CN1333401A - Antibiosis and crease-resistant fabric production method - Google Patents
Antibiosis and crease-resistant fabric production method Download PDFInfo
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- CN1333401A CN1333401A CN 00117001 CN00117001A CN1333401A CN 1333401 A CN1333401 A CN 1333401A CN 00117001 CN00117001 CN 00117001 CN 00117001 A CN00117001 A CN 00117001A CN 1333401 A CN1333401 A CN 1333401A
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Abstract
The production method of anti-bacterial crease resistant fabric applicable to high-ratio cotton and chemical fibre blending is characterized by its anti-bacterial liquor formula which adopts halogenated aromatic compound and derivative and utilizes acetic acid to regulate pH value to 4-5 and its crease-resisting liquor formula containing modified dimethylol dihydroxy-ethylene urea, strong-acid weak-alkali salt, organic acid mixed catalyst and organic silicone softening agent. Its production process incldues the following steps: firstly, padding with anti-bacterial liquor, drying and baking, and then padding with crease-resisting liquor, drying and baking. Its anti-bacterial effect is durable, and possesses good permeability and adhesion to fabric, and can be biodegraded, and its crease-resisting agent has no yellowing in the course of high-temp. baking, and its crease-resisting effect is good.
Description
The present invention relates to production method antibiotic in the caused by spinning industrial production, crease resistant fabric, refer in particular at high proportion the production method of antibiotic, the crease resistant fabric of cotton and chemical fibre blending.
Cotton textiles or cotton at high proportion and chemical fiber blended fabrics air-moisture-permeable, soft, comfortable and easy to wear.But weak point is this kind fabric poor flexibility, creases easily, and is not well-pressed, is difficult for improving product specification; In addition, when wearing, this kind fabric can adsorb the hot humid medium that human body distributes, for bacterial reproduction provides good environment.Prolific bacterium and microorganism can corrode human body, cause allergic, infection and bad smell.Fabric or clothes with the washing of 60 ℃ of water temperatures after, look very cleaning, but bacterium and microorganism exist still, sanitation performance is poor.
In recent years, use polybasic carboxylic acid, as 1,2,3,4-BTCA (BTCA) is carried out formaldehyde-free crease-proofing finishing to COTTON FABRIC more, and wrinkle resistance is improved, but polybasic carboxylic acid costs an arm and a leg poor practicability.Have research to replace BTCA to make anti wrinkling agent with cheap citric acid (CA), and make catalyst with sodium hypophosphite (SHP), triethanolamine (TEA) is made additive, and COTTON FABRIC is made formaldehyde-free crease-proofing finishing, and certain wrinkle resistant effect is arranged.
There is following problem usually in the antiseptic that antibiotic finish is adopted: antibacterial antiplaque agent bacterium spectrum is wideless, and antibacterial effect is not lasting, and antiseptic is toxic, and skin is had spread effect etc.
The production method that the purpose of this invention is to provide a kind of comparatively perfect antibiotic crease resistant fabric.
That content of the present invention comprises is antibiotic, prescription and finishing technique two parts of wrinkle proofing liquid.
Antiseptic is selected halogenated aromatic compound and derivative for use, and the prescription of antibiotic finishing solution is:
Halogenated aromatic compound and derivative antibacterial agent 1%～2% (weight ratio);
Acetic acid is regulated pH to 4～5;
Water adds to 100%.
Anti-creasing agent is selected the hydroxymethyl-2 dihydroxy-ethylene urea of modification for use, is reactive environment-friendly type shrink-resistant agent, and the prescription of wrinkle proofing liquid is:
The modification hydroxymethyl-2 dihydroxy-ethylene urea 40%～60% (weight ratio) of 40% concentration;
Strong acid weak base salt and organic acid mixed catalyst 10%～15% (weight ratio);
20% concentration macromolecule organic silicon emulsion softener, 15%～30% (weight ratio);
Water adds to 100%.
Antibiotic, wrinkle proofing technology is:
Fabric pads antibiotic finishing solution → oven dry (90～100 ℃ of temperature) → bake (120～140 ℃ of temperature, time 1.5～2.5min) → pad wrinkle proofing liquid → oven dry (90～100 ℃ of temperature) → bake (150～165 ℃ of temperature, time 3～4min) → shrinkproof processing (common process) → check.
Advantage of the present invention is that used antiseptic has durable antibiotic property to textile fabric, and fabric is had good penetration and adhesiveness, skin is had no stimulation, and favorable biological degradability is arranged; Used crease proofing agent high temperature bakes down not yellowing, but free extremely low with releasable for maldehyde content, wrinkle resistant effect is good.
Below provide embodiment.
Embodiment 1.
