CN1613506A - Sterilizing fumet and industrial manufacture - Google Patents
Sterilizing fumet and industrial manufacture Download PDFInfo
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- CN1613506A CN1613506A CN 200310103231 CN200310103231A CN1613506A CN 1613506 A CN1613506 A CN 1613506A CN 200310103231 CN200310103231 CN 200310103231 CN 200310103231 A CN200310103231 A CN 200310103231A CN 1613506 A CN1613506 A CN 1613506A
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Abstract
An antibacterial fumigating incense is prepared from Chinese-medicinal materials, fuel adhesive and disperser through shaping by dual-screw extruder.
Description
Technical field:
The present invention relates to a kind of antibacterial incense and industrially preparing process thereof.The invention still further relates to and use the purposes of twin (double) screw extruder in making the incense series products.
Background technology:
Incense has long history.Wherein health can be improved bad smell in the room air, repel mosquitoes and flies etc. with incense.In global sars prevention and control work, incense also plays certain sterilization.
The making traditional method of incense mostly is the pressing that the manual compacting of batching is formed.Mainly dependence experience of wherein many critical processes is judged, is not suitable for suitability for industrialized production, therefore how to make in workshop-based little factory, and the grasp dependence experience to technology is handed down from age to age.This mode of production not only efficient is extremely low, and the restive and adjustment of a lot of important parameter, and the quality of product also is difficult to guarantee.
Improve this situation, make the production technology of incense controlled, indivedual key factor digitized, the one, explore suitable manufacturing machine, the 2nd, find suitable incense prescription, make it be suitable for suitability for industrialized production.
Twin (double) screw extruder (laboratory work station-twin (double) screw extruder of producing as German Bradley Bender food instrument company) is a kind of machinery that is mainly used in fields such as polymer chemistry and food processing.Product in this extruder production of food processing field is mainly various extruding noodles, feedstuff and leisure food, and is easy to use as puffed food etc., is easy to control.
Torque rheology experimental station-twin (double) screw extruder that Germany Bradley Bender food instrument company produces adopts twin screw to extrude expanded principle.This instrument is made of main components such as feeder, modified, transmission in advance, extruding, heating and cooling, molding, cutting, controls.Material is therein by the promotion of extruder screw rod, pushes forward and goes in a zigzag.Material is pressurized, mix, compression, and pressurized heating under mechanisms such as propulsive force and frictional force obtains energy, and the high pressure conditions that reaches a high temperature becomes and has mobile gel.Material is under the state of High Temperature High Pressure, and all compositions have accumulated lot of energy, and when releasing normality suddenly, just increasing towards randomness is that entropy increase direction is carried out.Be accompanied by the difference of terms and conditions parameter, phenomenons such as extrusion modling just take place.
Chinese medicinal herb has traditional advantage aspect preventing and curing diseases, but has only a small amount of type such as mosquito incense aspect the incense being used to produce.
Summary of the invention:
One of purpose of the present invention is to explore the machinery of the incense production that is suitable for; Two of purpose is the suitable incense prescriptions of development, makes it be suitable for industrialization dirt and produces; Three of purpose is Chinese herbal medicine incenses that development can be used for improving hygienic conditions.
Technical scheme of the present invention is:
1. screen the suitable incense prescription of proportioning;
2. select for use twin (double) screw extruder to be used for incense production, the technology controlling and process in the process is determined various processing parameters by experiment.
The requirement that the present invention selects to fill a prescription is:
1. incense has sterilization or fungistatic effect;
2. have burning or combustion-supporting physicochemical property;
3. equipment there is not corrosion and pollution-free to environment for use;
4. charging easy to operate, easy, easily processing, cost are lower.
The incense prescription of the present invention's development is: Chinese herbal medicine, fuel, adhesive and dispersant.
Wherein said Chinese herbal medicine is to have the sterilization or the Chinese medicine of fungistatic effect, but comprise verification the verifying results or widely used in traditional medicine, as Radix Artemisia ordosicae, Herba Taraxaci, tarragon, sandalwood, Herba thymi vulgaris etc., available wherein one or more;
Fuel comprises sawdust, white carbon black, potassium nitrate etc., available wherein one or more;
Adhesive comprises starch, plant gum, incense adhesive specially (commercially available) etc., available wherein one or more:
Dispersant comprises water, vegetable oil, animal oil, available wherein one or more.
The present invention preferably fill a prescription (percentage by weight) be:
Radix Artemisia ordosicae (10-40%), sawdust (20-50%), starch (5-25%), water (10-30%)
The manufacture method of incense provided by the invention
1, batching: by the prescription batching, and mix homogeneously;
2, start twin (double) screw extruder, be preheating to required state;
3, charging;
4, instrument carries out extrusion operation;
5, collect finished product, shutdown.
