CN1360897A - Bee glue purifying technological process - Google Patents
Bee glue purifying technological process Download PDFInfo
- Publication number
- CN1360897A CN1360897A CN00137060A CN00137060A CN1360897A CN 1360897 A CN1360897 A CN 1360897A CN 00137060 A CN00137060 A CN 00137060A CN 00137060 A CN00137060 A CN 00137060A CN 1360897 A CN1360897 A CN 1360897A
- Authority
- CN
- China
- Prior art keywords
- bee glue
- filtrate
- propolis
- hot air
- air drying
- Prior art date
- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
- Granted
Links
- 239000003292 glue Substances 0.000 title claims abstract description 12
- 238000000034 method Methods 0.000 title claims abstract description 10
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 claims abstract description 21
- 239000002904 solvent Substances 0.000 claims abstract description 5
- 238000001914 filtration Methods 0.000 claims abstract description 4
- 238000004821 distillation Methods 0.000 claims abstract description 3
- 241000241413 Propolis Species 0.000 claims description 21
- 229940069949 propolis Drugs 0.000 claims description 21
- 239000000706 filtrate Substances 0.000 claims description 9
- 238000007602 hot air drying Methods 0.000 claims description 9
- 230000001476 alcoholic effect Effects 0.000 claims description 7
- 239000000796 flavoring agent Substances 0.000 claims description 5
- 235000019634 flavors Nutrition 0.000 claims description 5
- 238000009413 insulation Methods 0.000 claims description 5
- 230000015572 biosynthetic process Effects 0.000 claims description 4
- 238000005470 impregnation Methods 0.000 claims description 4
- 239000012535 impurity Substances 0.000 claims description 4
- 239000007788 liquid Substances 0.000 claims description 4
- 238000010992 reflux Methods 0.000 claims description 4
- 239000007787 solid Substances 0.000 claims description 4
- 239000012467 final product Substances 0.000 claims description 3
- 239000000843 powder Substances 0.000 abstract description 8
- 238000001816 cooling Methods 0.000 abstract description 4
- 239000003146 anticoagulant agent Substances 0.000 abstract 1
- 229940127219 anticoagulant drug Drugs 0.000 abstract 1
- 230000015271 coagulation Effects 0.000 abstract 1
- 238000005345 coagulation Methods 0.000 abstract 1
- 238000001035 drying Methods 0.000 abstract 1
- 238000000605 extraction Methods 0.000 abstract 1
- 230000000284 resting effect Effects 0.000 abstract 1
- 230000000694 effects Effects 0.000 description 3
- 239000012530 fluid Substances 0.000 description 3
- 239000000047 product Substances 0.000 description 3
- 239000003795 chemical substances by application Substances 0.000 description 2
- 230000002950 deficient Effects 0.000 description 2
- 238000010438 heat treatment Methods 0.000 description 2
- 239000000463 material Substances 0.000 description 2
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 description 2
- 239000001993 wax Substances 0.000 description 2
- 241000233866 Fungi Species 0.000 description 1
- 206010061218 Inflammation Diseases 0.000 description 1
- 229910004298 SiO 2 Inorganic materials 0.000 description 1
- VYPSYNLAJGMNEJ-UHFFFAOYSA-N Silicium dioxide Chemical compound O=[Si]=O VYPSYNLAJGMNEJ-UHFFFAOYSA-N 0.000 description 1
- 230000004523 agglutinating effect Effects 0.000 description 1
- 239000007766 cera flava Substances 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 201000010099 disease Diseases 0.000 description 1
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 1
- 239000003814 drug Substances 0.000 description 1
- 229940079593 drug Drugs 0.000 description 1
- 230000004054 inflammatory process Effects 0.000 description 1
- 239000012188 paraffin wax Substances 0.000 description 1
- 238000000746 purification Methods 0.000 description 1
- 230000028327 secretion Effects 0.000 description 1
- 230000032258 transport Effects 0.000 description 1
Landscapes
- Jellies, Jams, And Syrups (AREA)
- Medicines Containing Plant Substances (AREA)
Abstract
The technological process of purifying bee glue includes the steps of: extraction of coarse bee glue with ethanol solution and solvent, resting, filtering, distillation to receover ethanol, hot wind drying, cooling, crushing, etc. Compared with available technology, the present invention is simple, practical and low in cost. The wax content and other indexes of prepared bee glue product have reached the standard for natural bee glue and has high heat stability and no coagulation at normal temperature, so that it may be produced into bee glue powder without adding anticoagulant for further use.
Description
The present invention relates to a kind of process of bee glue purifying.
Propolis is Apis herborization axillalry bud secretions and mixes self goods and materials, and be applied in the material on Nidus Vespae slit or the inwall, it has good fungus and mildew resistance effect, and inflammation and the diseases many for the mankind have special curative effect, are a kind of natural medicines.Owing to contain more Cera Flava and other impurity in the natural propolis, therefore must could use through purifying.Chinese patent CN1151867A discloses a kind of purification and flouring technology of propolis, and it passes through following steps substantially:
1, thick propolis (picking up from the propolis of Nidus Vespae without any processing) is placed in the water and dissolves.
