CN1620876A - Fresh keeping tablet for grape produced adopting full powder direct pelleting method - Google Patents
Fresh keeping tablet for grape produced adopting full powder direct pelleting method Download PDFInfo
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- CN1620876A CN1620876A CN 200410036500 CN200410036500A CN1620876A CN 1620876 A CN1620876 A CN 1620876A CN 200410036500 CN200410036500 CN 200410036500 CN 200410036500 A CN200410036500 A CN 200410036500A CN 1620876 A CN1620876 A CN 1620876A
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Abstract
The grape freshness protecting tablet consists of pyrosulfite or bisulfite, delayed releasing skeleton material and proper excipient, and is prepared through crushing the said materials to 60 -mesh, mixing, and direct pressing to form tablet. The grape freshness protecting tablet has high slow and stable releasing of SO2, simple production process and low cost.
Description
(1) technical field
The invention belongs to the fruit and vegetable fresh-keeping agent process technology, particularly a kind of antistaling tablet for grapes that adopts the direct compression of full-powder method to produce.
(2) background technology
The application of grape fresh-keeping method depends on the characteristic of effective ingredient pyrosulfite or bisulfites.
Its principle is shown as shown in the formula letter:
Water is main " startup agent ", meets the water chemistry balance and moves right, and discharges SO
2, press down mould sterilization, strengthened the storage property of grape.In the grape storage environment, because humidity ratio is bigger, this condition of water possesses all the time.
In order to control SO
2Release and be convenient to carry out compressing tablet, when making antistaling tablet for grapes, added different auxiliary materials respectively.As: Chinese patent CN1359627A, CN1091354C, C741099833C etc.Disclosed antistaling tablet for grapes in these documents owing to the problem of employed slow-release material and excipient in the component that constitutes antistaling tablet, causes it can not adopt the direct compression of full-powder method to produce antistaling tablet for grapes, and can only use the film-making of particle pressed disc method.With particle pressed disc method compacting antistaling tablet for grapes, fusing earlier, granulation, compressing tablet again; Time-consuming, take can, expense factory building, expense equipment, also lose effective ingredient.
(3) summary of the invention
The present invention is directed to the deficiencies in the prior art a kind of available full powder stock is provided, with the antistaling tablet for grapes of rotary tablet machine direct tablet compressing, this invention has solved in the past antistaling tablet for grapes in a large amount of production, heat the problem of compressing tablet of granulating again earlier, thereby overcome problem time-consuming in the prior art, that expense can, be taken factory building, expense equipment and loss effective ingredient.
Technical scheme of the present invention is as follows:
By weight percentage, antistaling tablet for grapes is made up of following composition:
A, effective ingredient: pyrosulfite or bisulfites 74-94%
B, slow release framework material 5-13%
C, be suitable for the excipient 1-13% of direct tablet compressing.
Pyrosulfite is sodium pyrosulfite, potassium metabisulfite or their mixture; Bisulfites is sodium hydrogensulfite, potassium bisulfite or their mixture.
The slow release framework material comprises:
(A), reduce the material of dissolution rate:
A, erodible skeletal substance---(1) wax class, as: Chinese wax, beeswax, paraffin, Ka Naba wax, (2) fats, as: one or both in stearic acid, glycerin monostearate, sucrose list (two) stearate, butyl stearate, the hydrogenated vegetable oil; Perhaps,
B, hydrophilic colloid skeletal substance---(1) cellulose family, as: methylcellulose, sodium carboxymethylcellulose, hydroxypropyl methylcellulose, (2) resinae, as: polyvinylpyrrolidone, one or both in the carboxylic polrvinyl;
(B), reduce the material of diffusion velocity, be insoluble skeletal substance---(1) resinae, as: polyethylene, polyvinyl chloride, polyvinylacetate, polymethacrylates, acrylic resin II number, (2) cellulose family, as: one or both in microcrystalline cellulose, the ethyl cellulose.
Be suitable for the excipient of direct tablet compressing, comprise:
(A), one or both in lubricant---talcum powder, calcium stearate, dolomol, the high melting-point wax;
(B), one or both in glidant---magnesia, gel aluminum hydroxide, calcium monohydrogen phosphate, the superfine silica gel powder.
Above-mentioned raw materials pulverized in proportion mix; Use the direct compression of full-powder method, use the rotary tablet machine compressing tablet to get final product.
