CN1412287A - Essence, its preparation and application - Google Patents
Essence, its preparation and application Download PDFInfo
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- CN1412287A CN1412287A CN 01135906 CN01135906A CN1412287A CN 1412287 A CN1412287 A CN 1412287A CN 01135906 CN01135906 CN 01135906 CN 01135906 A CN01135906 A CN 01135906A CN 1412287 A CN1412287 A CN 1412287A
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- essence
- spices
- nano silicon
- based oxide
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- Fats And Perfumes (AREA)
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Abstract
The present invention provides an essence, its preparation method and application. It is made up by using nano silicone base oxide and perfume as raw material and adopting a synthesis process, including physical adsorption and chemical combination. Its fragrance can be uniformly and durably released out, and its quality is stable. It not only can be directly made into various products, but also can be added into other various materials to produce various pefumed products.
Description
Technical field
What the present invention relates to is a kind of essence and its production and use.
Background technology
Essence and daily life relation are very close, are tobacco foodstuffs industry, medical and health industry, daily chemical industry and other industrial indispensable important source material.According to medical evidence, but the fragrance Ginseng Extract, and steadily function of human body makes us relaxed and joyful.Along with improving constantly of quality of life standard, people are more and more big to the demand of essence product, and are also more and more high to the requirement of essence quality simultaneously.The essence of people's use at present its fragrance is in the ordinary course of things held time below 100 days, the stable effective ingredients of essence is poor, the volatilization of fragrance is subject to the influence of envrionment temperature, humidity and causes the fragrance volatilization inhomogeneous, essence adds its fragrance malleable of back in other products, and these essence are also more perishable.
Summary of the invention
At above problem, the technical problem to be solved in the present invention will provide a kind of guarantor fragrant lasting exactly, stores convenient transportation, and the fragrance volatilization evenly can be added in multiple product and the fragrance not essence of malleable and the preparation method and the purposes of this essence.
Essence provided by the invention, it forms so that nano silicon-based oxide and spices are synthetic, and also just saying so with the nano silicon-based oxide is that base-material constitutes after with spices physical adsorption and Chemical bond.
The preparation method of essence provided by the invention makes after making spices and nano silicon-based oxide synthetic.So-called synthesizing is exactly that nano silicon-based oxide carries out physical adsorption and Chemical bond to spices.Wherein spices can be selected the spices of any kind of for use, comprises natural animal perfume material, plant perfume and synthetic spices, and can these spices be allocated use arbitrarily according to desired flavor type.The add-on of nano silicon-based oxide according to the synthesis capability of selected spices and nano silicon-based oxide between the 30-90% of gross weight.
The preparation method of essence provided by the invention is spices to be distilled to generate spices steam earlier, again nano silicon-based oxide and spices steam are synthesized, after cooling drying form.Spices steam is the water vapor of carrying the spices mist of oil secretly that produces in still-process.
The preparation method of essence provided by the invention, the synthetic of nano silicon-based oxide and spices steam is spices steam importing steam condenser to be sprayed into nano silicon-based oxide in the steam condenser simultaneously carry out with the mode of spices vapor mixing.
The preparation method of essence provided by the invention also can be dissolved dispersion with spices earlier in ethanol, nano silicon-based oxide is dispersed in this solution again, removes ethanol at last and makes.In this method, also can select the organic solvent of other kinds for use, as long as this organic solvent neither can learn reaction with essence, can not carry out chemical reaction, certainly also otherwise can influence the functions of use of essence with nano silicon-based oxide yet.
The preparation method of essence provided by the invention, the purity of the nano silicon-based oxide of employing be more than 90%, the particle initial size between 10-30nm, aggregation size≤100nm, particle shape is spherical, the surface is how little mesoporous and have a large amount of hydroxyls and a residual bond.The trade mark of producing as Zhoushan Tomorrow Nanomaterials Co., Ltd is the nano silicon-based oxide of SP1, DP1, HP1.
The purposes of essence provided by the invention is a product of essence provided by the invention and various carrier being made volatilization fragrance.
The purposes of essence provided by the invention is to use as perfume or air aromatic after becoming liquid state or clay shape essence to pour into aerosolizer directly or with liquid flavor with alcohol dilution in essence provided by the invention, extension rate be 1-10 doubly.
The purposes of essence provided by the invention, essence provided by the invention can be added in the various materials and manufacture flavor article, and addition is at 0.1%-20%.As be added in various fibers and the fibre product and make the fragrance textile fabrics, be added on and make the fragrance plasthetics in the plastic cement, be added on and make paper product, printed matter in the paper, or be added in coating, the makeup even penetrate in the bamboo wood and make panoramic perfumed product or the like.