2, heating dewaxing: be about to be soaked with the water heating of thick propolis, emerge after the feasible wax dissolving wherein, reach separating effect.
3, separate after the waxiness propolis is extracted (as ethanol etc.), filtering and impurity removing with solvent.
4, solvent is reclaimed, obtain the propolis fluid extract.
5, as need powder process, the propolis fluid extract can be crushed to 120 order to 140 orders behind hot air drying, for making at room temperature or being lower than under the room temperature non-cakedly slightly, often add the ratio that the anti-agglomerating agent SiO 2 powder reaches 13-20%.
Adopt the propolis after above-mentioned prior art is purified still to contain wax, fusing point is lower, can only be fluid extract usually, is not easy further processing and use, transports, stores all inconvenient.And after hot air drying adds silicon dioxide powder, though solved agglutinating deficiency, gained be bee glue product in fact, and non-natural propolis extract, its application has been subjected to certain limitation.The defective of existing product is unreasonable the causing of process by prior art.
Purpose of the present invention be exactly provide in order to overcome the defective that above-mentioned prior art exists that a kind of technology is simple, the product dewaxing fully, be difficult for the process of the bee glue purifying of bonding, Heat stability is good.
Purpose of the present invention can be achieved through the following technical solutions: a kind of process of bee glue purifying, be characterized in, and comprise following processing step:
(1) thick propolis is directly added in the solvent alcoholic solution extract, reflux obtained extracting solution in 30 to 360 minutes in reflux, or merceration obtained impregnation liquid in 1 to 15 day, and the weight ratio of described thick propolis and alcoholic solution is 1: 3 to 1: 10;
(2) with extracting solution or impregnation liquid filtering and impurity removing, filtrate is left standstill, and insulation is 2 to 30 hours in the environment below 15 ℃;
(3) above-mentioned filtrate after standing is filtered with 80 to 400 purpose sieve apertures again;
(4) filtrate that obtains is carried out distilling under reduced pressure and is reclaimed ethanol, does not have the alcohol flavor until distillation;
(5) after the solid formation that distilling under reduced pressure is obtained leaves standstill 3 to 4 days, place 8 mesh sieves or pallet, with less than 100 ℃ hot air drying 30 to 240 minutes;
(6) solid formation behind the hot air drying is cooled off, the reuse pulverizer is crushed to 20 to 80 orders and gets final product.
Compared with prior art, technology of the present invention is simple, practical, cost is low, the propolis paraffin content that adopts prepared of the present invention is less than 3% weight, and other indexs meet the standard of natural propolis, and fusing point is more than 55 ℃, Heat stability is good, noncondensing under the room temperature, needn't add anti-agglomerating agent and get final product powder process, the propolis powder of making is convenient to further use very much.
Below in conjunction with embodiment, the invention will be further described.
Embodiment 1:
Thick propolis is added the alcoholic solution of 10 times of weight, and merceration 15 days filters rear filtrate and leaves standstill, and insulation is 30 hours in 0 to 15 ℃ of environment; Filter 400 orders, reclaim ethanol to there not being the alcohol flavor in 60 ℃ of vacuum concentrating apparatus, take out, place and dried 3-4 days, be put in 8 mesh sieves or other pallets with 60 ℃ hot air drying 240 minutes, cooling is crushed to 20 to 80 purpose powder.
Embodiment 2:
Thick propolis is added the alcoholic solution of 6 times of weight, be heated to and refluxed 2 hours, be chilled to room temperature, filter, filtrate is left standstill, and insulation is 30 hours in environment below 12 ℃.Filter 200 orders, in 60 ℃ of vacuum concentrating apparatus, reclaim ethanol, take out, place and dried 3-4 days to there not being the alcohol flavor, with in 8 mesh sieves or other pallets with 40 ℃ hot air drying 180 minutes, cooling is crushed to 20 to 80 purpose powder.
Embodiment 3:
Thick propolis is added the alcoholic solution of 4 times of weight, be heated to and refluxed 0.5 hour, be chilled to room temperature, filter, filtrate is left standstill, and insulation is 2 hours in-2 ℃ of environment.Filter 80 orders, in 60 ℃ of vacuum concentrating apparatus, reclaim ethanol, take out, place and dried 3-4 days to there not being the alcohol flavor, with in 8 mesh sieves or other pallets with 85 ℃ hot air drying 30 minutes, cooling is crushed to 20 to 80 purpose powder.
