CN1357643A - Lengthened magnesium alloy - Google Patents
Lengthened magnesium alloy Download PDFInfo
- Publication number
- CN1357643A CN1357643A CN01135446A CN01135446A CN1357643A CN 1357643 A CN1357643 A CN 1357643A CN 01135446 A CN01135446 A CN 01135446A CN 01135446 A CN01135446 A CN 01135446A CN 1357643 A CN1357643 A CN 1357643A
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- China
- Prior art keywords
- weight
- magnesium alloy
- extrusion
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- comparative example
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C23/00—Alloys based on magnesium
- C22C23/04—Alloys based on magnesium with zinc or cadmium as the next major constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C23/00—Alloys based on magnesium
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22C—ALLOYS
- C22C23/00—Alloys based on magnesium
- C22C23/02—Alloys based on magnesium with aluminium as the next major constituent
-
- C—CHEMISTRY; METALLURGY
- C22—METALLURGY; FERROUS OR NON-FERROUS ALLOYS; TREATMENT OF ALLOYS OR NON-FERROUS METALS
- C22F—CHANGING THE PHYSICAL STRUCTURE OF NON-FERROUS METALS AND NON-FERROUS ALLOYS
- C22F1/00—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working
- C22F1/06—Changing the physical structure of non-ferrous metals or alloys by heat treatment or by hot or cold working of magnesium or alloys based thereon
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- Chemical & Material Sciences (AREA)
- Engineering & Computer Science (AREA)
- Materials Engineering (AREA)
- Mechanical Engineering (AREA)
- Metallurgy (AREA)
- Organic Chemistry (AREA)
- Physics & Mathematics (AREA)
- Thermal Sciences (AREA)
- Crystallography & Structural Chemistry (AREA)
- Extrusion Of Metal (AREA)
- Forging (AREA)
Abstract
Provided is a wrought magnesium alloy of which forming rate by extrusion can be increased compared with the conventional one, and which has sufficient mechanical properties and corrosion resistance as those of a structural material. The wrought magnesium alloy contains, by weight, 0.1% to 1.0% aluminum, 0.1% to 2.0% zinc, 0.1% to 1.0% manganese, < =0.04% copper, < =0.05% silicon, < =0.005% iron and < =0.005% nickel.
Description
Technical field
The relevant lengthened magnesium alloy of the present invention, as be used to push, alloy material that processing is elongated in calendering etc., and process the building structural materials that makes by elongating with this alloy material.
Background technology
Here so-called " elongating processing " is meant that required shape is processed in process extruding, pressurization, forgings etc. such as forged material to extrusion molding material, rolled material, press molding material.
The lengthened magnesium alloy that is used for building structural materials was used as the M1 of the JIS of aluminum-zinc alloy in the past always.This M1 contains the aluminium of 3.0 weight % and the zinc of 1.0 weight %.
But the above-mentioned lengthened magnesium alloy of using till today is when extrusion processing, if forming speed is very fast, then molding can produce fracture, so just can not be shaped.And oxidation takes place in the molding surface, and surface properties is worsened, and can not be shaped.
On the other hand, the forming speed during the magnesium alloy rolling processing wishes to improve.
The content of invention
According to above-mentioned situation, the objective of the invention is to provide lengthened magnesium alloy, it can with than in the past faster forming speed carry out extrusion processing, as structured material, it has sufficient mechanical property and corrosion resistance nature.
For reaching this purpose, feature of the present invention is, below the above 1.0 weight % of aluminium content 0.1 weight %, below the above 2.0 weight % of zinc content 0.1 weight %, below the above 1.0 weight % of manganese content 0.1 weight %, below the copper content 0.04 weight %, below the silicone content 0.05 weight %, below the iron level 0.005 weight %, below the nickel content 0.005 weight %.
During with lengthened magnesium alloy blank extrusion molding of the present invention, both made extrusion speed be about original 10 times, extrusion molded article does not rupture yet, and can be not on fire and can not be shaped owing to surface oxidation.Therefore, can with than originally faster extrusion speed come extrusion molding to make the Structure of magnesium alloy material.
With the physical properties of the extrusion molding goods of lengthened magnesium alloy of the present invention, as tensile strength, proof stress, elongation, corrosion resistance nature is all than in the past goods excellence, as the mechanical property of light material especially than in the past goods excellence.
Aluminium content is because during the discontented 0.1 weight % of aluminium content below the 1.0 weight % more than 0.1 weight %, can not obtain sufficient mechanical property as structured material, and when surpassing 1.0 weight %, is difficult to again obtain than extrusion speed faster in the past.
