CN104514558A - Trace element detection method among wells - Google Patents

Trace element detection method among wells Download PDF

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Publication number
CN104514558A
CN104514558A CN201310470380.0A CN201310470380A CN104514558A CN 104514558 A CN104514558 A CN 104514558A CN 201310470380 A CN201310470380 A CN 201310470380A CN 104514558 A CN104514558 A CN 104514558A
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Prior art keywords
well
trace element
tracer
determination agent
oil
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CN201310470380.0A
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Chinese (zh)
Inventor
张庆珍
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Tianjin Dagang Oilfield Shengda Technology Co Ltd
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Tianjin Dagang Oilfield Shengda Technology Co Ltd
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Priority to CN201310470380.0A priority Critical patent/CN104514558A/en
Publication of CN104514558A publication Critical patent/CN104514558A/en
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    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B49/00Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells
    • E21B49/08Obtaining fluid samples or testing fluids, in boreholes or wells
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B47/00Survey of boreholes or wells
    • E21B47/10Locating fluid leaks, intrusions or movements
    • E21B47/11Locating fluid leaks, intrusions or movements using tracers; using radioactivity
    • EFIXED CONSTRUCTIONS
    • E21EARTH OR ROCK DRILLING; MINING
    • E21BEARTH OR ROCK DRILLING; OBTAINING OIL, GAS, WATER, SOLUBLE OR MELTABLE MATERIALS OR A SLURRY OF MINERALS FROM WELLS
    • E21B49/00Testing the nature of borehole walls; Formation testing; Methods or apparatus for obtaining samples of soil or well fluids, specially adapted to earth drilling or wells

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  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Geology (AREA)
  • Mining & Mineral Resources (AREA)
  • Physics & Mathematics (AREA)
  • Environmental & Geological Engineering (AREA)
  • Fluid Mechanics (AREA)
  • General Life Sciences & Earth Sciences (AREA)
  • Geochemistry & Mineralogy (AREA)
  • Geophysics (AREA)
  • Geophysics And Detection Of Objects (AREA)

Abstract

The invention belongs to the technical field of tracing tests, and particularly relates to a trace element detection method among wells. The trace element detection method among the wells includes following steps: screening trace element tracer, calculating the use amount of the trace element tracer, injecting the trace element tracer into a water injection well after the use amount of the trace element tracer is figured out, sampling and detecting the trace element tracer, performing fitting on a trace element tracer production curve, figuring out stratum parameters, performing dynamic and static analysis on an oil well of a monitored well area, using a half analytic method to analyze, process and explain tracing monitoring information, and quantitatively or qualitatively acquiring static and dynamic information among oil reservoir wells, among layers of each oil reservoir well, in each layer of each oil reservoir well and around the oil well of the monitored well area; performing geologic modeling, obtaining a characteristic parameter variation rule, performing numerical simulation calibration and perfection, evaluating measure development effects, and designing measure technological parameters. The trace element detection method among the wells is simple and convenient to operate, low in cost and wide in application prospect.

