CN1597841A - White light fluorescent powder excited by blue light and its use, manufacturing process and manufacturing device - Google Patents
White light fluorescent powder excited by blue light and its use, manufacturing process and manufacturing device Download PDFInfo
- Publication number
- CN1597841A CN1597841A CNA2004100417849A CN200410041784A CN1597841A CN 1597841 A CN1597841 A CN 1597841A CN A2004100417849 A CNA2004100417849 A CN A2004100417849A CN 200410041784 A CN200410041784 A CN 200410041784A CN 1597841 A CN1597841 A CN 1597841A
- Authority
- CN
- China
- Prior art keywords
- manufacturing process
- fluorescent powder
- blue
- gas
- light excited
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 238000004519 manufacturing process Methods 0.000 title claims abstract description 43
- 239000000843 powder Substances 0.000 title claims abstract description 38
- 238000006243 chemical reaction Methods 0.000 claims abstract description 19
- 239000002243 precursor Substances 0.000 claims abstract description 17
- 238000000889 atomisation Methods 0.000 claims abstract description 14
- 239000007788 liquid Substances 0.000 claims abstract description 9
- 229910052684 Cerium Inorganic materials 0.000 claims abstract description 5
- 229910052693 Europium Inorganic materials 0.000 claims abstract description 5
- 229910052775 Thulium Inorganic materials 0.000 claims abstract description 5
- 229910052771 Terbium Inorganic materials 0.000 claims abstract description 3
- 239000000463 material Substances 0.000 claims description 27
- 239000003595 mist Substances 0.000 claims description 12
- 239000008367 deionised water Substances 0.000 claims description 8
- 229910021641 deionized water Inorganic materials 0.000 claims description 8
- 239000012530 fluid Substances 0.000 claims description 8
- 238000010438 heat treatment Methods 0.000 claims description 8
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Chemical compound O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 8
- 150000001875 compounds Chemical class 0.000 claims description 7
- 239000002253 acid Substances 0.000 claims description 6
- 239000000654 additive Substances 0.000 claims description 6
- 230000000996 additive effect Effects 0.000 claims description 6
- 125000002091 cationic group Chemical group 0.000 claims description 6
- 238000001035 drying Methods 0.000 claims description 6
- 239000002245 particle Substances 0.000 claims description 6
- 238000012545 processing Methods 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- 238000001354 calcination Methods 0.000 claims description 5
- 238000005516 engineering process Methods 0.000 claims description 5
- 229920000742 Cotton Polymers 0.000 claims description 4
- LYCAIKOWRPUZTN-UHFFFAOYSA-N Ethylene glycol Chemical compound OCCO LYCAIKOWRPUZTN-UHFFFAOYSA-N 0.000 claims description 4
- 239000011449 brick Substances 0.000 claims description 4
- 239000013078 crystal Substances 0.000 claims description 4
- -1 polyoxyethylene Polymers 0.000 claims description 4
- 229910052782 aluminium Inorganic materials 0.000 claims description 3
- VEXZGXHMUGYJMC-UHFFFAOYSA-M Chloride anion Chemical compound [Cl-] VEXZGXHMUGYJMC-UHFFFAOYSA-M 0.000 claims description 2
- 229910052688 Gadolinium Inorganic materials 0.000 claims description 2
- 229920003171 Poly (ethylene oxide) Polymers 0.000 claims description 2
- 150000001768 cations Chemical class 0.000 claims description 2
- WGCNASOHLSPBMP-UHFFFAOYSA-N hydroxyacetaldehyde Natural products OCC=O WGCNASOHLSPBMP-UHFFFAOYSA-N 0.000 claims description 2
- 229910052500 inorganic mineral Inorganic materials 0.000 claims description 2
- 238000012423 maintenance Methods 0.000 claims description 2
- 239000011707 mineral Substances 0.000 claims description 2