Zinc content is because during the discontented 0.1 weight % of zinc content below the 2.0 weight % more than 0.1 weight %, and corrosion-resistant, and when surpassing 2.0 weight % is difficult to again obtain than extrusion speed faster in the past.
Manganese content is because the erosion resistance the best in this scope below 1.0 weight % more than the 0.1 weight %.Manganese content is lower than 0.1 weight %, and the obvious variation of erosion resistance, and when surpassing 1.0 weight % is difficult to again obtain than extrusion speed faster in the past.
Lengthened magnesium alloy of the present invention preferably contains below the above 0.8 weight % of aluminium 0.2 weight %, below the above 1.0 weight % of zinc 0.2 weight %, manganese 0.3 weight %, below the above 0.04 weight % of copper 0.02 weight %, below the above 0.03 weight % of silicon 0.02 weight %, iron 0.004 weight %, below the nickel 0.001 weight %, all the other are magnesium.
According to experimental result, in these content ranges, not only extrusion speed is than in the past fast about 10 times, and mechanical propertiess such as the tensile strength of extrusion molded article are also than in the past excellence.
Copper, silicon.Iron, nickel all are the unavoidable impurities elements.
Also can add calcium to improve flame retardant resistance.The calcium addition is advisable with 0.3～1.0 weight %.
The content of rare earth elements such as yttrium, neodymium, cerium all when 100ppm is following, can improve high-temperature mechanical property by weight.
Description of drawings
Fig. 1 is the sectional view of shape material behind the extrusion molding.
Fig. 2 is section form shape material the sectional view extrusion molding after different with Fig. 1.
The concrete mode of implementing
(embodiment)
Table 1 is depicted as the composition of embodiment 1 to 3, and embodiment 1～3 is the blank of lengthened magnesium alloy, wherein, quantitatively adds aluminium, zinc, manganese, silicon, iron, copper, nickel, and Bal. (rest part) is a magnesium.The unit of table 1 is weight % again.
(comparative example)
The blank of comparative example 1～3 is formed also as shown in table 1.
Table 1
| ????Al | ????Zn | ????Mn | ????Si | ????Fe | ????Cu | ????Ni | ????Mg | |
| Embodiment 1 | ????0.5 | ????0.25 | ????0.3 | ????0.03 | ????0.004 | ????0.03 | ????0.001 | ????Bal. |
| Embodiment 2 | ????0.8 | ????0.2 | ????0.3 | ????0.02 | ????0.004 | ????0.02 | ????0.001 | ????Bal. |
| Embodiment 3 | ????0.2 | ????1.0 | ????0.3 | ????0.03 | ????0.004 | ????0.04 | ????0.001 | ????Bal. |
| Comparative example 1 | ????3.0 | ????1.0 | ????0.3 | ????0.02 | ????0.005 | ????0.04 | ????0.002 | ????Bal. |
| Comparative example 2 | ????0.8 | ????2.5 | ????0.3 | ????0.03 | ????0.004 | ????0.03 | ????0.001 | ????Bal. |
| Comparative example 3 | ????0.8 | ????0.5 | ????1.2 | ????0.03 | ????0.004 | ????0.03 | ????0.001 | ????Bal. |
In embodiment 1～3 and the comparative example 1～3, extrusion molding is the shape material of shape extremely as shown in Figure 1.Experiment is carried out under different extrusion speeds, 5 meters/minute, 10,15...70 rice/minutes.Its result is shown in following table 2.Again, the size of shape material shown in Figure 1 is that W is 50mm, and S is 15mm, and t (thickness) is 1.2mm.The extruding condition of each embodiment and comparative example is, blank temperature is 400 ℃, and nip load is 3～500 ten thousand newton.
Table 2
| Extrusion speed (rice/minute) | ||||||
| ??5 | ??10 | ??15 | ??30 | ??50 | ??70 | |
| Embodiment 1 | ??○ | ??○ | ??○ | ??○ | ??○ | ??○ |
| Embodiment 2 | ??○ | ??○ | ??○ | ??○ | ??○ | ??× |
| Embodiment 3 | ??○ | ??○ | ??○ | ??○ | ??○ | ??× |
| Comparative example 1 | ??○ | ??× | ??× | ??- | ??- | ??- |
| Comparative example 2 | ??○ | ??× | ??× | ??- | ??- | ??- |
| Comparative example 3 | ??× | ??× | ??- | ??- | ??- | |
Symbol in the table 2, [zero] is can extrusion molding, [*] for rupture, the surface properties deterioration, [-] can not extrusion molding for to rupture.