Description

A kind of micro-inter-well test method
[technical field]
The invention belongs to Tracer Test Technology field, particularly relate to a kind of micro-inter-well test method.
[background technology]
Along with oil reservoir development is to meticulous water filling, meticulous steam injection future development, production test also changes to meticulous zonal testing direction gradually, and the means of reservoir monitoring are also more and more important.Inter-well tracer test method describes to have the important means of reservoir heterogeneity and mobility between closing well, can determine that well group is connective, the feature such as high permeability formation, fault properties and remaining oil saturation evaluation between oil-water well by this technology.Inter-well tracer test test is injected in water injection well by tracer, monitors the output situation of tracer around in producing well, if there is tracer to occur in producing well, then proves that water injection well is communicated with producing well, and be the main direction of propulsion injecting water.Utilize the break through of tracer, can determine that each well injects the tempo of penetration of fluid, the number of connectivity layer is relevant to the peak value of tracer output, by software the Fitting Calculation, can the connecting degree of quantitative description water injection well and producing well and reservoir in the plane with the anisotropic in longitudinal direction.The tracer selected can follow the trail of injection fluid effectively, monitoring tracer in well and oil reservoir in dynamic, enroll data exactly, obtained a result by computational analysis, thus reach the object of inter-well test.
Interwell tracer comprises chemical tracer, radioactive tracer, stable isotope tracer, Uranium determination agent.1, chemical tracer mainly comprises: the 1) inorganic salts of Yi Rong: as SCN-, CL-, Br-, I-, NO3-etc., and this kind of tracer is few in surface of stratum absorption, and consumption is little, and the photometer measuring method that is easily split detects.2) fluorescent dye class: as anionic dyes such as famille rose, alizarin red agents, but this kind of dyestuff is large in surface of stratum adsorbance, and some compositions in stratum also can interference analysis, so the time of staying just can not use more than 5 days in the earth formation.3) halogenated hydrocarbons and small molecule alcohol: as fluoro trichloromethane, trichloro-ethylene, dibromopropane etc., they are few in surface of stratum adsorbance, and easily for gas chromatography detects, but impact is had on the aft-loaded airfoil of crude oil.In recent years, along with polymer flooding, Weak Gels drive the expansion of range of application, stratum water quality changed, and brought many difficulties to the detection of chemical tracer and result, and even part tracer can't detect, and does not reach expected effect.2, radioactive tracer mainly contains tritium for compound, as HTO, hydrogen tritide, tritiate heptane etc., although this kind of tracer has few, the easy to detect and detection resolution advantages of higher of consumption, but because they have radioactivity, unfavorable to personnel, Environmental security, application is very restricted.3, stable isotope tracer has without pyrolytic conversion, "dead" harm, consumption is few, execute-in-place is convenient, certainty of measurement high, but the variety protection of stable isotope tracer is few, still need to be activated by the atomic reactor of indoor after some sampling, its radioactive activity is measured by neutron activation method, indoor detection can only be carried out by International Atomic Energy Agency to operate, its analytical test means are numerous and diverse, somewhat expensive, and application is restricted.4, Uranium determination agent is forth generation inter-well test tracer, compared with first three plants tracer, it is the main development direction of current inter-well test tracer, it have "dead", pollution-free, security and stability is good, consumption is few, low price, cost are lower and analysis precision advantages of higher, receive the favor of field operations personnel.
Trace element inter-well tracer test technology is the result that inter-well tracer test technology further develops, it be utilize do not have in stratum and contained fluid thereof or content is atomic, sedimentary characteristic is comparatively concentrated trace element as tracer, draw subsurface reservoir information by monitoring sampled well.It achieve the transformation from qualitative to quantitative, and effectively can react distribution situation and the characteristics of motion of underground fluid, relevant formation parameter can be obtained simultaneously, thus evaluate reservoir situation quantitatively.The analysis precision of micro substance is high, and general chemical analysis can only reach 10-6 level, and micro substance analysis can reach 10-12 level.But the operating procedure of existing micro-inter-well test method is more loaded down with trivial details, cost is more, manpower and materials cost is high.
[summary of the invention]
In order to solve the problems of the technologies described above, the object of the present invention is to provide a kind of micro-inter-well test method, operating procedure is fairly simple, cost is less, manpower and materials cost is low, comprises the steps:
(1) Uranium determination agent is screened: the oil well water sample and Injection Well water sample of monitoring wellblock are sampled, ICP-MS instrument is utilized to analyze institute's sample thief, carry out Uranium determination agent compatibility and adsorption test simultaneously, select that background concn in stratum is low, stratum absorption less, safety non-toxic, the Uranium determination agent good with the fluid compatibility of institute's spike;
(2) consumption of Uranium determination agent is calculated: according to the injection rate of the Uranium determination agent filtered out in formula A=μM of DLV calculation procedure (1), wherein V=∏ R2 Ф hS, μ-assurance coefficient, MDL-minimal detectable concentration, V-stratum maximum dilution volume, the average well spacing of R-, h-oil reservoir average thickness, Ф-oil reservoir average pore, the average water saturation of S-oil reservoir;
