CN1582702A - Tea candy without sugar and with low calorie and its production - Google Patents
Tea candy without sugar and with low calorie and its production Download PDFInfo
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- CN1582702A CN1582702A CNA2004100227558A CN200410022755A CN1582702A CN 1582702 A CN1582702 A CN 1582702A CN A2004100227558 A CNA2004100227558 A CN A2004100227558A CN 200410022755 A CN200410022755 A CN 200410022755A CN 1582702 A CN1582702 A CN 1582702A
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- sweet tea
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Abstract
A saccharide-free low-caloricity sweet tea sugar for the patients of obesity, diabetes and cardiovascular and cerebrovascular diseases is prepared from tea leaves through choosing tea leaves, extracting in water, filtering, removing impurities, adsorbing eluting, decoloring, concentrating, drying, proportionally mixing with vegetative polybasic alditol, inclusion, recrystalizing and drying.
Description
(1) technical field:
The present invention relates to the health food made by plant extract, low heat energy sweet tea sugar of specifically a kind of sugar-free and manufacture method thereof.
(2) background technology:
(Rubus Suavissmus S is the Rosaceae rubus Lee) to sweet tea, has heat-clearing and toxic substances removing, antiallergic, moistening the lung and resolving phlegm cough-relieving, anti-fat lipid-lowering and blood-pressure-lowing, reduce cholesterolemia, suppress and delay sclerosis of blood vessels, prevent and treat health cares such as coronary heart disease and diabetes.The extract of sweet tea---glycosides is a kind of high sugariness (than sweet 250 times of sucrose), material low in calories, but because sweet tea has special bitter taste, it is very big that it is directly used in the food and drink difficulty of processing, so rarely found in the market have Folium hydrangeae strigosae to sell for sugar product.
(3) summary of the invention:
The present invention will disclose few, the good water solubility of a kind of bitter taste, can place of sucrose be used for the sweet tea sugar low in calories that various types of beverages, food are processed.
The present invention also will disclose the manufacture method of above-mentioned sweet tea sugar low in calories.
The manufacture method of the low heat energy sweet tea sugar of a kind of sugar-free, its step is as follows:
1) choose 50～200 weight portions do not have mildew and rot, the pure clean sweet tea cured leaf of no insect pest;
2) the sweet tea cured leaf is added water and carry out water and carry, the water extract is merged filter again;
3) in filtrate, add the bivalent cation material and make its pH value=9～12, treat contamination precipitation after, sediment separate out; Wherein said bivalent cation material generally is calcium salt or magnesium salt, preferably Ca (OH)
2, MgCO
3
4) get supernatant, the supernatant pH value is neutralized to neutrality, carry out adsorbing separation with macroporous adsorbent resin; Described macroporous adsorbent resin is preferably nonpolar styrene type copolymer macroporous adsorbent resin, as model is: the macroporous adsorbent resin of D101, D102, AB-8;
5) the ethanol elution styrene type copolymer macroporous adsorptive resins of usefulness volumetric concentration 50%～70%;
6) eluent reuse weakly-basic anion exchange macropore ion exchange resin is decoloured; Described weakly-basic anion exchange macropore ion exchange resin for being generally acrylic type copolymer weakly-basic anion exchange macroporous resin as model is: the macroporous resin of D280, D900;
7) destaining solution is carried out vacuum concentration under 50～70 ℃ of temperature;
8) again that it is dry under 80～90 ℃ of temperature, get the sweet tea extract;
9) add 50～200 weight portion plant fermentation multi-sugar alcohols and sweet tea extract mixing, in said mixture, add 1～12 weight portion, volumetric concentration again and be 85%～100% ethanol, under 30～50 ℃ of temperature, fully stir, and leave standstill and treat its enclose recrystallization;
10) with the dry finished product that gets under 80～90 ℃ of temperature of the extract behind the enclose.
In the manufacture method of the low heat energy sweet tea sugar of above-mentioned sugar-free, the best proportioning of each component raw material is as follows: (in weight portion)
Sweet tea cured leaf 40～60
Plant fermentation multi-sugar alcohol 80～100.
Described plant fermentation multi-sugar alcohol is preferably erythritol or xylitol.
Since the present invention be earlier sweet tea through water carry, remove impurity, separation, eluting, concentrate, dry, it is less to obtain a kind of bitter taste, glycosides content is than higher sweet tea extract, and glycosides itself is a kind of high sugariness sweeter 250 times than sucrose, material low in calories, again with itself and plant multi-sugar alcohol enclose recrystallization, the low heat energy sweet tea sugar finished product of sugar-free.Sweet tea sugar of the present invention does not contain the material that sucrose, glucose, starch etc. can change into the human heat, and fresh and sweet nothing is bitter, color is light, good water solubility, it is a kind of Folium hydrangeae strigosae health beverage, also being the low heat energy sweeting agent of a kind of sugar-free, can being widely used in beverage, coffee, milk, the cooking and food processing, also is the people's of obesity, diabetes, cardio-cerebral vascular disease patient and inedibility sucrose sugar substitute.