- 150000002823 nitrates Chemical class 0.000 claims description 2
- 150000007524 organic acids Chemical class 0.000 claims description 2
- 230000001590 oxidative effect Effects 0.000 claims description 2
- 238000012856 packing Methods 0.000 claims description 2
- 150000003839 salts Chemical class 0.000 claims description 2
- 229910052710 silicon Inorganic materials 0.000 claims description 2
- 150000003467 sulfuric acid derivatives Chemical class 0.000 claims description 2
- 229910052727 yttrium Inorganic materials 0.000 claims description 2
- 238000000034 method Methods 0.000 abstract description 5
- 238000002360 preparation method Methods 0.000 abstract description 3
- 238000011031 large-scale manufacturing process Methods 0.000 abstract 1
- 238000000746 purification Methods 0.000 abstract 1
- 229910001404 rare earth metal oxide Inorganic materials 0.000 abstract 1
- 238000009423 ventilation Methods 0.000 abstract 1
- 239000000243 solution Substances 0.000 description 15
- 239000007787 solid Substances 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 238000009826 distribution Methods 0.000 description 6
- 238000010574 gas phase reaction Methods 0.000 description 6
- GRYLNZFGIOXLOG-UHFFFAOYSA-N Nitric acid Chemical compound O[N+]([O-])=O GRYLNZFGIOXLOG-UHFFFAOYSA-N 0.000 description 4
- 229910004298 SiO 2 Inorganic materials 0.000 description 4
- 238000000498 ball milling Methods 0.000 description 4
- 229910017604 nitric acid Inorganic materials 0.000 description 4
- 229910002651 NO3 Inorganic materials 0.000 description 3
- 229910019655 synthetic inorganic crystalline material Inorganic materials 0.000 description 3
- 239000012808 vapor phase Substances 0.000 description 3
- 239000007864 aqueous solution Substances 0.000 description 2
- 238000005352 clarification Methods 0.000 description 2
- 238000004891 communication Methods 0.000 description 2
- 238000010790 dilution Methods 0.000 description 2
- 239000012895 dilution Substances 0.000 description 2
- 239000002223 garnet Substances 0.000 description 2
- 238000009434 installation Methods 0.000 description 2
- 230000001788 irregular Effects 0.000 description 2
- 238000002156 mixing Methods 0.000 description 2
- 229910052761 rare earth metal Inorganic materials 0.000 description 2
- 238000010532 solid phase synthesis reaction Methods 0.000 description 2
- 238000010792 warming Methods 0.000 description 2
- NHNBFGGVMKEFGY-UHFFFAOYSA-N Nitrate Chemical compound [O-][N+]([O-])=O NHNBFGGVMKEFGY-UHFFFAOYSA-N 0.000 description 1
- XAGFODPZIPBFFR-UHFFFAOYSA-N aluminium Chemical compound [Al] XAGFODPZIPBFFR-UHFFFAOYSA-N 0.000 description 1
- 239000004411 aluminium Substances 0.000 description 1
- JNDMLEXHDPKVFC-UHFFFAOYSA-N aluminum;oxygen(2-);yttrium(3+) Chemical compound [O-2].[O-2].[O-2].[Al+3].[Y+3] JNDMLEXHDPKVFC-UHFFFAOYSA-N 0.000 description 1
- 230000015572 biosynthetic process Effects 0.000 description 1
- 229910019990 cerium-doped yttrium aluminum garnet Inorganic materials 0.000 description 1
- 238000000975 co-precipitation Methods 0.000 description 1
- 238000013461 design Methods 0.000 description 1
- 238000010586 diagram Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 230000005284 excitation Effects 0.000 description 1
- 238000001027 hydrothermal synthesis Methods 0.000 description 1
- 239000000203 mixture Substances 0.000 description 1
- 238000010298 pulverizing process Methods 0.000 description 1
- 230000000630 rising effect Effects 0.000 description 1
- 238000003980 solgel method Methods 0.000 description 1
- 238000003746 solid phase reaction Methods 0.000 description 1
- 238000010671 solid-state reaction Methods 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 239000000758 substrate Substances 0.000 description 1
- 238000003786 synthesis reaction Methods 0.000 description 1
