CN1360213A - Tracing technique for detecting micro substance between wells in oil field - Google Patents

Tracing technique for detecting micro substance between wells in oil field Download PDF

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Publication number
CN1360213A
CN1360213A CN 01138834 CN01138834A CN1360213A CN 1360213 A CN1360213 A CN 1360213A CN 01138834 CN01138834 CN 01138834 CN 01138834 A CN01138834 A CN 01138834A CN 1360213 A CN1360213 A CN 1360213A
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well
tracer agent
oil
water
tracer
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CN1166964C (en
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刘安建
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Beijing Siwei trend Energy Technology Co., Ltd.
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刘安建
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Abstract

A micro substance tracing detection technique between wells in oil field is characterized by that the micro substance in the strata water and water-source water in oil field is used as tracing agent, and a tracing agent explaining software is used to process the test result of sample, obtaining dynamic parameters. Its advantages are high feasibility, adaptability and resolution, low cost and stable performance.

Description

Tracing technique for detecting micro substance between wells in oil field
The present invention relates to a kind of measuring technology that oilfield development process measures formation fluids, displacement state information that is used for.
In oilfield development process, for in time, analyze exactly, grasp by the displacement of various fluids such as oil, gas, water in the exploitation oil reservoir, migration situation and dynamic, so that take to develop the adjustment scheme accordingly and measure improves development effectiveness, the spike measuring technology is monitored relevant oil, gas, well between needs employing well, the admission related data.Since over half a century, the spike measuring technology has experienced the development course of chemical tracer-radioisotope tracer-non radioactive isotope tracer agent between the well of domestic and international oil field.Wherein, the first generation chemical tracers such as inorganic salts, dyestuff, halogenated hydrocarbons and alcohols that adopt the fifties need the mining site operation, and consumption is big, the cost height, adaptability and alternative poor, measuring resolution is low, and the part tracer agent brings influence to well logging, well logging interpretation and back processing, and drawbacks such as environment and personal security problem are arranged, be superseded gesture gradually; Though seventies research, what use is that the second generation radioisotope tracer of representative has few, the easy to detect and detection resolution of consumption than advantages such as height with tritium and tritide, but owing to have radioactivity, unfavorable to personnel, Environmental security, its application is restricted; The research eighties, the third generation tracer agent of using are representative with deuterium and compound thereof, advantage is same as the second generation, and the environment and the safety problem of mining site input oil-water well, sampling, management etc. have been overcome, but because non radioactive isotope tracer agent kind still less, only be not to be allowed to condition at mining site in use to demonstrate radioactivity, still need activate after the sampling by indoor atomic pile, measure its radioactivity with neutron activation method, and can only carry out indoor detecting operation by International Atomic Energy Agency, and analytical test is numerous and diverse, the expense costliness makes its application limited.
The object of the present invention is to provide a kind of both easy to detectly, the detection resolution height can obtain oil reservoir and annotate sampled-current body multidate information, and tracing technique for detecting micro substance between wells in oil field expensive less, that personnel's environment do not had injury.
Measuring technology provided by the invention is to realize like this.This kind measuring technology is to carry out on the basis of background concentration high resolving power total analysis at local water and source water to monitored oil field or oil well, find out wherein do not have or very one or more (on oil well single or multi-section multi-layer decide) high purity elements of trace as tracer material, it is processed into liquid, gas or the pressed powder synchronous with tracked fluid, press the reservoir condition design quantity, add or the mining site injection from well head; Then, by observing well wellhead sampling and sample preparation, purification, on high resolving power test equipment,, and utilize the tracer agent interpretation software that the sample detection result is handled, obtain dynamic parameter tracked tracer agent high speed detection simultaneously; At last, dynamically tracer agent analysis result and software processes result are carried out analysis interpretation, the client is provided required various dynamic datas in conjunction with on-the-spot oil-water well production.The implementation step of this measuring technology is as follows:
1, formulates the test implementation scheme, select, inject well, monitor well pound sign, test purpose, essential implementation, scheduling etc. comprising block, well group, zone of interest;
2, oil-field water is carried out total analysis, determine to select behind the background concentration one or more wherein not have or very the material of trace as tracer agent;
3, calculate definite tracer agent consumption.According to the data such as well spacing, reservoir thickness, factor of porosity, water percentage, percent continuity and instrument lowest detectable limit of well group, follow these steps to and formula calculates the micro substance tracer agent consumption (being generally several hectograms that restrain) of use:
At first, calculate the maximum dilution volume that injects the stratum:
Vp=πr 2·h·φ·Sw·Er
In the formula:
Vp-maximum dilution volume, m 3
The distance of r-injection well and sampled well, m;
H-injection well net thickness, m;
Sw-layer of sand water saturation, %;
Er-percent continuity, %;
φ--factor of porosity, %;
Secondly, calculate the dosage of tracer agent:
A=μ·MDL·Vp
In the formula:
A-tracer agent consumption, gram;
μ-guarantee coefficient;
MDL-instrument lowest detectable limit;
4, inject well by design quantity to tracer agent and add and anticipate tracer agent aqueous solution or the complex solution for preparing, dosing method can adopt the well head specific purpose tool directly to add or adopt waterflood-transmission line to inject at well head;
5, take a sample at monitor well by the sampling system and the requirement of embodiment regulation;
6, utilize resolution can reach ppq level (1 * 10 -15) inductively coupled plasma mass spectrometry instrument (ICP-MS) sample is in time analyzed, and draw the tracer agent production curve;
7, utilize the tracer agent interpretation software that the tracer agent production curve is carried out match, obtain formation parameter distribution situation and actual fluid-channeling channel parameter;
8, according to the formation parameter distribution situation, analyze to inject fluid level channelling situation, by to seeing that tracer agent time, well spacing calculate, obtain channelling direction and speed;
9,, obtain the vertical actual channelling situation of fluid in conjunction with profile-log of water injection or notes vapour well steam entry profile according to actual fluid-channeling channel parameter;
10, utilize above-mentioned match explanation results, analyze main flow, main passage channelling parameter and the connection situation of oozing;
11, according to the geologic model of setting up,, calculate relevant coefficient of heterogeneity (Lorenz constant, V-factor etc.), carry out the situation analysis of oil reservoir heterogeneous body according to conventional oil reservoir heterogeneous body evaluation method;
12, utilize explanation of crude oil or viscous crude migration rule simulation softward and tracer agent numerical simulation software, relevant dynamic and static and production logging data to make an explanation, obtain the remaining oil saturation distribution situation.
Oil field provided by the present invention micro substance well-to-well tracer test technology in recent years in China Liaohe River, North China, long celebrating oil field carried out tentative enforcement and application, and accomplishes the end in view respectively, obtained good result.For example, well group S1+2 oil reservoir to the cold 43 45-164 well groups in Liaohe Oil Field and two exploitation via steam injection viscous crude of 43-164 well group has added 120 grams and 3.5 gram tracer agents at 45-164 well and 43-164 well respectively by above-mentioned implementation step, and test, obtained following achievement:
(1) determined that vapour scurries well steam propulsion speed;
(2) determined vapour scurry direction and streamline and up and down between series of strata vapour scurry situation;
(3) determined that notes vapour involves scope and parameter (area coefficient, volume factor and sweep efficiency);
(4) by numerical simulation, the pressure field of monitoring and calculate well group when annotating tracer breakthrough distributes;
(5) to handling up well and observe between the well vapour on every side and scurry the crack situation and analyze;
(6) reservoir heterogeneity (Lauren magnetic constant, V-factor) is described;
(7) determined oil reservoir group and the quantity that vapour is scurried, stifled vapour or profile control scheme thinking are provided;
(8) determined remaining oil saturation and distribution situation thereof between test well group well.
Measuring technology provided by the invention is easy to implement, easy to detect, tracer agent has that expense is low, wide in variety, adaptability is strong, consumption is few, detection resolution is high, can differentiate single plant and multiple tracer agent, mining site add characteristics such as convenient, no personal safety and environmental problem and stable performance, high-low temperature resistant simultaneously between the well that is adopted, have a extensive future, to monitoring and instructing oil-field development that the important practical meaning is arranged.