(4) specific embodiment:
Embodiment 1:
Get not have and go rotten, the pure sweet tea cured leaf of no insect pest 100g uses 1000ml boiling tap water 2 hours, after filtering with filter cloth, gets 1 hour after-filtration of its filtering residue reuse 800ml boiling tap water, merges twice filtrate and gets the about 1500ml of extracting solution.In extracting solution, add aqua calcis, make its pH value=9～12, and with its static 1 hour, the reuse gradient method separates supernatant with precipitate, the supernatant volumetric concentration is neutralized to neutrality for the 10%NaOH aqueous solution, then by the interior styrene type copolymer macroporous adsorbent resin glass column that 100gD101, diameter 25mm, high 300mm are housed, carry out adsorbing separation, reuse volumetric concentration 70% ethanol 500ml washs macroporous resin column after treating whole dried liquid streams, collects whole cleaning mixture at the bottom of post.Again with cleaning mixture by the processing of decolouring of the interior 100g of being equipped with D280, diameter 25mm, high 300mm acrylic type copolymer weakly-basic anion exchange macroporous resin glass column, at the bottom of post, collect whole destaining solution then.The vacuum concentration cleaning mixture is to original volume about 1/20 under 60 ℃ of temperature, and spray drying obtains the light glycosides content of color than higher sweet tea extract under 85 ℃ of temperature.Get 196g erythritol and the above-mentioned sweet tea extract mixing that obtains again, adding the 8ml volumetric concentration again is that 98% ethanol was fully stirring about 15～25 minutes under 20～40 ℃ of temperature, and then it is left standstill about 20～40 minutes, after obtaining bright crystalline thing, dry under 85 ℃ of temperature, sterilization promptly get water content and are lower than 5% finished product.
Embodiment 2:
Get not have and go rotten, the pure sweet tea cured leaf of no insect pest 50g uses 500ml boiling tap water 2 hours, after filtering with filter cloth, gets 1 hour after-filtration of its filtering residue reuse 400ml boiling tap water, merges twice filtrate and gets the about 750ml of extracting solution.In extracting solution, add magnesium carbonate solution, make its pH value=11, and with its static 1 hour, the reuse gradient method separates supernatant with precipitate, the supernatant volumetric concentration is neutralized to neutrality for the 10%NaOH aqueous solution, by the interior styrene type copolymer macroporous adsorbent resin glass column that 100g D102, diameter 25mm, high 300mm are housed, carries out adsorbing separation then, reuse volumetric concentration 70% ethanol 500ml washs macroporous resin column after treating whole dried liquid streams, collects whole cleaning mixture at the bottom of post.Again with cleaning mixture by the processing of decolouring of the interior 100g of being equipped with D900, diameter 25mm, high 300mm acrylic type copolymer weakly-basic anion exchange macroporous resin glass column, at the bottom of post, collect whole destaining solution then.The vacuum concentration cleaning mixture is to original volume about 1/20 under 50 ℃ of temperature, and spray drying obtains the light glycosides content of color than higher sweet tea extract under 80 ℃ of temperature.Get 98g xylitol and the above-mentioned sweet tea extract mixing that obtains again, adding the 4ml volumetric concentration again is that 95% ethanol was fully stirring about 20 minutes under 30 ℃ of temperature, and then it is left standstill about 30 minutes, after obtaining bright crystalline thing, dry under 80 ℃ of temperature, sterilization promptly get water content and are lower than 5% finished product.
Embodiment 3:
Get not have and go rotten, the pure sweet tea cured leaf of no insect pest 200g uses 2000ml boiling tap water 2 hours, after filtering with filter cloth, gets 1 hour after-filtration of its filtering residue reuse 1600ml boiling tap water, merges twice filtrate and gets the about 3000ml of extracting solution.In extracting solution, add aqua calcis, make its pH value=11, and with its static 1 hour, the reuse gradient method separates supernatant with precipitate, supernatant is neutralized to neutrality with volumetric concentration 10%NaOH aqueous solution, by the interior styrene type copolymer macroporous adsorbent resin glass column that 100gAB-8, diameter 25mm, high 300mm are housed, carries out adsorbing separation then, reuse volumetric concentration 70% ethanol 500ml washs macroporous resin column after treating whole dried liquid streams, collects whole cleaning mixture at the bottom of post.Again with cleaning mixture by the processing of decolouring of the interior 100g of being equipped with D280, diameter 25mm, high 300mm acrylic type copolymer weakly-basic anion exchange macroporous resin glass column, at the bottom of post, collect whole destaining solution then.The vacuum concentration cleaning mixture is to original volume about 1/20 under 60 ℃ of temperature, and spray drying obtains the light glycosides content of color than higher sweet tea extract under 80 ℃ of temperature.Get 294g erythritol and the above-mentioned sweet tea extract mixing that obtains again, adding the 8ml volumetric concentration again is that 90% ethanol was fully stirring about 20 minutes under 30 ℃ of temperature, and then it is left standstill about 30 minutes, after obtaining bright crystalline thing, dry under 85 ℃ of temperature, sterilization promptly get water content and are lower than 5% finished product.