Claims (1)
1, a kind of process of bee glue purifying is characterized in that, comprises following processing step:
(1) thick propolis is directly added in the solvent alcoholic solution extract, reflux obtained extracting solution in 30 to 360 minutes in reflux, or merceration obtained impregnation liquid in 1 to 15 day, and the weight ratio of described thick propolis and alcoholic solution is 1: 3 to 1: 10;
(2) with extracting solution or impregnation liquid filtering and impurity removing, filtrate is left standstill, and insulation is 2 to 30 hours in the environment below 15 ℃;
(3) above-mentioned filtrate after standing is filtered with 80 to 400 purpose sieve apertures again;
(4) filtrate that obtains is carried out distilling under reduced pressure and is reclaimed ethanol, does not have the alcohol flavor until distillation;
(5) after the solid formation that distilling under reduced pressure is obtained leaves standstill 3 to 4 days, place 8 mesh sieves or pallet, with less than 100 ℃ hot air drying 30 to 240 minutes;
(6) solid formation behind the hot air drying is cooled off, the reuse pulverizer is crushed to 20 to 80 orders and gets final product.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB00137060XA CN1188139C (en) | 2000-12-28 | 2000-12-28 | Bee glue purifying technological process |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CNB00137060XA CN1188139C (en) | 2000-12-28 | 2000-12-28 | Bee glue purifying technological process |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1360897A true CN1360897A (en) | 2002-07-31 |
| CN1188139C CN1188139C (en) | 2005-02-09 |
Family
ID=4597648
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CNB00137060XA Expired - Fee Related CN1188139C (en) | 2000-12-28 | 2000-12-28 | Bee glue purifying technological process |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1188139C (en) |
Cited By (7)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1330296C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis soft capsule and its preparation method |
| CN1330256C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis honey sweets and preparation process |
| CN101966491A (en) * | 2010-10-20 | 2011-02-09 | 苏州光韵达光电科技有限公司 | Sieve plate for centrifugal drying machine |
| CN101390884B (en) * | 2008-10-23 | 2011-05-11 | 陈宜斗 | No-alcohol preparation method of natural propolis |
| CN102973609A (en) * | 2012-11-30 | 2013-03-20 | 扬州大学 | Propolis ethanol extract for treating alcoholic fatty liver, preparation method and applications in production of enteric-coated tablets |
| CN103655628A (en) * | 2013-10-11 | 2014-03-26 | 中国农业科学院蜜蜂研究所 | Propolis extract and application thereof |
| CN109198352A (en) * | 2018-09-14 | 2019-01-15 | 杭州和蜂园保健品有限公司 | A kind of propolis solid beverage powder and preparation method thereof |
-
2000
- 2000-12-28 CN CNB00137060XA patent/CN1188139C/en not_active Expired - Fee Related
Cited By (9)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1330296C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis soft capsule and its preparation method |
| CN1330256C (en) * | 2003-06-08 | 2007-08-08 | 刘进祖 | Propolis honey sweets and preparation process |
| CN101390884B (en) * | 2008-10-23 | 2011-05-11 | 陈宜斗 | No-alcohol preparation method of natural propolis |
| CN101966491A (en) * | 2010-10-20 | 2011-02-09 | 苏州光韵达光电科技有限公司 | Sieve plate for centrifugal drying machine |
| CN102973609A (en) * | 2012-11-30 | 2013-03-20 | 扬州大学 | Propolis ethanol extract for treating alcoholic fatty liver, preparation method and applications in production of enteric-coated tablets |
| CN102973609B (en) * | 2012-11-30 | 2014-07-09 | 扬州大学 | Propolis ethanol extract for treating alcoholic fatty liver, preparation method and applications in production of enteric-coated tablets |
| CN103655628A (en) * | 2013-10-11 | 2014-03-26 | 中国农业科学院蜜蜂研究所 | Propolis extract and application thereof |
| CN103655628B (en) * | 2013-10-11 | 2015-12-09 | 中国农业科学院蜜蜂研究所 | A kind of propolis extract and application thereof |
| CN109198352A (en) * | 2018-09-14 | 2019-01-15 | 杭州和蜂园保健品有限公司 | A kind of propolis solid beverage powder and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1188139C (en) | 2005-02-09 |
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Legal Events
| Date | Code | Title | Description |
|---|---|---|---|
| C10 | Entry into substantive examination | ||
| SE01 | Entry into force of request for substantive examination | ||
| C06 | Publication | ||
| PB01 | Publication | ||
| C14 | Grant of patent or utility model | ||
| GR01 | Patent grant | ||
| ASS | Succession or assignment of patent right |
Owner name: REN JIANLI Free format text: FORMER OWNER: SHANGHAI DACHENG BIOLOGICAL PRODUCTS CO., LTD. Effective date: 20050408 |
|
| C41 | Transfer of patent application or patent right or utility model | ||
| TR01 | Transfer of patent right |
Effective date of registration: 20050408 Address after: 200030 No. 666, 8 Hongqiao Road, Shanghai, 1603 Patentee after: Ren Jianli Address before: 201804 Shanghai Jiading District Huangdu New Huang Road No. 136 B Patentee before: Dacheng Biologic Products Co., Ltd., Shanghai |
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| C19 | Lapse of patent right due to non-payment of the annual fee | ||
| CF01 | Termination of patent right due to non-payment of annual fee |