The specific embodiment:
The screening of embodiment 1 incense composition of raw materials
Experimental selection several commercially available vegetable materials commonly used are primary raw material, are combined into 4 kinds of prescriptions and a matched group mutually, and adjust different dispersant.(table 1).
Table 1 incense composition of raw materials is selected
| Radix Artemisia ordosicae | Starch | Sawdust | Water | |
| Contrast | ????30％ | ????5％ | ????55％ | ????30％ |
| Prescription 1 | ????30％ | ????20％ | ????45％ | ????45％ |
| Prescription 2 | ????30％ | ????20％ | ????40％ | ????45％ |
| Prescription 3 | ????30％ | ????20％ | ????40％ | ????50％ |
| Prescription 4 | ????30％ | ????20％ | ????40％ | ????55％ |
The result shows: matched group is low owing to dispersant, the formed product difficulty.1～4 all can molding and fill a prescription, but the product appearance color have any different slightly, need further do combustion experiment and identify.
Embodiment 2 manufacture processes and method
1) instrument: the twin (double) screw extruder (Brabender Lab-Station2-Screw Extruder) that German Bradley Bender food instrument production company produces;
2) environmental condition: room temperature, relative humidity 80-90%.
3) processing step:
A) consumption of pressing prescription 1-4 is adjusted moisture with the raw material mix homogeneously:
B) start twin (double) screw extruder, be preheating to required state;
C) charging; Instrument carries out extrusion operation;
D) collect finished product, shutdown.
In experimentation, paying close attention to the variation of material, in time adjusting experiment condition, and noting the pressure and the moment of torsion in a certain stage according to both variations at machine internal pressure and moment of torsion.With reference to the combustion experiment of incense finished product, determine product formula and sophisticated technology.
4) extruding condition screening
Experimental result sees Table 2.
Table 2 temperature and prescription are to the influence of squeezing parameter
| The sample title | Extrusion temperature (℃) | Moment of torsion (Nm) | Pressure (Bar) | ||||
| Meansigma methods X | Maximum Max | Minimum M in | Meansigma methods X | Maximum Max | Minimum M in | ||
| Contrast | ????30-80 | ?244.94 | ?287.3 | ?235.7 | ?85.55 | ?86.4 | ?84.9 |
| Prescription 1 | ??40-110 | ??44.9 | ??53.6 | ??35.1 | ??18.79 | ??19.7 | ??17 |
| Prescription 2 | ??45-105 | ??43.93 | ??52.6 | ??34.9 | ??16.00 | ??17.6 | ??14.5 |
| Prescription 3 | ??35-130 | ??38.81 | ??41.7 | ??37.2 | ??12.18 | ??12.6 | ??11.7 |
| Prescription 4 | ??50-120 | ??32.93 | ??35.4 | ??26.8 | ??9.59 | ??9.9 | ??9.2 |
Conclusion:
Matched group causes moment of torsion and pressure all higher because extrusion temperature and material dispersed agent content are low excessively.This not only influences the fltting speed of material in screw rod, and has directly influenced the output and the quality of product.
1～4 selected suitable extrusion temperature and fill a prescription, moment of torsion and pressure are all comparatively moderate, have possessed the feasibility on the processing technique.
The combustion experiment of embodiment 3 incense finished products
Difference intercepted length 20cm, weight is about the incense finished product of 1.9g, and burning is to complete, and the back is write down burning time and is also collected combustion product and weigh.Experimental data sees Table 3.
The combustion experiment of table 3 incense finished product
| Sample | Moisture (%) | Burning time (min/20cm) | Combustion residue heavy (mg/20cm) |
| Prescription 1 | ????8.11 | ????47 | ????40 |
| Prescription 2 | ????7.86 | ????43 | ????80 |
| Prescription 3 | ????7.77 | ????39 | ????80 |
| Prescription 4 | ????7.76 | ????30 | ????60 |
Conclusion:
From the incendiary result of the test of incense finished product as can be seen, the product that dispersant is high more, burning velocity is fast more.Because dispersant evaporates in processing and dry run, make the organizational structure of incense more loose, be easy to burning.
The sterilization experiment of embodiment 4 incense finished products
1. experiment place: 30m
2Indoor, except that required desk of the test of putting and support, there are not other foreign material, door and window is closed.
Among experiment material: the embodiment 1 prescription 4 incenses; Antibacterial and mould medium are poured into behind the sterilization respectively in the disinfectant culture dish, and be stand-by.