Claims (1)

1, a kind of tracing technique for detecting micro substance between wells in oil field, it is characterized in that, this technology be: local water and source water to monitored oil field or oil well carry out on the basis of background concentration high resolving power total analysis, find out wherein do not have or very the trace one or more high purity elements as tracer material, it is processed into liquid, gas or the pressed powder synchronous with tracked fluid, press the reservoir condition design quantity, add or the mining site injection from well head; Then, by observing well wellhead sampling and sample preparation, purification, on high resolving power test equipment,, and utilize the tracer agent interpretation software that the sample detection result is handled, obtain dynamic parameter tracked tracer agent high speed detection simultaneously; At last, dynamically tracer agent analysis result and software processes result are carried out analysis interpretation, the client is provided required various dynamic datas in conjunction with on-the-spot oil-water well production; The implementation step of this measuring technology is as follows:
(1) well, monitor well pound sign, test purpose, essential implementation, scheduling etc. are selected, injected to location survey examination embodiment comprising block, well group, zone of interest;
(2) oil-field water is carried out total analysis, determine to select one or more micro substances as tracer agent behind the background concentration;
(3) calculate to determine the tracer agent consumption,, follow these steps to and formula calculates the micro substance tracer agent consumption of use according to the data such as well spacing, reservoir thickness, factor of porosity, water percentage, percent continuity and instrument lowest detectable limit of well group:
At first, calculate the maximum dilution volume that injects the stratum: Vp=π r 2In the h φ SwEr formula: Vp-maximum dilution volume, n 3The distance of r-injection well and sampled well, m; H-injection well net thickness, m; Sw-layer of sand water saturation, %; Er-percent continuity, %; φ--factor of porosity, %;
Secondly, calculate the dosage of tracer agent:
A=μ·MDL·Vp
In the formula:
B-tracer agent consumption, gram;
μ-guarantee coefficient;
MDL-instrument lowest detectable limit
(4) anticipate the tracer agent for preparing by adding to tracer agent injection well by design quantity, dosing method can adopt the well head specific purpose tool directly to add or adopt waterflood-transmission line to inject at well head;
(5) take a sample at monitor well by the sampling system and the requirement of embodiment regulation;
(6) the inductively coupled plasma mass spectrometry instrument that utilizes resolution can reach the ppq level is in time analyzed sample, and draws the tracer agent production curve;
(7) utilize the tracer agent interpretation software that the tracer agent production curve is carried out match, obtain formation parameter distribution situation and actual fluid-channeling channel parameter;
(8) according to the formation parameter distribution situation, analyze to inject fluid level channelling situation, by to seeing that tracer agent time, well spacing calculate, obtain channelling direction and speed;
(9), obtain the vertical actual channelling situation of fluid in conjunction with profile-log of water injection or notes vapour well steam entry profile according to actual fluid-channeling channel parameter;
(10) utilize above-mentioned match explanation results, analyze main flow, main passage channelling parameter and the connection situation of oozing;
(11) according to the geologic model of setting up,, calculate relevant coefficient of heterogeneity, carry out the situation analysis of oil reservoir heterogeneous body according to conventional oil reservoir heterogeneous body evaluation method;
(12) utilize explanation of crude oil or viscous crude migration rule simulation softward and tracer agent numerical simulation software, relevant dynamic and static and production logging data to make an explanation, obtain the remaining oil saturation distribution situation.
CNB01138834XA 2001-12-13 2001-12-13 Tracing technique for detecting micro substance between wells in oil field Expired - Fee Related CN1166964C (en)

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Cited By (21)

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CN1325942C (en) * 2002-08-23 2007-07-11 中国原子能科学研究院 Perturbation well-to-well tracing test method
GB2438216A (en) * 2006-05-17 2007-11-21 Schlumberger Holdings Methods and systems for evaluation of hydrocarbon reservoirs and associated fluids using biological tags and real-time polymerase chain reaction
CN100489266C (en) * 2005-07-07 2009-05-20 中国石油大学(北京) Method for detecting fluid-channeling channel of oil field
CN1699998B (en) * 2005-06-06 2011-08-31 里群 Constant quantity substance tracer agent for oilfield monitoring and application in oil deposit dynamic monitoring
CN102353750A (en) * 2011-06-03 2012-02-15 中国石油天然气股份有限公司 Crude oil low-temperature oxidation experimental device for light oil reservoir air-injection oil extraction
CN102392636A (en) * 2011-11-03 2012-03-28 中国石油大学(华东) Underground fluid channel parameter description method for water drive development of sandstone reservoir
CN104564049A (en) * 2015-01-22 2015-04-29 中国石油大学(华东) Detection method of polymer flooding and gathering channel
CN101548264B (en) * 2006-10-31 2015-05-13 埃克森美孚上游研究公司 Modeling and management of reservoir systems with material balance groups
CN104747149A (en) * 2015-01-22 2015-07-01 中国石油大学(华东) Detecting method of binary combined flooding agent migration channel
CN104903724A (en) * 2012-11-15 2015-09-09 麦克罗-奇瑟斯公司 Tracer particles, and methods for making same
CN105019894A (en) * 2015-07-29 2015-11-04 长江大学 Method and system for establishing multilayer oil pool inter-well connectivity model
CN106680147A (en) * 2017-01-10 2017-05-17 新疆大学 Application of halohydrin as water injection chemical tracer in oil field
CN106707365A (en) * 2016-12-06 2017-05-24 中国石油大学(华东) Method for monitoring geothermal reservoir temperature and fracture distribution and device thereof
CN106996293A (en) * 2017-05-23 2017-08-01 濮阳市易发化工有限公司 Oil field trace matter detection monitoring technology
CN107989600A (en) * 2017-12-13 2018-05-04 北京捷贝通石油技术有限公司 A kind of water base trace chemistry tracer and the method for measuring water injection well inter well connectivity
CN107989588A (en) * 2017-11-10 2018-05-04 东方宝麟科技发展(北京)有限公司 Utilize each section of oil gas water section method and system of environment-friendly type tracer test horizontal well
CN108691533A (en) * 2018-05-07 2018-10-23 西南石油大学 A kind of profile-log of water injection test device and method based on temperature monitoring
CN109138989A (en) * 2018-08-07 2019-01-04 大庆东方兴盛石油科技服务有限公司 Tracer monitoring technique method
CN110566184A (en) * 2019-09-17 2019-12-13 广西师范大学 Use of14Method for tracing oil field well by C nuclide
CN111257967A (en) * 2020-01-13 2020-06-09 苏州星烁纳米科技有限公司 Oil field tracer and oil field tracing method
CN117808986A (en) * 2024-01-08 2024-04-02 成都北方石油勘探开发技术有限公司 Water-drive reservoir dominant channel identification and quantification method

