 2008-05-23 2010-06-02 清华大学 Crude oil blending multi-period optimized crude oil concocting and scheduling method
CN101887255B (en) * 2009-05-14 2012-07-04 宝山钢铁股份有限公司 Real-time data transmission device and method thereof
CN102375411A (en) * 2010-08-21 2012-03-14 中国石油化工股份有限公司 Online oil product blending method and device
CN102393636A (en) * 2011-09-22 2012-03-28 任季明 Control system and method for petroleum refining process
CN102393636B (en) * 2011-09-22 2013-09-25 任季明 Control system and method for petroleum refining process
CN104515861A (en) * 2013-09-28 2015-04-15 中国石油化工股份有限公司 Integrated on-line measurement system for gasoline and diesel oil
CN104515861B (en) * 2013-09-28 2016-04-20 中国石油化工股份有限公司 Gasoline and diesel oil integration on-line measurement system
CN103941760A (en) * 2014-04-30 2014-07-23 浙江中控软件技术有限公司 Method and device for blending product oil and data integration optimal control server
CN108931496B (en) * 2018-02-05 2021-06-04 北京航程迈进科技发展有限公司 Method for modeling gasoline sample by adopting modeling system of gasoline sample
CN108931496A (en) * 2018-02-05 2018-12-04 北京航程迈进科技发展有限公司 A kind of modeling and method of gasoline sample
CN108333943B (en) * 2018-02-26 2021-05-07 华东理工大学 Crude oil blending online optimization method based on incremental mode
CN108333943A (en) * 2018-02-26 2018-07-27 华东理工大学 Crude oil based on incremental mode concocts method for on-line optimization
CN111359523A (en) * 2020-02-17 2020-07-03 上海华理自动化系统工程有限公司 Advanced control system for oil blending
CN111359523B (en) * 2020-02-17 2024-01-26 上海华理自动化系统工程有限公司 Advanced control system for oil blending
CN113760002A (en) * 2021-09-01 2021-12-07 南京富岛信息工程有限公司 Heavy oil preheating device and method for near infrared spectrum analysis
CN113760002B (en) * 2021-09-01 2022-07-15 南京富岛信息工程有限公司 Heavy oil preheating device and method for near infrared spectrum analysis

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