3. experimental technique:
1) incense being placed in the middle of the room, is the center of circle with it, selects 3 points (A, B, C) respectively on 50cm, 100cm, 150cm radius respectively, places each 2 on the culture dish that fills antibacterial and mould medium respectively at selected each point place.
2) before lighting incense, the culture dish lid is opened, placed 30 minutes, then culture dish is built, remove.In contrast.
3) light 3 of incenses, until its after-flame, for handling for the first time.Then, place each 2 on the culture dish that fills bacteria culture media and mould medium respectively at above-mentioned selected each point place, open the culture dish lid, placed 30 minutes, then, culture dish is built, remove.
4) refire 1 incense (3), repeat 4 step,, finish until test for handling for the second time.
5) the above-mentioned culture dish that fills bacteria culture media is placed 36 ± 1 ℃ of constant incubators, cultivated 48 hours, count the total plate count in each culture dish.Place 25～28 ℃ of constant incubators to cultivate on the above-mentioned culture dish that fills mould medium, begin after 3 days to observe, cultivate altogether and observed 5 days.Count the total plate count in each culture dish.
4. experimental result
Computational methods: sterilizing rate (%)=(contrast clump count-processing back clump count) * 100/ contrast clump count
The results are shown in Table 4, table 5,
Table 4 incense is to the inhibition effect of antibacterial in the air
| The testing site | ????A | ????B | ????C |
| Contrast clump count (individual) | ????35 | ????31.5 | ????29.5 |
| Handle back clump count (individual) for the first time | ????19.5 | ????20 | ????15 |
| Sterilizing rate (%) | ????44.3 | ????36.5 | ????49.2 |
| Handle back clump count (individual) for the second time | ????12 | ????15.5 | ????13 |
| Sterilizing rate (%) | ????65.7 | ????50.8 | ????55.9 |
(annotate: the use amount of handling incense for the first time is 3, and the use amount of handling incense for the second time is 6.)
Table 5 incense is to the inhibition effect of mycete in the air
| The testing site | ????A | ????B | ????C |
| Contrast clump count (individual) | ????14 | ????11 | ????15.5 |
| Handle back clump count (individual) for the first time | ????7 | ????5.5 | ????7.5 |
| Sterilizing rate (%) | ????50 | ????50 | ????51.6 |
| Handle back clump count (individual) for the second time | ????5.5 | ????5.5 | ????7 |
| Sterilizing rate (%) | ????56.7 | ????50 | ????55 |
(annotate: the use amount of handling incense for the first time is 3, and the use amount of handling incense for the second time is 6.)
5. experiment conclusion:
This incense all more than 40%, shows that this incense finished product has comparatively obvious sterilization effect to the sterilizing rate of airborne antibacterial and mycete.The use amount of incense affects its sterilization effects simultaneously, and along with the increase of combustion incense quantity, sterilizing rate also improves.
Claims (4)
1. the industrially preparing process of an incense is characterized as and uses the twin (double) screw extruder manufacturing.
2. the prescription of an incense includes Chinese herbal medicine, fuel, adhesive and dispersant.
3. the prescription of the described incense of claim 2, wherein said Chinese herbal medicine is one or more in Radix Artemisia ordosicae, Herba Taraxaci, tarragon, sandalwood, the Herba thymi vulgaris; Fuel comprises one or more in sawdust, white carbon black, the potassium nitrate; Adhesive comprises one or more in starch, plant gum, the incense adhesive specially; Dispersant comprises one or more in water, vegetable oil, the animal oil.