It is the antiseptic of SANITIZED that the trade mark of Switzerland Clariant chemical industry Co., Ltd is selected in halogenated aromatic compound and derivative antibacterial agent, can anti-Staphylococcus aureus StaphyLococcus Aureus, Escherichia coli Escherichia Coli and trichomycin Trichophyton Meutagrophytes bacterial classifications such as (fungies).The antibiotic finish formula of liquid is:
Antiseptic SANITIZED90-04 1.5% (weight ratio);
Acetic acid is regulated pH to 4.5;
Water adds to 100%.
Embodiment 2.
The modification hydroxymethyl-2 dihydroxy-ethylene urea is selected the wrinkle resistant resin finishing agent of the Switzerland's vapour Bagong KNITTEX of department environment-friendly type; Selection of catalysts is decided according to resin activation grade size, and weak acid strong alkali salt is wherein selected magnesium chloride for use, and organic acid is selected citric acid for use, and the ratio that both mix is 5: 8 (weight ratio); Softener generally can be selected nonionic-weak cation type organic silicon emulsion for use, especially can adopt high molecular elastomer silicone more than 200,000.This elastomer is network structure, can increase wrinkle resistance in fabrics, has increased again with resilience, and fabric feeling is obviously sliding along soft.The wrinkle proofing formula of liquid is:
The KNITTEX FEL 40% (weight ratio) of 40% concentration;
Mixed catalyst: magnesium chloride/citric acid 5%/8% (weight ratio);
Silicone softening agent WF-343 20% (weight ratio);
Silicone softening agent 708-B 10% (weight ratio);
Water adds to 100%.
Embodiment 3.
The Anti-bacterial and Crease process using is padded antimicrobial fluid earlier, with reduction fabric face temperature, and suitably reduces the speed of a motor vehicle to reduce coefficient of friction, and the groove interlayer to reduce the working solution temperature, guarantees working solution stability with the cold water circulation, and concrete parameter is:
Pad antimicrobial fluid → oven dry (95 ℃ of temperature) → bake (130 ℃ of temperature, time 2min) → pad wrinkle resistant liquid → oven dry (95 ℃ of temperature) → the bake shrinkproof processing of (160 ℃ of temperature, time 3.5min) → common process → check.
After the selection and process choice to domestic and international all kinds of antiseptics, resin wrinkle proofing, catalyst and softener, to 55/45 (cotton/as to wash), 45 * 45,133 * 72 fabrics are produced in enormous quantities, and manufacture experimently into shirt, and effect is remarkable.After testing, antibacterial effect reaches ATCC6538 international standard, EMPA334 international standard; Wrinkle resistant effect is delayed bullet 263, washing shrinkage 1.2% * 0.4%, content of formaldehyde 6.9ppm.
Wrinkle resistant index contrast sees the following form before and after the arrangement.Method of testing standard broadwise tearing brute force behind the index arrangement prefinishing, N 8.4 6.5 GB/T3917.1 folding lines recover the angle, spend 189 263 GB/T3819 washing shrinkages, % warp-wise 1.6 1.2 GB/T8629 2AF broadwises 1 0.4 GB/T8629 2AF content of formaldehyde 6.9ppm GB/T2912 A
Claims (2)
1. the production method of antibiotic, crease resistant fabric is characterized in that described method adopts antibiotic, wrinkle proofing formula of liquid to be:
A. antibiotic finish formula of liquid:
Halogenated aromatic compound and derivative antibacterial agent 1%～2% (weight ratio);
Acetic acid is regulated pH to 4～5;
Water adds to 100%.
B. wrinkle proofing formula of liquid:
The modification hydroxymethyl-2 dihydroxy-ethylene urea 40%～60% (weight ratio) of 40% concentration;
Strong acid weak base salt and organic acid mixed catalyst 10%～15% (weight ratio);
20% concentration macromolecule organic silicon emulsion softener, 15%～30% (weight ratio);
Water adds to 100%.