Claims (8)
1, the manufacture method of the low heat energy sweet tea sugar of a kind of sugar-free, its step is as follows:
1) chooses 50～200 weight portion sweet tea cured leafs;
2) sweet tea cured leaf water is carried, merged water extract and filtration;
3) in filtrate, add the bivalent cation material and make its pH value=9～12, treat contamination precipitation after, sediment separate out;
4) get its supernatant, the supernatant pH value is neutralized to neutrality, carry out adsorbing separation with nonpolar macroporous adsorption resin;
5) use ethanol elution;
6) eluent reuse weakly-basic anion macropore ion exchange resin is decoloured;
7) destaining solution is carried out vacuum concentration under 30～60 ℃;
8) be dried again, get the sweet tea extract;
9) add 50～200 weight portion plant fermentation multi-sugar alcohols and sweet tea extract mixing, add 1～12 weight portion, volumetric concentration again and be ethanol fully stirring under 30～50 ℃ of temperature of 85%～100%, and leave standstill and treat its enclose recrystallization;
10) be dried finished product.
2, the manufacture method of the low heat energy sweet tea sugar of sugar-free according to claim 1, it is characterized in that: the each component raw material is as follows in the weight portion proportioning:
Sweet tea cured leaf 40～60
Plant fermentation multi-sugar alcohol 80～100.
3, the manufacture method of the low heat energy sweet tea sugar of sugar-free according to claim 2, it is characterized in that: described plant fermentation multi-sugar alcohol is erythritol or xylitol.
4, the manufacture method of the low heat energy sweet tea sugar of sugar-free according to claim 2, it is characterized in that: described bivalent cation material is calcium salt or magnesium salt.
5, the manufacture method of the low heat energy sweet tea sugar of sugar-free according to claim 2, it is characterized in that: described vacuum concentration temperature is 50～70 ℃.
6, the manufacture method of the low heat energy sweet tea sugar of sugar-free according to claim 2, it is characterized in that: described twice exsiccant temperature is 80～90 ℃.
7, the manufacture method of the low heat energy sweet tea sugar of sugar-free according to claim 4, it is characterized in that: described calcium salt is Ca (OH)
2, described magnesium salt is MgCO
3
8, the low heat energy sweet tea sugar of sugar-free of the described method manufacturing of claim 1～7.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100227558A CN1309843C (en) | 2004-06-04 | 2004-06-04 | Tea candy without sugar and with low calorie and its production |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB2004100227558A CN1309843C (en) | 2004-06-04 | 2004-06-04 | Tea candy without sugar and with low calorie and its production |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1582702A true CN1582702A (en) | 2005-02-23 |
| CN1309843C CN1309843C (en) | 2007-04-11 |
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| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB2004100227558A Expired - Fee Related CN1309843C (en) | 2004-06-04 | 2004-06-04 | Tea candy without sugar and with low calorie and its production |
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Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102150775A (en) * | 2011-01-07 | 2011-08-17 | 陈显刚 | Sweetener and preparation method thereof |
| CN103004989A (en) * | 2012-11-30 | 2013-04-03 | 崇左市天添乳品厂 | Mulberry buffalo milk and preparation method thereof |
| CN104262427A (en) * | 2014-09-30 | 2015-01-07 | 桂林三宝药业有限公司 | Method for extracting rubusoside from sweet tea leaves |
| EP3033949A1 (en) | 2013-12-23 | 2016-06-22 | International Flavors & Fragrances Inc. | Transglucosylated rubus suavissimus extract and methods of preparation and use |
-
2004
- 2004-06-04 CN CNB2004100227558A patent/CN1309843C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102150775A (en) * | 2011-01-07 | 2011-08-17 | 陈显刚 | Sweetener and preparation method thereof |
| CN102150775B (en) * | 2011-01-07 | 2012-12-19 | 陈显刚 | Sweetener and preparation method thereof |
| CN103004989A (en) * | 2012-11-30 | 2013-04-03 | 崇左市天添乳品厂 | Mulberry buffalo milk and preparation method thereof |
| EP3033949A1 (en) | 2013-12-23 | 2016-06-22 | International Flavors & Fragrances Inc. | Transglucosylated rubus suavissimus extract and methods of preparation and use |
| CN104262427A (en) * | 2014-09-30 | 2015-01-07 | 桂林三宝药业有限公司 | Method for extracting rubusoside from sweet tea leaves |
| CN104262427B (en) * | 2014-09-30 | 2017-02-01 | 桂林三宝药业有限公司 | Method for extracting rubusoside from sweet tea leaves |
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| Publication number | Publication date |
|---|---|
| CN1309843C (en) | 2007-04-11 |
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Granted publication date: 20070411 Termination date: 20160604 |