- 238000010189 synthetic method Methods 0.000 description 1
- 238000005406 washing Methods 0.000 description 1
- 150000003746 yttrium Chemical class 0.000 description 1
- 229910019901 yttrium aluminum garnet Inorganic materials 0.000 description 1
Classifications
-
- Y—GENERAL TAGGING OF NEW TECHNOLOGICAL DEVELOPMENTS; GENERAL TAGGING OF CROSS-SECTIONAL TECHNOLOGIES SPANNING OVER SEVERAL SECTIONS OF THE IPC; TECHNICAL SUBJECTS COVERED BY FORMER USPC CROSS-REFERENCE ART COLLECTIONS [XRACs] AND DIGESTS
- Y02—TECHNOLOGIES OR APPLICATIONS FOR MITIGATION OR ADAPTATION AGAINST CLIMATE CHANGE
- Y02B—CLIMATE CHANGE MITIGATION TECHNOLOGIES RELATED TO BUILDINGS, e.g. HOUSING, HOUSE APPLIANCES OR RELATED END-USER APPLICATIONS
- Y02B20/00—Energy efficient lighting technologies, e.g. halogen lamps or gas discharge lamps
Landscapes
- Luminescent Compositions (AREA)
Abstract
Description
Classification | Solid phase method is synthetic | Vapor phase process is synthetic |
Relative brightness (%) | 100 | ????124 |
Emission main peak (nm) | 541 | ????538 |
Size distribution | Wide | Narrow |
Pattern | Irregular | Solid sphere |
Dispersed | Reunite and lump, need ball milling | Be uniformly dispersed |
Classification | Solid phase method is synthetic | Vapor phase process is synthetic |
Relative brightness (%) | 100 | ????129 |
Emission main peak (nm) | 551 | ????557 |
Size distribution | Wide | Narrow |
Pattern | Irregular | Solid sphere |
Dispersed | Reunite and lump, need ball milling | Be uniformly dispersed |
Claims (15)
Priority Applications (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100417849A CN100412158C (en) | 2004-08-25 | 2004-08-25 | White light fluorescent powder excited by blue light and its use, manufacturing process and manufacturing device |
Applications Claiming Priority (1)
Application Number | Priority Date | Filing Date | Title |
---|---|---|---|
CNB2004100417849A CN100412158C (en) | 2004-08-25 | 2004-08-25 | White light fluorescent powder excited by blue light and its use, manufacturing process and manufacturing device |
Publications (2)
Publication Number | Publication Date |
---|---|
CN1597841A true CN1597841A (en) | 2005-03-23 |
CN100412158C CN100412158C (en) | 2008-08-20 |
Family
ID=34665254
Family Applications (1)
Application Number | Title | Priority Date | Filing Date |
---|---|---|---|
CNB2004100417849A Expired - Fee Related CN100412158C (en) | 2004-08-25 | 2004-08-25 | White light fluorescent powder excited by blue light and its use, manufacturing process and manufacturing device |
Country Status (1)
Country | Link |
---|---|
CN (1) | CN100412158C (en) |
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1312252C (en) * | 2005-11-28 | 2007-04-25 | 广州有色金属研究院 | Method and apparatus for preparing PDP fluorescent material |
JP2009541521A (en) * | 2006-06-21 | 2009-11-26 | テジュ エレクトロニック マテリアルズ カンパニー リミテッド | Thulium-containing phosphor for white light emitting diode and method for producing the same |
CN101210181B (en) * | 2006-12-29 | 2010-05-19 | 财团法人工业技术研究院 | Fluorescent material, white light luminescent device and false proof coating |
CN101126024B (en) * | 2007-09-07 | 2010-06-09 | 江苏博睿光电有限公司 | Fluorescent powder for white light emitting diode and preparation method thereof |
CN101705095B (en) * | 2009-09-21 | 2011-08-10 | 四川新力光源有限公司 | Yellow light afterglow material and preparation method thereof as well as LED illuminating device using same |
CN103217016A (en) * | 2013-04-09 | 2013-07-24 | 南京信息职业技术学院 | Inorganic powder material synthesizer |
Family Cites Families (4)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
JP2666414B2 (en) * | 1988-10-17 | 1997-10-22 | ソニー株式会社 | Green phosphor |
JP4623403B2 (en) * | 2000-04-06 | 2011-02-02 | 日立金属株式会社 | Ceramics, ceramic powder production method and ceramic production method. |