The preparation method of essence provided by the invention, adopting spices and nano silicon-based oxide is raw material.Nano silicon-based oxide is as base-material, its surface energy height, is rich in little mesoporous (little mesoporous aperture 0.5-0.7nm) and particle surface exists a large amount of hydroxyls and residual bond.The flavor compounds molecular diameter is generally less than 0.1nm, and there are many unsaturated link(age)s on the surface.Both mix back easy generation physical adsorption and Chemical bond and synthesize, the many flavor compounds molecules of the little mesoporous the inside inspiration of nano particle after physical adsorption and Chemical bond, and the outside is also coated by many flavor compounds molecules.The preparation method of essence provided by the invention sprays into the method for spices steam or in organic solvent both are carried out the blended method, makes both obtain fully, synthesize completely with nano silicon-based oxide.The preparation method of essence provided by the invention, it is simple also to have equipment, processing ease, characteristics such as cost is low.Essence provided by the invention because the nano silicon-based oxide particle is to the absorption of flavor compounds molecule, thereby guaranteed evenly lasting release of its fragrance and makes the fragrance hold-time more than 200 days; In addition because the Chemical bond of nano silicon-based oxide particle and flavor compounds molecule makes essence form a kind of stable status, so also not perishable.In addition because nano particle diameter is little, foreign matter content is few and transparent, the flavor compounds molecule is again a small molecules, both have very high transparency and perviousness after making essence, can not only directly make various essence goods and be applied to all kinds of places and make it air delicate fragrance, and can make an addition to the outward appearance of making various flavor articles in the various materials and not influencing goods.Because slowly-releasing, persistent advantage that essence provided by the invention had, in these purposes, the addition of essence can suitably reduce, thereby has reduced the production cost of flavor article.As seen it is lasting that essence provided by the invention possesses the perfume of guarantor, and the fragrance volatilization is evenly never degenerated, and the characteristics of easily preserving and transporting also have been widely used.
Embodiment
Embodiment 1: present embodiment has proposed following several essence:
| Odor type | Nano silicon-based oxide content (%) |
| Rose | ????30 |
| Jasmine | ????75 |
| Moschus | ????35 |
| Turmeric | ????50 |
| Narcissus | ????45 |
| Almond | ????60 |
| Santal | ????80 |
| Lemon | ????55 |
| Apple | ????40 |
| Fragrant thoroughwort | ????70 |
Embodiment 2: the water distillation that 1000 gram roseleafs is immersed in still pot, after treating that mixing steam that liquid level top forms spice oil and water is spices steam, this spices steam is imported in the condenser, simultaneously 200 gram nano silicon-based oxides are sprayed into this condenser with atomizer, make both thorough mixing synthetic, then through cooling and the dry powdery essence that obtains with rose scent.
Embodiment 3: 100 gram cream jasmin frances are distilled in still pot, the mixing steam of spice oil that the liquid level top is formed and water imports in the condenser then, simultaneously 200 gram nano silicon-based oxides are sprayed into condenser, make both thorough mixing synthetic, then through cooling and the dry essence that obtains with Flower of Arabian Jasmine fragrance.
Embodiment 4: 20 gram Moschus are submerged in the still pot that fills water distill, the mixing steam of spice oil that the liquid level top is formed and water imports in the condenser then, simultaneously 200 gram nano silicon-based oxides are sprayed into condenser, make both thorough mixing synthetic, then through cooling and the dry essence that just can obtain with the Moschus flavor.
Embodiment 5: apple spice 50 grams are dissolved in the 300 gram ethanol (chemical pure), then 100 gram nano silicon-based oxides are well dispersed in this solution, to this mixed solution heating ethanol is volatilized fully at last and obtain the essence of apple fragrance type.
Embodiment 6: fragrant thoroughwort spices 100 grams are dissolved in the 300 gram ethanol (chemical pure), then 100 gram nano silicon-based oxides are well dispersed in this solution, to this mixed solution heating ethanol is volatilized fully at last and obtain the essence of fragrant thoroughwort odor type.
Embodiment 7: will then pour into the essence sprays that makes jasmine fragrance in the aerosolizer with 10 gram jasmine fragrance essence provided by the invention abundant dispersion in 50 gram ethanol.
Embodiment 8: essence 2 grams of rose scent provided by the invention are added in the paper pulp of producing paper handkerchief, produce the paper handkerchief of 1000 gram rose scents.