4. the prescription of the described incense of claim 2, its optimum ratio (percentage by weight) is: Radix Artemisia ordosicae 10-40%, sawdust 20-50%, starch 5-25%, water 10-30%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2003101032317A CN1304060C (en) | 2003-11-03 | 2003-11-03 | Sterilizing fumet and industrial manufacture |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2003101032317A CN1304060C (en) | 2003-11-03 | 2003-11-03 | Sterilizing fumet and industrial manufacture |
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| Publication Number | Publication Date |
|---|---|
| CN1613506A true CN1613506A (en) | 2005-05-11 |
| CN1304060C CN1304060C (en) | 2007-03-14 |
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| Application Number | Title | Priority Date | Filing Date |
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| CNB2003101032317A Expired - Fee Related CN1304060C (en) | 2003-11-03 | 2003-11-03 | Sterilizing fumet and industrial manufacture |
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Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101263876B (en) * | 2008-04-04 | 2011-02-16 | 李运龙 | Food incense and fumigating cabinet for fumigating food by food incense |
| CN101322851B (en) * | 2008-07-31 | 2011-11-16 | 吕坤秋 | Method for producing Tibetan medicinal herb incense |
| CN103654253A (en) * | 2012-09-21 | 2014-03-26 | 林国隆 | Ingredients and production method for incense reducing nanmu bark sticky powder amount |
| CN104000464A (en) * | 2014-06-17 | 2014-08-27 | 陈智辉 | Environment-friendly incense |
| CN105707218A (en) * | 2016-03-03 | 2016-06-29 | 和县朱韩瓜果种植家庭农场 | Preparation method of disinfection incense in cold storage of pomegranate fruit |
| CN105724560A (en) * | 2016-03-03 | 2016-07-06 | 和县朱韩瓜果种植家庭农场 | Method for preparing dried figs |
| CN105767134A (en) * | 2016-03-03 | 2016-07-20 | 和县朱韩瓜果种植家庭农场 | Preparation method of dried kiwi fruits |
| CN105999340A (en) * | 2016-05-13 | 2016-10-12 | 德施普科技发展温州有限公司 | Nerve soothing incense and preparation method thereof |
| CN107684328A (en) * | 2017-10-13 | 2018-02-13 | 郝兴 | Make fragrant technique |
| CN108498833A (en) * | 2018-06-07 | 2018-09-07 | 福建兴隆香业有限公司 | A kind of extra-strong tea agalloch eaglewood and preparation method thereof |
| CN109010886A (en) * | 2018-08-14 | 2018-12-18 | 王灯生 | A kind of incense ashes Conglobation type fragrant incense and preparation method thereof |
| CN109042644A (en) * | 2018-08-13 | 2018-12-21 | 王灯生 | A kind of desinsection degerming fragrant incense |
| CN109966531A (en) * | 2019-04-22 | 2019-07-05 | 江苏安心养老服务股份有限公司 | Mulberry stacte composition and preparation method thereof |
Family Cites Families (2)
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| CN1041055C (en) * | 1991-04-13 | 1998-12-09 | 赵永福 | Sterilizing incense for poultry |
| CN1338314A (en) * | 2000-08-17 | 2002-03-06 | 郭光林 | Non-smoke sanitary incense with bamboo stick |
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2003
- 2003-11-03 CN CNB2003101032317A patent/CN1304060C/en not_active Expired - Fee Related
Cited By (14)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101263876B (en) * | 2008-04-04 | 2011-02-16 | 李运龙 | Food incense and fumigating cabinet for fumigating food by food incense |
| CN101322851B (en) * | 2008-07-31 | 2011-11-16 | 吕坤秋 | Method for producing Tibetan medicinal herb incense |
| CN103654253A (en) * | 2012-09-21 | 2014-03-26 | 林国隆 | Ingredients and production method for incense reducing nanmu bark sticky powder amount |
| CN103654253B (en) * | 2012-09-21 | 2015-10-28 | 林国隆 | Nanju peel can be reduced or remitted stick the component prescription of the perfume (or spice) of powder consumption and manufacture the method for this perfume (or spice) |
| CN104000464A (en) * | 2014-06-17 | 2014-08-27 | 陈智辉 | Environment-friendly incense |
| CN105724560A (en) * | 2016-03-03 | 2016-07-06 | 和县朱韩瓜果种植家庭农场 | Method for preparing dried figs |
| CN105707218A (en) * | 2016-03-03 | 2016-06-29 | 和县朱韩瓜果种植家庭农场 | Preparation method of disinfection incense in cold storage of pomegranate fruit |
| CN105767134A (en) * | 2016-03-03 | 2016-07-20 | 和县朱韩瓜果种植家庭农场 | Preparation method of dried kiwi fruits |
| CN105999340A (en) * | 2016-05-13 | 2016-10-12 | 德施普科技发展温州有限公司 | Nerve soothing incense and preparation method thereof |
| CN107684328A (en) * | 2017-10-13 | 2018-02-13 | 郝兴 | Make fragrant technique |
| CN108498833A (en) * | 2018-06-07 | 2018-09-07 | 福建兴隆香业有限公司 | A kind of extra-strong tea agalloch eaglewood and preparation method thereof |
| CN109042644A (en) * | 2018-08-13 | 2018-12-21 | 王灯生 | A kind of desinsection degerming fragrant incense |
| CN109010886A (en) * | 2018-08-14 | 2018-12-18 | 王灯生 | A kind of incense ashes Conglobation type fragrant incense and preparation method thereof |
| CN109966531A (en) * | 2019-04-22 | 2019-07-05 | 江苏安心养老服务股份有限公司 | Mulberry stacte composition and preparation method thereof |
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|---|---|
| CN1304060C (en) | 2007-03-14 |
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