Again, in embodiment 1 and the comparative example 1, extrusion molding is the shape material of shape extremely as shown in Figure 2, and its result is as shown in table 3.Again, the size of shape material shown in Figure 2 is that W is 40mm, and S is 20mm, and V is 15mm, and t (thickness) is 2.0mm.Other conditions are identical with the extrusion molding shown in the table 2.Identical in the table 3 in the meaning of symbol and the table 2.
Table 3
| Extrusion speed (rice/minute) | ||||||
| ??1 | ??2 | ??5 | ??10 | ??15 | ??20 | |
| Embodiment 1 | ??○ | ??○ | ??○ | ??○ | ??○ | ??○ |
| Comparative example 1 | ??○ | ??○ | ??× | ??- | ??- | ??- |
Again, in embodiment 1～3 and the comparative example 1～3, the shape material of extrusion molding under each extrusion speed in table 2 has been carried out the mensuration of tensile strength, its result as shown in the following Table 4.Being determined on the universal testing machine of tensile strength carried out.The unit of table 4 is MPa (million pascal).Again, in the comparative example 1～3 of table 4, when extrusion speed reaches 10 meters/timesharing, as table 2[*] shown in, surface properties worsens, but for for the purpose of the comparison, has still measured tensile strength.
Table 4
| Extrusion speed (rice/minute) | ||||
| ???5 | ???10 | ????30 | ????70 | |
| Embodiment 1 | ??240 | ??240 | ????240 | ????240 |
| Embodiment 2 | ??250 | ??250 | ????250 | ????240 |
| Embodiment 3 | ??240 | ??240 | ????240 | ????230 |
| Comparative example 1 | ??280 | ??200 | Can not push | Can not push |
| Comparative example 2 | ??260 | ??180 | Can not push | Can not push |
| Comparative example 3 | ??270 | ??200 | Can not push | Can not push |
As shown in Table 2, in embodiment 1～3, extrusion speed (finished product speed) is respectively 5～50 meters/timesharing, can both extrusion molding, and the deterioration of surface properties does not take place in the outward appearance range estimation.Especially among the embodiment 1, under 70 meters/minute speed, surface properties does not worsen yet, can also extrusion molding.With respect to this, in the comparative example 1～3, speed is 10 meters/timesharing, though can the extrusion molding surface properties worsen, and under the speed more than 15 meters/minute, fracture takes place can not extrusion molding.That is, the extrusion speed of embodiment 1～3 comparative example 1～3 more than 10 times the time still can extrusion molding.
In the shape material extruding of as shown in Figure 2 section form, shown in the embodiment 1 of table 3, be that 20 meters/timesharing can also extrusion molding, but in comparative example 1, be that 5 meters/timesharing is just ruptured, can not extrusion molding.By the result of table 2 and table 3 as can be known, the section form difference of extruding shape material, extrusion speed is also different, but when same section form, the extrusion speed of embodiments of the invention is faster more than 10 times than comparative example.
The tensile strength of each embodiment and comparative example gained shape material as shown in Table 4, in the comparative example 1～3, extrusion speed one is fast, and tensile strength just obviously reduces, and the situation of present embodiment is, the similar energy the when tensile strength when extrusion speed is fast is slow with extrusion speed is identical.Especially be 10 meters/timesharing at extrusion speed, any tensile strength good than comparative example 1～3 all of embodiment 1～3.General typical tensile strength of elongating with aluminium alloy A6063 (JIS) is 220MPa, and the tensile strength of present embodiment is better than this elongation aluminium alloy.
In embodiment 1～3, also measured 0.2% elasticity polarity stress and elongation.0.2% elasticity polarity stress is 110～130MPa, and elongation is 8～12%, and the corrosion decrement of carrying out with 5%NaCl salt solution after 24 hours the spray testing is 2mg/cm
2/ day, with this evaluation criteria as erosion resistance.These physical propertiess are elongated almost or omit with aluminium alloy 6063 (JIS) with general, can be used as the lightweight structural material use.
Among the embodiment 1～3, also respectively with the blank manufacturing extruding shape material that has further added 0.3～1.0 weight % calcium, can extrusion molding under the speed identical with the foregoing description 1～3, mechanical property is also identical simultaneously, compare with the above-mentioned shape material that does not add calcium, because surface oxidation and incidence on fire reduces to some extent is so improved flame retardant resistance.
Among the embodiment 1～3, also respectively with further having added the blank manufacturing extruding shape material of rare earth elements such as the yttrium below 100ppm, neodymium, cerium by weight, can extrusion molding under the speed identical with the foregoing description 1～3, and the mechanical property under the high temperature (200-300 ℃) is better than the foregoing description.