2. production method as claimed in claim 1 is characterized in that antibiotic, wrinkle proofing technology that described method adopts are:
Fabric pad antibiotic finishing solution → oven dry (90～100 ℃ of temperature) → bake (120～140 ℃ of temperature. time 1.5～2.5min) → pad wrinkle proofing liquid → oven dry (90～100 ℃ of temperature) → bake (150～165 ℃ of temperature, time 3～4min) → shrinkproof processing (common process) → check.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00117001 CN1333401A (en) | 2000-07-06 | 2000-07-06 | Antibiosis and crease-resistant fabric production method |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN 00117001 CN1333401A (en) | 2000-07-06 | 2000-07-06 | Antibiosis and crease-resistant fabric production method |
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| CN1333401A true CN1333401A (en) | 2002-01-30 |
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| CN 00117001 Pending CN1333401A (en) | 2000-07-06 | 2000-07-06 | Antibiosis and crease-resistant fabric production method |
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Cited By (10)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101407996B (en) * | 2008-10-16 | 2011-08-17 | 鹤山北丰家用纺织品有限公司 | Method for processing full cotton crease-resistant fabric |
| CN102517893A (en) * | 2011-11-10 | 2012-06-27 | 广东省均安牛仔服装研究院 | Jeans garment shaping liquid as well as preparation method and application thereof in ultraviolet light photocatalytic shaping and finishing method |
| CN102605622A (en) * | 2012-03-22 | 2012-07-25 | 上海龙头（集团）股份有限公司 | After-finishing technology for reducing shrinkage rate of bamboo fiber fabric and bedding |
| CN102634983A (en) * | 2011-12-28 | 2012-08-15 | 广东省均安牛仔服装研究院 | Finishing liquor for antibacterial crumpling of jeans garment and preparation method of jeans garment |
| CN103046337A (en) * | 2012-12-14 | 2013-04-17 | 常熟常圣服饰有限公司 | Method for producing jeans wear |
| CN103061064A (en) * | 2012-12-14 | 2013-04-24 | 江苏黄果树服饰有限公司 | Method for producing jeans garments |
| CN103510383A (en) * | 2013-09-10 | 2014-01-15 | 上海工程技术大学 | Method for improving crease resistance and shrinkage resistance of Lyocell bamboo fiber |
| CN104452289A (en) * | 2014-12-23 | 2015-03-25 | 常熟市华博毛纺织有限公司 | Finishing process of shirt fabric |
| CN105297445A (en) * | 2015-12-07 | 2016-02-03 | 常熟市华谊织造有限公司 | After-finishing process of real silk fabric |
| CN112981961A (en) * | 2021-03-05 | 2021-06-18 | 鲁泰纺织股份有限公司 | Preparation method of light-energy self-disinfecting formaldehyde-free non-ironing fabric |
-
2000
- 2000-07-06 CN CN 00117001 patent/CN1333401A/en active Pending
Cited By (13)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN101407996B (en) * | 2008-10-16 | 2011-08-17 | 鹤山北丰家用纺织品有限公司 | Method for processing full cotton crease-resistant fabric |
| CN102517893A (en) * | 2011-11-10 | 2012-06-27 | 广东省均安牛仔服装研究院 | Jeans garment shaping liquid as well as preparation method and application thereof in ultraviolet light photocatalytic shaping and finishing method |
| CN102517893B (en) * | 2011-11-10 | 2016-01-20 | 广东省均安牛仔服装研究院 | Jeans style keeping liquid and preparation method thereof, and the purposes in ultraviolet light photocatalysis sizing method for sorting |
| CN102634983A (en) * | 2011-12-28 | 2012-08-15 | 广东省均安牛仔服装研究院 | Finishing liquor for antibacterial crumpling of jeans garment and preparation method of jeans garment |
| CN102634983B (en) * | 2011-12-28 | 2015-04-15 | 广东省均安牛仔服装研究院 | Finishing liquor for antibacterial crumpling of jeans garment and preparation method of jeans garment |
| CN102605622A (en) * | 2012-03-22 | 2012-07-25 | 上海龙头（集团）股份有限公司 | After-finishing technology for reducing shrinkage rate of bamboo fiber fabric and bedding |
| CN103046337A (en) * | 2012-12-14 | 2013-04-17 | 常熟常圣服饰有限公司 | Method for producing jeans wear |
| CN103061064A (en) * | 2012-12-14 | 2013-04-24 | 江苏黄果树服饰有限公司 | Method for producing jeans garments |
| CN103510383A (en) * | 2013-09-10 | 2014-01-15 | 上海工程技术大学 | Method for improving crease resistance and shrinkage resistance of Lyocell bamboo fiber |
| CN103510383B (en) * | 2013-09-10 | 2016-04-27 | 上海工程技术大学 | A kind of method improving Lyocell bamboo fiber anti-wrinkle shrink-proof performance |
| CN104452289A (en) * | 2014-12-23 | 2015-03-25 | 常熟市华博毛纺织有限公司 | Finishing process of shirt fabric |
| CN105297445A (en) * | 2015-12-07 | 2016-02-03 | 常熟市华谊织造有限公司 | After-finishing process of real silk fabric |
| CN112981961A (en) * | 2021-03-05 | 2021-06-18 | 鲁泰纺织股份有限公司 | Preparation method of light-energy self-disinfecting formaldehyde-free non-ironing fabric |
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