(3) water injection well is injected in the Uranium determination agent calculating handy amount in step (2): implant operation selects general implant operation, multi-section multi-layer to inject (pulling water nozzle) operation or multi-section multi-layer injects (lower leaf tubing string) operation one wherein;
(4) Uranium determination agent sampling and detection: after injecting the end of job, according to sampling designing requirement, sample time is relatively fixing, carries out sampling detect Uranium determination agent output concentration to the oil well of monitoring wellblock, drafting Uranium determination agent production curve;
(5) utilize the Uranium determination agent production curve obtained in step (4) to carry out matching, calculate formation parameter;
(6) static and dynamic analysis is carried out to the oil well of monitoring wellblock, utilize semi-analytic method to analyze tracer monitoring information, process and explain, quantitatively or be qualitatively familiar with static state, multidate information between oil reservoir well, in interlayer, layer and around the oil well of monitoring wellblock;
(7) carry out Geologic modeling according to the information obtained in step (6), obtain characteristic parameter Changing Pattern, carry out numerical simulation correction and perfect, evaluation measures development effectiveness, design measure technological parameter.
Beneficial effect of the present invention is: operating procedure of the present invention is fairly simple, cost is less, manpower and materials cost is low, easy to implement; The present invention, according to the feature in monitoring oil field, filters out the Uranium determination agent being suitable for field use, is convenient to efficiently carrying out of follow-up work; The method makes field operations personnel recognize oil reservoir inside, provides the data for information about of oil reservoir remaining oil saturation and the regularity of distribution thereof in oilfield development process, for oil field Efficient Development and long term stable production provide strong technical support and guarantee.The invention provides a kind of easy and simple to handle, cost is few, the micro-inter-well test method that has a extensive future.
[detailed description of the invention]
Below in conjunction with embodiment, the invention will be further described.
Embodiment
A kind of micro-inter-well test method, comprises the steps:
(1) Uranium determination agent is screened: the oil well water sample and Injection Well water sample of monitoring wellblock are sampled, ICP-MS instrument is utilized to analyze institute's sample thief, carry out Uranium determination agent compatibility and adsorption test simultaneously, select that background concn in stratum is low, stratum absorption less, safety non-toxic, the Uranium determination agent good with the fluid compatibility of institute's spike;
(2) consumption of Uranium determination agent is calculated: according to the injection rate of the Uranium determination agent filtered out in formula A=μM of DLV calculation procedure (1), wherein V=∏ R2 Ф hS, μ-assurance coefficient, MDL-minimal detectable concentration, V-stratum maximum dilution volume, the average well spacing of R-, h-oil reservoir average thickness, Ф-oil reservoir average pore, the average water saturation of S-oil reservoir;
(3) water injection well is injected in the Uranium determination agent calculating handy amount in step (2): implant operation selects general implant operation, multi-section multi-layer to inject (pulling water nozzle) operation or multi-section multi-layer injects (lower leaf tubing string) operation one wherein;
(4) Uranium determination agent sampling and detection: after injecting the end of job, according to sampling designing requirement, sample time is relatively fixing, carries out sampling detect Uranium determination agent output concentration to the oil well of monitoring wellblock, drafting Uranium determination agent production curve;
(5) utilize the Uranium determination agent production curve obtained in step (4) to carry out matching, calculate formation parameter;
(6) static and dynamic analysis is carried out to the oil well of monitoring wellblock, utilize semi-analytic method to analyze tracer monitoring information, process and explain, quantitatively or be qualitatively familiar with static state, multidate information between oil reservoir well, in interlayer, layer and around the oil well of monitoring wellblock;
(7) carry out Geologic modeling according to the information obtained in step (6), obtain characteristic parameter Changing Pattern, carry out numerical simulation correction and perfect, evaluation measures development effectiveness, design measure technological parameter.
Operating procedure of the present invention is fairly simple, cost is less, manpower and materials cost is low, easy to implement; The present invention, according to the feature in monitoring oil field, filters out the Uranium determination agent being suitable for field use, is convenient to efficiently carrying out of follow-up work; The method makes field operations personnel recognize, and oil reservoir is inner, the data for information about of oil reservoir remaining oil saturation and the regularity of distribution thereof in oilfield development process is provided, for oil field Efficient Development and long term stable production provide strong technical support and guarantee, have a extensive future.
Above one embodiment of the present of invention have been described in detail, but described content being only preferred embodiment of the present invention, can not being considered to for limiting practical range of the present invention.All equalizations done according to the present patent application scope change and improve, and all should still belong within patent covering scope of the present invention.