Lengthened magnesium alloy of the present invention is not limited to be used on the extrusion molding, also can be used for calendering, press molding, forging, and these fabricated products can obtain the effect same with the extrusion molding goods.
As mentioned above, utilize the present invention, can with than in the past faster extrusion speed magnesium alloy is carried out extrusion molding processing.And the surface properties that can not occur causing because of the fracture of extrusion molding goods or surface oxidation are on fire etc. worsens.
Claims (4)
1. elongate the magnesium alloy materials that is processed into building structural materials, wherein, contain the following aluminium of the above 1.0 weight % of 0.1 weight %, 0.1 the following zinc of the above 2.0 weight % of weight %, 0.1 the following manganese of the above 1.0 weight % of weight %, the copper that 0.04 weight % is following, the silicon that 0.05 weight % is following, 0.005 the iron that weight % is following, the nickel that 0.005 weight % is following.
2. the described magnesium alloy of claim 1 wherein, also contains the following calcium of the above 1.0 weight % of 0.3 weight %.
3. the described magnesium alloy of claim 1 wherein, also contains rare earth elements such as the yttrium below 100ppm, neodymium, cerium by weight.
4. building structural materials is characterized in that, is made through elongating processing by the described alloy material of claim 1.
Applications Claiming Priority (2)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| JP2000367217A JP2002173730A (en) | 2000-12-01 | 2000-12-01 | Wrought magnesium alloy |
| JP367217/00 | 2000-12-01 |
Publications (1)
| Publication Number | Publication Date |
|---|---|
| CN1357643A true CN1357643A (en) | 2002-07-10 |
Family
ID=18837681
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN01135446A Pending CN1357643A (en) | 2000-12-01 | 2001-09-28 | Lengthened magnesium alloy |
Country Status (8)
| Country | Link |
|---|---|
| US (1) | US20020102179A1 (en) |
| JP (1) | JP2002173730A (en) |
| KR (1) | KR20020043157A (en) |
| CN (1) | CN1357643A (en) |
| AU (1) | AU6877701A (en) |
| DE (1) | DE10148573A1 (en) |
| GB (1) | GB2369625A (en) |
| TW (1) | TW530094B (en) |
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100363145C (en) * | 2005-05-20 | 2008-01-23 | 东北轻合金有限责任公司 | Method for manufacturing extruded bar from magnesium alloy |
| CN101177745B (en) * | 2007-10-16 | 2010-04-21 | 中国科学院长春应用化学研究所 | Magnesium-silicon intermediate, high-magnesium aluminum alloy thereby and their preparation method |
| CN103388094A (en) * | 2013-07-22 | 2013-11-13 | 天津东义镁制品股份有限公司 | A magnesium alloy LED fluorescent lamp section material and a manufacturing method thereof |
| CN109266931A (en) * | 2018-08-23 | 2019-01-25 | 江苏理工学院 | A kind of high-performance magnesium-alloy and preparation method thereof |
| CN111235448A (en) * | 2020-01-19 | 2020-06-05 | 重庆大学 | Novel magnesium alloy for building template and preparation method thereof |
| CN114574742A (en) * | 2022-02-28 | 2022-06-03 | 吉林大学 | Corrosion-resistant weak-texture magnesium alloy for casting and rolling and preparation method thereof |
Families Citing this family (11)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| JP2004115862A (en) * | 2002-09-26 | 2004-04-15 | Toyo Kohan Co Ltd | Malleable magnesium sheet excellent in formability and its manufacturing method |
| US20050194072A1 (en) * | 2004-03-04 | 2005-09-08 | Luo Aihua A. | Magnesium wrought alloy having improved extrudability and formability |
| CN103060585B (en) * | 2012-12-14 | 2015-07-08 | 威瑞泰科技发展(宁波)有限公司 | Smelting method for Al-Mg-Mn-Cu-Ti aluminum alloy |
| WO2015127174A1 (en) | 2014-02-21 | 2015-08-27 | Terves, Inc. | Fluid activated disintegrating metal system |
| CN110004339B (en) | 2014-04-18 | 2021-11-26 | 特维斯股份有限公司 | Electrochemically active in situ formed particles for controlled rate dissolution tool |