Compared with prior art, the invention has the beneficial effects as follows: the fresh-keeping function of 1, having optimized antistaling tablet for grapes: make the SO in the antistaling tablet for grapes
2Stable release 6-8 month, and SO
2Percentage composition descends about 7% month by month: according to conventional preservation technique and using method, when using dosage was 2 ‰ of grape weight-4 ‰, the drug effect phase can reach 6-8 month.2, realized with direct compression of full-powder method large-scale production antistaling tablet for grapes.Save operations such as fusing, granulation, save time, economize and can, economize factory building and equipment, reduced the raw material heat loss, reduced cost.
(4) description of drawings
Fig. 1: the direct compression of full-powder method is produced the technological process of antistaling tablet for grapes.
Among the figure: 1, pyrosulfite or bisulfites 2, the material 3 that reduces dissolution rate, the material 4 that reduces diffusion velocity, lubricant 5, glidant 6, low-temperature grinding 7, weigh 8 respectively, mix 9, stir 10, compressing tablet 11, tablet quality check 12, packing.
(5) specific embodiment
Embodiment 1:
Prescription: sodium pyrosulfite 86%; Paraffin 10%: polyethylene 2.5%; Calcium stearate 0.5%; Gel aluminum hydroxide 1%.(polyethylene, M=1.8 ten thousand ~ 3.5 ten thousand).
Technology: earlier the material paraffin 2 that reduces dissolution rate is carried out low-temperature grinding 6, to 60 orders; Sodium pyrosulfite 1, the material polyethylene 3 that reduces diffusion velocity, lubricant stearic acid calcium 4, glidant gel aluminum hydroxide 5 are directly chosen more than 60 orders.Above-mentioned raw materials is weighed 7 respectively, and the back mixes 8, stirs 9 again, makes the bulky powder raw material, can flow freely, and angle of repose≤45 ° are used rotary tablet machine direct tablet compressing 10 then, through tablet quality check 11, pack 12 at last.
The technology of following examples is substantially with example one.
Embodiment 2, prescription: potassium metabisulfite 80%; Polyvinylpyrrolidone 3%; Acrylic resin II number 10%; Dolomol 1%; Calcium monohydrogen phosphate 6%.(polyvinylpyrrolidone, M=about 40,000; Acrylic resin II number, M=about 13.5 ten thousand).
Embodiment 3, prescription: sodium pyrosulfite 75%; Sodium carboxymethylcellulose 8%; Polymethacrylates 4%; Talcum powder 3%; Calcium monohydrogen phosphate 10%.(sodium carboxymethylcellulose, M=2.1 ten thousand～50,000; Polymethacrylates, M=35 ten thousand～550,000).
Embodiment 4, prescription: sodium pyrosulfite 89%; Single stearic acid glycerine lipoprotein 5%; Microcrystalline cellulose 4%; Calcium stearate 1.5%; Superfine silica gel powder 0.5%.(microcrystalline cellulose, M=about 3.6 ten thousand).
Embodiment 5, prescription: sodium pyrosulfite 93%; Sucrose list (two) stearate 1%; Microcrystalline cellulose 5%; Dolomol 0.3%; Magnesia 0.7%.(microcrystalline cellulose, M=about 3.6 ten thousand).
Claims (5)
1, a kind of antistaling tablet for grapes that adopts the direct compression of full-powder method to produce is characterized in that being made up of pyrosulfite or bisulfites, slow release framework material, the excipient that is suitable for direct tablet compressing, and above-mentioned each weight percentages of components is as follows:
Pyrosulfite or bisulfites 74-94%
Slow release framework material 5-13%
Be suitable for the excipient 1-13% of direct tablet compressing.
2, the antistaling tablet for grapes of employing direct compression of full-powder method production according to claim 1 is characterized in that described pyrosulfite is selected from sodium pyrosulfite, potassium metabisulfite or their mixture; Bisulfites is selected from sodium hydrogensulfite, potassium bisulfite or their mixture.
3, the antistaling tablet for grapes of employing direct compression of full-powder method production according to claim 1 is characterized in that described slow release framework material comprises:
(A) reduce the material of dissolution rate:
A, erodible framework material are selected from (1) wax class, as: Chinese wax, beeswax, paraffin, Ka Nabala,
(2) fats, as: one or both in stearic acid, single stearic acid glycerine lipoprotein, sucrose list (two) stearate, stearic acid butyl ester, the hydrogenated vegetable oil; Perhaps,
B, hydrophilic colloid framework material are selected from (1) cellulose family, as: methylcellulose, sodium carboxymethylcellulose, hydroxypropyl methylcellulose, (2) resinae, as: one or both in polyvinylpyrrolidone, the carboxylic polrvinyl;
(B) material that reduces diffusion velocity is selected from (1) resinae, as: polyethylene, polyvinyl chloride, polyvinylacetate, polymethacrylates, acrylic resin II number, (2) cellulose family, as: one or both in microcrystalline cellulose, the ethyl cellulose.