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CN1325942C (en) * 2002-08-23 2007-07-11 中国原子能科学研究院 Perturbation well-to-well tracing test method
CN1699998B (en) * 2005-06-06 2011-08-31 里群 Constant quantity substance tracer agent for oilfield monitoring and application in oil deposit dynamic monitoring
CN100489266C (en) * 2005-07-07 2009-05-20 中国石油大学(北京) Method for detecting fluid-channeling channel of oil field
GB2438216A (en) * 2006-05-17 2007-11-21 Schlumberger Holdings Methods and systems for evaluation of hydrocarbon reservoirs and associated fluids using biological tags and real-time polymerase chain reaction
GB2438216B (en) * 2006-05-17 2008-11-19 Schlumberger Holdings Methods and systems for evaluation of hydrocarbon reservoirs and associated fluids using biological tags and real-time polymerase chain reactions
CN101548264B (en) * 2006-10-31 2015-05-13 埃克森美孚上游研究公司 Modeling and management of reservoir systems with material balance groups
CN102353750A (en) * 2011-06-03 2012-02-15 中国石油天然气股份有限公司 Crude oil low-temperature oxidation experimental device for light oil reservoir air-injection oil extraction
CN102353750B (en) * 2011-06-03 2014-05-14 中国石油天然气股份有限公司 Crude oil low-temperature oxidation experimental device for light oil reservoir air-injection oil extraction
CN102392636A (en) * 2011-11-03 2012-03-28 中国石油大学(华东) Underground fluid channel parameter description method for water drive development of sandstone reservoir
CN102392636B (en) * 2011-11-03 2015-07-08 山东石大油田技术服务股份有限公司 Underground fluid channel parameter description method for water drive development of sandstone reservoir
CN104903724A (en) * 2012-11-15 2015-09-09 麦克罗-奇瑟斯公司 Tracer particles, and methods for making same
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CN105019894B (en) * 2015-07-29 2017-11-14 长江大学 A kind of stratified reservoir inter well connectivity method for establishing model and system
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CN106707365A (en) * 2016-12-06 2017-05-24 中国石油大学(华东) Method for monitoring geothermal reservoir temperature and fracture distribution and device thereof
CN106680147A (en) * 2017-01-10 2017-05-17 新疆大学 Application of halohydrin as water injection chemical tracer in oil field
CN106996293A (en) * 2017-05-23 2017-08-01 濮阳市易发化工有限公司 Oil field trace matter detection monitoring technology
CN107989588A (en) * 2017-11-10 2018-05-04 东方宝麟科技发展(北京)有限公司 Utilize each section of oil gas water section method and system of environment-friendly type tracer test horizontal well
CN107989600A (en) * 2017-12-13 2018-05-04 北京捷贝通石油技术有限公司 A kind of water base trace chemistry tracer and the method for measuring water injection well inter well connectivity
CN107989600B (en) * 2017-12-13 2023-09-12 捷贝通石油技术集团股份有限公司 Water-based trace chemical tracer and method for measuring connectivity between water injection wells
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CN109138989A (en) * 2018-08-07 2019-01-04 大庆东方兴盛石油科技服务有限公司 Tracer monitoring technique method
CN110566184A (en) * 2019-09-17 2019-12-13 广西师范大学 Use of14Method for tracing oil field well by C nuclide
CN111257967A (en) * 2020-01-13 2020-06-09 苏州星烁纳米科技有限公司 Oil field tracer and oil field tracing method
CN117808986A (en) * 2024-01-08 2024-04-02 成都北方石油勘探开发技术有限公司 Water-drive reservoir dominant channel identification and quantification method

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