| GB201413327D0 (en) | 2014-07-28 | 2014-09-10 | Magnesium Elektron Ltd | Corrodible downhole article |
| JP6552111B2 (en) * | 2016-03-11 | 2019-07-31 | 公益財団法人鉄道総合技術研究所 | Method for producing extruded shape of flame retardant magnesium alloy |
| JP7116394B2 (en) * | 2017-02-28 | 2022-08-10 | 国立研究開発法人物質・材料研究機構 | Magnesium alloy and method for producing magnesium alloy |
| US20200232070A1 (en) * | 2019-01-18 | 2020-07-23 | Divergent Technologies, Inc. | Aluminum alloy compositions |
| DE112020004656T5 (en) * | 2019-09-30 | 2022-06-15 | Ohio State Innovation Foundation | Magnesium alloys and methods of making and using them |
| DE102022206662A1 (en) | 2022-06-30 | 2024-01-04 | Volkswagen Aktiengesellschaft | High-strength, age-hardenable magnesium alloy comprising Al, Ca, Mn and Y |
Family Cites Families (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| BE466388A (en) * | ||||
| GB513627A (en) * | 1938-01-14 | 1939-10-18 | Ig Farbenindustrie Ag | Improvements in and relating to magnesium alloys |
| GB690783A (en) * | 1950-08-16 | 1953-04-29 | Dow Chemical Co | Improvements in making alloy extruded forms by powder metallurgy |
| GB746545A (en) * | 1953-03-18 | 1956-03-14 | Dow Chemical Co | Manufacture of magnesium alloy extrusions |
| GB960027A (en) * | 1962-04-27 | 1964-06-10 | Magnesium Elektron Ltd | Improvements in or relating to magnesium base alloys |
| GB974571A (en) * | 1962-06-05 | 1964-11-04 | Magnesium Elektron Ltd | Improvements in or relating to magnesium base alloys |
| US3146096A (en) * | 1962-11-23 | 1964-08-25 | Dow Chemical Co | Weldable high strength magnesium base alloy |
| WO1995012002A1 (en) * | 1993-10-25 | 1995-05-04 | Vladimir Georgievich Smelikov | High strength alloy |
-
2000
- 2000-12-01 JP JP2000367217A patent/JP2002173730A/en active Pending
-
2001
- 2001-09-04 TW TW090121873A patent/TW530094B/en active
- 2001-09-06 AU AU68777/01A patent/AU6877701A/en not_active Abandoned
- 2001-09-12 GB GB0122030A patent/GB2369625A/en not_active Withdrawn
- 2001-09-27 KR KR1020010060071A patent/KR20020043157A/en not_active Application Discontinuation
- 2001-09-28 US US09/964,602 patent/US20020102179A1/en not_active Abandoned
- 2001-09-28 CN CN01135446A patent/CN1357643A/en active Pending
- 2001-10-01 DE DE10148573A patent/DE10148573A1/en not_active Ceased
Cited By (8)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100363145C (en) * | 2005-05-20 | 2008-01-23 | 东北轻合金有限责任公司 | Method for manufacturing extruded bar from magnesium alloy |
| CN101177745B (en) * | 2007-10-16 | 2010-04-21 | 中国科学院长春应用化学研究所 | Magnesium-silicon intermediate, high-magnesium aluminum alloy thereby and their preparation method |
| CN103388094A (en) * | 2013-07-22 | 2013-11-13 | 天津东义镁制品股份有限公司 | A magnesium alloy LED fluorescent lamp section material and a manufacturing method thereof |
| CN109266931A (en) * | 2018-08-23 | 2019-01-25 | 江苏理工学院 | A kind of high-performance magnesium-alloy and preparation method thereof |
| CN111235448A (en) * | 2020-01-19 | 2020-06-05 | 重庆大学 | Novel magnesium alloy for building template and preparation method thereof |
| CN111235448B (en) * | 2020-01-19 | 2021-11-23 | 重庆大学 | Magnesium alloy for building template and preparation method thereof |
| CN114574742A (en) * | 2022-02-28 | 2022-06-03 | 吉林大学 | Corrosion-resistant weak-texture magnesium alloy for casting and rolling and preparation method thereof |
| CN114574742B (en) * | 2022-02-28 | 2022-11-01 | 吉林大学 | Corrosion-resistant weak texture magnesium alloy for casting and rolling and preparation method thereof |
Also Published As
| Publication number | Publication date |
|---|---|
| GB0122030D0 (en) | 2001-10-31 |
| TW530094B (en) | 2003-05-01 |
| JP2002173730A (en) | 2002-06-21 |
| KR20020043157A (en) | 2002-06-08 |
| DE10148573A1 (en) | 2002-06-13 |
| AU6877701A (en) | 2002-06-13 |
| US20020102179A1 (en) | 2002-08-01 |
| GB2369625A (en) | 2002-06-05 |
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