4, the antistaling tablet for grapes of employing direct compression of full-powder method production according to claim 1 is characterized in that the described excipient that is suitable for direct tablet compressing comprises:
(A) lubricant is selected from one or both in talcum powder, calcium stearate, dolomol, the high melting-point wax;
(B) glidant is selected from one or both in magnesia, gel aluminum hydroxide, calcium monohydrogen phosphate, the superfine silica gel powder.
5, according to claim 1 or 2 or ... the antistaling tablet for grapes that 4 described employing direct compression of full-powder methods are produced is characterized in that with the moulding of direct compression of full-powder method.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100365007A CN100409754C (en) | 2004-12-15 | 2004-12-15 | Fresh keeping tablet for grape produced adopting full powder direct pelleting method |
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| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100365007A CN100409754C (en) | 2004-12-15 | 2004-12-15 | Fresh keeping tablet for grape produced adopting full powder direct pelleting method |
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| Publication Number | Publication Date |
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| CN1620876A true CN1620876A (en) | 2005-06-01 |
| CN100409754C CN100409754C (en) | 2008-08-13 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB2004100365007A Active CN100409754C (en) | 2004-12-15 | 2004-12-15 | Fresh keeping tablet for grape produced adopting full powder direct pelleting method |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105540043A (en) * | 2015-12-14 | 2016-05-04 | 山东营养源食品科技有限公司 | Controlled release type grape preservative paper and preparation method thereof |
| CN108719450A (en) * | 2018-06-29 | 2018-11-02 | 山西省农业科学院农产品贮藏保鲜研究所 | A kind of green grape antistaling tablet and preparation method thereof precisely discharged based on storage period |
| CN109705717A (en) * | 2019-01-12 | 2019-05-03 | 山东营养源食品科技有限公司 | A kind of coating composition, preparation method and its usage |
| CN112878105A (en) * | 2021-01-26 | 2021-06-01 | 新疆农业大学 | Slow-release 1-MCP preservative paper for preservation of Xinjiang small white apricots and application thereof |
Family Cites Families (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1048792A (en) * | 1989-07-05 | 1991-01-30 | 合肥教育工业新技术应用研究所 | Really, vegetables, food preservation film |
| CN1099833C (en) * | 1999-02-09 | 2003-01-29 | 天津市农产品保鲜研究中心 | Fresh-keeping agent for grape and its production method |
| CN1091354C (en) * | 1999-06-30 | 2002-09-25 | 中国科学院新疆物理研究所 | Long-acting antistaling tablet for grapes |
| CN1167351C (en) * | 2000-12-19 | 2004-09-22 | 于天颖 | Antistaling agent for grape |
| CN1263386C (en) * | 2001-10-22 | 2006-07-12 | 新疆大学 | Long-acting antistaling agent for grape |
-
2004
- 2004-12-15 CN CNB2004100365007A patent/CN100409754C/en active Active
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN105540043A (en) * | 2015-12-14 | 2016-05-04 | 山东营养源食品科技有限公司 | Controlled release type grape preservative paper and preparation method thereof |
| CN108719450A (en) * | 2018-06-29 | 2018-11-02 | 山西省农业科学院农产品贮藏保鲜研究所 | A kind of green grape antistaling tablet and preparation method thereof precisely discharged based on storage period |
| CN109705717A (en) * | 2019-01-12 | 2019-05-03 | 山东营养源食品科技有限公司 | A kind of coating composition, preparation method and its usage |
| CN112878105A (en) * | 2021-01-26 | 2021-06-01 | 新疆农业大学 | Slow-release 1-MCP preservative paper for preservation of Xinjiang small white apricots and application thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN100409754C (en) | 2008-08-13 |
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Address after: Fuyang Street Jibei Development Zone in Jiyang County of Ji'nan City, Shandong province 251400 Patentee after: SHANDONG NUTRIENT SOURCE FOOD TECHNOLOGY Co.,Ltd. Address before: 250100 No. 202 industrial North Road, Shandong, Ji'nan Patentee before: JINAN YINGYANGYUAN FOOD Co.,Ltd. |
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Effective date of registration: 20230630 Address after: No. 87 Fuyang Street, Jibei Street, Jiyang District, Jinan City, Shandong Province, 251400 (600 meters west of the bus station and north of the road) Patentee after: SHANDONG AOWEITE BIOTECHNOLOGY Co.,Ltd. Address before: 251400 Fuyang Street, Jibei Development Zone, Jiyang County, Jinan City, Shandong Province Patentee before: SHANDONG NUTRIENT SOURCE FOOD TECHNOLOGY Co.,Ltd. |
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