Claims (9)
1, a kind of essence is characterized in that it forms so that nano silicon-based oxide and spices are synthetic.
2, the preparation method of essence as claimed in claim 1 makes after it is characterized in that making spices and nano silicon-based oxide synthetic.
3, the preparation method of essence as claimed in claim 2 is characterized in that its technological process is spices to be distilled to generate spices steam earlier, and is again that nano silicon-based oxide and spices steam is synthetic, at last with the resultant cooling drying.
4, the preparation method of essence as claimed in claim 3 is characterized in that the synthetic of nano silicon-based oxide and spices steam is to carry out with the mode of spices vapor mixing so that spices steam importing steam condenser is sprayed into nano silicon-based oxide in the steam condenser simultaneously.
5, the preparation method of essence as claimed in claim 2 is characterized in that its technological process is earlier spices to be dissolved dispersion in ethanol, nano silicon-based oxide is dispersed in this solution again, removes ethanol at last.
6, as the preparation method of claim 2 or 3 or 4 or 5 described essence, the purity that it is characterized in that the nano silicon-based oxide that adopted is more than 90%, the particle initial size is between 10-30nm, aggregation size≤100nm, particle shape is spherical, and the surface is how little mesoporous and have a large amount of hydroxyls and a residual bond.
7, the purposes of essence as claimed in claim 1 is characterized in that essence and various carrier are made the product of volatilization fragrance.
8, as the purposes of claim 1 or 7 described essence, it is characterized in that using as perfume or air aromatic after essence becomes liquid state or clay shape essence to pour into aerosolizer directly or with liquid flavor with alcohol dilution, extension rate be 1-10 doubly.
9, as the purposes of claim 1 or 7 described essence, it is characterized in that essence is added in the various materials and manufacture flavor article, addition is at 0.1%-20%.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01135906 CN1412287A (en) | 2001-10-16 | 2001-10-16 | Essence, its preparation and application |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 01135906 CN1412287A (en) | 2001-10-16 | 2001-10-16 | Essence, its preparation and application |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1412287A true CN1412287A (en) | 2003-04-23 |
Family
ID=4673343
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN 01135906 Pending CN1412287A (en) | 2001-10-16 | 2001-10-16 | Essence, its preparation and application |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1412287A (en) |
Cited By (5)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1943650B (en) * | 2006-10-30 | 2011-04-20 | 韩倩琰 | Rose liquid eye drops |
| CN104109985A (en) * | 2014-07-16 | 2014-10-22 | 广东华泰纸业有限公司 | Method for producing fragrant newsprinting paper |
| CN104988741A (en) * | 2015-06-11 | 2015-10-21 | 江苏阳光股份有限公司 | Fragrance easy-care treating method of cotton shirt |
| CN105011361A (en) * | 2015-07-17 | 2015-11-04 | 云南中烟工业有限责任公司 | Method for preparing liquid molecules-embedded non-flammable perfuming material |
| CN111420478A (en) * | 2020-04-08 | 2020-07-17 | 东莞市艾尔佳过滤器制造有限公司 | Long-acting slow-release fragrance air conditioner filter element and processing method thereof |
-
2001
- 2001-10-16 CN CN 01135906 patent/CN1412287A/en active Pending
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1943650B (en) * | 2006-10-30 | 2011-04-20 | 韩倩琰 | Rose liquid eye drops |
| CN104109985A (en) * | 2014-07-16 | 2014-10-22 | 广东华泰纸业有限公司 | Method for producing fragrant newsprinting paper |
| CN104988741A (en) * | 2015-06-11 | 2015-10-21 | 江苏阳光股份有限公司 | Fragrance easy-care treating method of cotton shirt |
| CN105011361A (en) * | 2015-07-17 | 2015-11-04 | 云南中烟工业有限责任公司 | Method for preparing liquid molecules-embedded non-flammable perfuming material |
| CN105011361B (en) * | 2015-07-17 | 2018-11-09 | 云南中烟工业有限责任公司 | A kind of preparation method of the embedded non-burning flavoring material of fluid molecule |
| CN111420478A (en) * | 2020-04-08 | 2020-07-17 | 东莞市艾尔佳过滤器制造有限公司 | Long-acting slow-release fragrance air conditioner filter element and processing method thereof |
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| C06 | Publication | ||
| PB01 | Publication | ||
| C02 | Deemed withdrawal of patent application after publication (patent law 2001) | ||
| WD01 | Invention patent application deemed withdrawn after publication |