Claims (1)

1. a micro-inter-well test method, is characterized in that, comprise the steps:
(1) Uranium determination agent is screened: the oil well water sample and Injection Well water sample of monitoring wellblock are sampled, ICP-MS instrument is utilized to analyze institute's sample thief, carry out Uranium determination agent compatibility and adsorption test simultaneously, select that background concn in stratum is low, stratum absorption less, safety non-toxic, the Uranium determination agent good with the fluid compatibility of institute's spike;
(2) consumption of Uranium determination agent is calculated: according to the injection rate of the Uranium determination agent filtered out in formula A=μM of DLV calculation procedure (1), wherein V=∏ R2 Ф hS, μ-assurance coefficient, MDL-minimal detectable concentration, V-stratum maximum dilution volume, the average well spacing of R-, h-oil reservoir average thickness, Ф-oil reservoir average pore, the average water saturation of S-oil reservoir;
(3) water injection well is injected in the Uranium determination agent calculating handy amount in step (2): implant operation selects general implant operation, multi-section multi-layer to inject (pulling water nozzle) operation or multi-section multi-layer injects (lower leaf tubing string) operation one wherein;
(4) Uranium determination agent sampling and detection: after injecting the end of job, according to sampling designing requirement, sample time is relatively fixing, carries out sampling detect Uranium determination agent output concentration to the oil well of monitoring wellblock, drafting Uranium determination agent production curve;
(5) utilize the Uranium determination agent production curve obtained in step (4) to carry out matching, calculate formation parameter;
(6) static and dynamic analysis is carried out to the oil well of monitoring wellblock, utilize semi-analytic method to analyze tracer monitoring information, process and explain, quantitatively or be qualitatively familiar with static state, multidate information between oil reservoir well, in interlayer, layer and around the oil well of monitoring wellblock;
(7) carry out Geologic modeling according to the information obtained in step (6), obtain characteristic parameter Changing Pattern, carry out numerical simulation correction and perfect, evaluation measures development effectiveness, design measure technological parameter.
CN201310470380.0A 2013-10-07 2013-10-07 Trace element detection method among wells Pending CN104514558A (en)

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Cited By (14)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105672994A (en) * 2015-12-29 2016-06-15 核工业北京化工冶金研究院 Tracing method in in-situ uranium mining
CN106368679A (en) * 2016-08-31 2017-02-01 潍坊华诺生物科技有限公司 Microelement tracer agent used for offshore oilfield and use method thereof
CN106707365A (en) * 2016-12-06 2017-05-24 中国石油大学(华东) Method for monitoring geothermal reservoir temperature and fracture distribution and device thereof
CN107989600A (en) * 2017-12-13 2018-05-04 北京捷贝通石油技术有限公司 A kind of water base trace chemistry tracer and the method for measuring water injection well inter well connectivity
CN108005641A (en) * 2017-12-13 2018-05-08 北京捷贝通石油技术有限公司 A kind of oil base trace chemistry tracer and the method for evaluating each section of oil-producing contribution rate of horizontal well
CN109138989A (en) * 2018-08-07 2019-01-04 大庆东方兴盛石油科技服务有限公司 Tracer monitoring technique method
CN109577966A (en) * 2018-11-29 2019-04-05 四川富利斯达石油科技发展有限公司 Using the method for tracer monitoring individual well residual oil saturation
CN110566184A (en) * 2019-09-17 2019-12-13 广西师范大学 Use of14Method for tracing oil field well by C nuclide
CN110644975A (en) * 2019-09-27 2020-01-03 西安石油大学 Fracture-cavity type oil reservoir tracer curve quantitative interpretation method
CN110778313A (en) * 2019-10-15 2020-02-11 天津大港油田圣达科技有限公司 Rare earth element tracer interwell monitoring technology
CN111980639A (en) * 2020-09-23 2020-11-24 青岛大地新能源技术研究院 Oil layer tracing monitoring method based on cooperation of perforation and tracer and tracing perforating bullet
CN112943226A (en) * 2019-12-11 2021-06-11 天津大港油田圣达科技有限公司 Method for evaluating staged fracturing effect and oil-water contribution of each stage of horizontal well by oil-water tracer
CN113027429A (en) * 2019-12-09 2021-06-25 天津大港油田圣达科技有限公司 Tracing technology for monitoring horizontal well fracturing fluid flowback rate
CN113756790A (en) * 2021-09-07 2021-12-07 西安石油大学 Novel multi-section productivity evaluation method for oil and gas well