CN1180052C (en) * | 2000-06-26 | 2004-12-15 | 中国科学院长春光学精密机械与物理研究所 | Wavelength-converting luminous material of white light for LED |
CN1206313C (en) * | 2000-12-30 | 2005-06-15 | 大连路明发光科技股份有限公司 | New type long-persistence material |
-
2004
- 2004-08-25 CN CNB2004100417849A patent/CN100412158C/en not_active Expired - Fee Related
Cited By (6)
Publication number | Priority date | Publication date | Assignee | Title |
---|---|---|---|---|
CN1312252C (en) * | 2005-11-28 | 2007-04-25 | 广州有色金属研究院 | Method and apparatus for preparing PDP fluorescent material |
JP2009541521A (en) * | 2006-06-21 | 2009-11-26 | テジュ エレクトロニック マテリアルズ カンパニー リミテッド | Thulium-containing phosphor for white light emitting diode and method for producing the same |
CN101210181B (en) * | 2006-12-29 | 2010-05-19 | 财团法人工业技术研究院 | Fluorescent material, white light luminescent device and false proof coating |
CN101126024B (en) * | 2007-09-07 | 2010-06-09 | 江苏博睿光电有限公司 | Fluorescent powder for white light emitting diode and preparation method thereof |
CN101705095B (en) * | 2009-09-21 | 2011-08-10 | 四川新力光源有限公司 | Yellow light afterglow material and preparation method thereof as well as LED illuminating device using same |
CN103217016A (en) * | 2013-04-09 | 2013-07-24 | 南京信息职业技术学院 | Inorganic powder material synthesizer |
Also Published As
Publication number | Publication date |
---|---|
CN100412158C (en) | 2008-08-20 |
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Legal Events
Date | Code | Title | Description |
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C06 | Publication | ||
PB01 | Publication | ||
C10 | Entry into substantive examination | ||
SE01 | Entry into force of request for substantive examination | ||
C14 | Grant of patent or utility model | ||
GR01 | Patent grant | ||
EE01 | Entry into force of recordation of patent licensing contract |
Assignee: Jiangsu Yong Shi Lighting Co.,Ltd. Assignor: Nanjing Tech University Contract fulfillment period: 2009.8.31 to 2012.8.30 Contract record no.: 2009320001624 Denomination of invention: White light fluorescence powder excitated by blue light and its application mfg. technology and mfg. apparatus Granted publication date: 20080820 License type: Exclusive license Record date: 20090902 |
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LIC | Patent licence contract for exploitation submitted for record |
Free format text: EXCLUSIVE LICENSE; TIME LIMIT OF IMPLEMENTING CONTACT: 2009.8.31 TO 2012.8.30; CHANGE OF CONTRACT Name of requester: JIANGSU YONGSHI LIGHTING CO., LTD. Effective date: 20090902 |
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EC01 | Cancellation of recordation of patent licensing contract |
Assignee: JIANGSU YONG SHI LIGHTING Co.,Ltd. Assignor: Nanjing Tech University Contract record no.: 2009320001624 Date of cancellation: 20140923 |
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LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
EE01 | Entry into force of recordation of patent licensing contract |
Application publication date: 20050323 Assignee: JIANGSU HAODE ENERGY-SAVING PHOTOELECTRICITY TECHNOLOGY CO.,LTD. Assignor: Nanjing Tech University Contract record no.: 2015320000144 Denomination of invention: White light fluorescence powder excitated by blue light and its application mfg. technology and mfg. apparatus Granted publication date: 20080820 License type: Common License Record date: 20150407 |
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LICC | Enforcement, change and cancellation of record of contracts on the licence for exploitation of a patent or utility model | ||
CF01 | Termination of patent right due to non-payment of annual fee | ||
CF01 | Termination of patent right due to non-payment of annual fee |
Granted publication date: 20080820 Termination date: 20170825 |