Cited By (18)

* Cited by examiner, † Cited by third party
Publication number Priority date Publication date Assignee Title
CN105672994A (en) * 2015-12-29 2016-06-15 核工业北京化工冶金研究院 Tracing method in in-situ uranium mining
CN106368679A (en) * 2016-08-31 2017-02-01 潍坊华诺生物科技有限公司 Microelement tracer agent used for offshore oilfield and use method thereof
CN106707365A (en) * 2016-12-06 2017-05-24 中国石油大学(华东) Method for monitoring geothermal reservoir temperature and fracture distribution and device thereof
CN108005641B (en) * 2017-12-13 2023-08-15 捷贝通石油技术集团股份有限公司 Oil-based trace chemical tracer and method for evaluating contribution rate of oil production of each section of horizontal well
CN107989600A (en) * 2017-12-13 2018-05-04 北京捷贝通石油技术有限公司 A kind of water base trace chemistry tracer and the method for measuring water injection well inter well connectivity
CN108005641A (en) * 2017-12-13 2018-05-08 北京捷贝通石油技术有限公司 A kind of oil base trace chemistry tracer and the method for evaluating each section of oil-producing contribution rate of horizontal well
CN107989600B (en) * 2017-12-13 2023-09-12 捷贝通石油技术集团股份有限公司 Water-based trace chemical tracer and method for measuring connectivity between water injection wells
CN109138989A (en) * 2018-08-07 2019-01-04 大庆东方兴盛石油科技服务有限公司 Tracer monitoring technique method
CN109577966A (en) * 2018-11-29 2019-04-05 四川富利斯达石油科技发展有限公司 Using the method for tracer monitoring individual well residual oil saturation
CN110566184A (en) * 2019-09-17 2019-12-13 广西师范大学 Use of14Method for tracing oil field well by C nuclide
CN110644975A (en) * 2019-09-27 2020-01-03 西安石油大学 Fracture-cavity type oil reservoir tracer curve quantitative interpretation method
CN110644975B (en) * 2019-09-27 2022-10-21 西安石油大学 Fracture-cavity type oil reservoir tracer curve quantitative interpretation method
CN110778313A (en) * 2019-10-15 2020-02-11 天津大港油田圣达科技有限公司 Rare earth element tracer interwell monitoring technology
CN113027429A (en) * 2019-12-09 2021-06-25 天津大港油田圣达科技有限公司 Tracing technology for monitoring horizontal well fracturing fluid flowback rate
CN112943226A (en) * 2019-12-11 2021-06-11 天津大港油田圣达科技有限公司 Method for evaluating staged fracturing effect and oil-water contribution of each stage of horizontal well by oil-water tracer
CN111980639A (en) * 2020-09-23 2020-11-24 青岛大地新能源技术研究院 Oil layer tracing monitoring method based on cooperation of perforation and tracer and tracing perforating bullet
CN113756790A (en) * 2021-09-07 2021-12-07 西安石油大学 Novel multi-section productivity evaluation method for oil and gas well
CN113756790B (en) * 2021-09-07 2023-10-03 西安石油大学 Multi-section productivity evaluation method for oil and gas well

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Application publication date: 20150415