CN102517893A - Jeans garment shaping liquid as well as preparation method and application thereof in ultraviolet light photocatalytic shaping and finishing method - Google Patents
Jeans garment shaping liquid as well as preparation method and application thereof in ultraviolet light photocatalytic shaping and finishing method Download PDFInfo
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- CN102517893A CN102517893A CN2011103659604A CN201110365960A CN102517893A CN 102517893 A CN102517893 A CN 102517893A CN 2011103659604 A CN2011103659604 A CN 2011103659604A CN 201110365960 A CN201110365960 A CN 201110365960A CN 102517893 A CN102517893 A CN 102517893A
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- ultraviolet light
- keeping liquid
- style keeping
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- 239000007788 liquid Substances 0.000 title claims abstract description 176
- 230000001699 photocatalysis Effects 0.000 title claims abstract description 148
- 238000000034 method Methods 0.000 title claims abstract description 60
- 238000007493 shaping process Methods 0.000 title claims abstract description 14
- 238000002360 preparation method Methods 0.000 title abstract description 40
- 238000005406 washing Methods 0.000 claims abstract description 100
- 238000001035 drying Methods 0.000 claims abstract description 71
- 230000005855 radiation Effects 0.000 claims abstract description 67
- 239000003795 chemical substances by application Substances 0.000 claims abstract description 43
- 239000003351 stiffener Substances 0.000 claims abstract description 37
- 230000000149 penetrating effect Effects 0.000 claims abstract description 36
- 229910052742 iron Inorganic materials 0.000 claims abstract description 34
- 238000007146 photocatalysis Methods 0.000 claims description 144
- 238000012545 processing Methods 0.000 claims description 130
- XEEYBQQBJWHFJM-UHFFFAOYSA-N iron Substances [Fe] XEEYBQQBJWHFJM-UHFFFAOYSA-N 0.000 claims description 101
- 239000007921 spray Substances 0.000 claims description 101
- 230000007613 environmental effect Effects 0.000 claims description 39
- 238000013461 design Methods 0.000 claims description 37
- SOQBVABWOPYFQZ-UHFFFAOYSA-N oxygen(2-);titanium(4+) Chemical compound [O-2].[O-2].[Ti+4] SOQBVABWOPYFQZ-UHFFFAOYSA-N 0.000 claims description 36
- 229920002125 Sokalan® Polymers 0.000 claims description 21
- 239000004584 polyacrylic acid Substances 0.000 claims description 21
- 239000003814 drug Substances 0.000 claims description 6
- 238000005303 weighing Methods 0.000 claims description 6
- ABLZXFCXXLZCGV-UHFFFAOYSA-N Phosphorous acid Chemical compound OP(O)=O ABLZXFCXXLZCGV-UHFFFAOYSA-N 0.000 claims description 3
- 239000000203 mixture Substances 0.000 claims description 3
- 238000003756 stirring Methods 0.000 claims description 3
- 150000001732 carboxylic acid derivatives Chemical class 0.000 claims 2
- 230000000694 effects Effects 0.000 abstract description 38
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 abstract description 35
- WSFSSNUMVMOOMR-UHFFFAOYSA-N Formaldehyde Chemical compound O=C WSFSSNUMVMOOMR-UHFFFAOYSA-N 0.000 abstract description 9
- GWEVSGVZZGPLCZ-UHFFFAOYSA-N Titan oxide Chemical compound O=[Ti]=O GWEVSGVZZGPLCZ-UHFFFAOYSA-N 0.000 abstract description 7
- 238000004519 manufacturing process Methods 0.000 abstract description 6
- 230000003197 catalytic effect Effects 0.000 abstract description 2
- KWSLGOVYXMQPPX-UHFFFAOYSA-N 5-[3-(trifluoromethyl)phenyl]-2h-tetrazole Chemical compound FC(F)(F)C1=CC=CC(C2=NNN=N2)=C1 KWSLGOVYXMQPPX-UHFFFAOYSA-N 0.000 abstract 1
- 239000002253 acid Substances 0.000 abstract 1
- 229910001379 sodium hypophosphite Inorganic materials 0.000 abstract 1
- 238000005507 spraying Methods 0.000 abstract 1
- 239000004408 titanium dioxide Substances 0.000 abstract 1
- 239000003054 catalyst Substances 0.000 description 68
- 239000001488 sodium phosphate Substances 0.000 description 33
- 229910000162 sodium phosphate Inorganic materials 0.000 description 33
- RYFMWSXOAZQYPI-UHFFFAOYSA-K trisodium phosphate Chemical compound [Na+].[Na+].[Na+].[O-]P([O-])([O-])=O RYFMWSXOAZQYPI-UHFFFAOYSA-K 0.000 description 33
- 230000008859 change Effects 0.000 description 32
- 238000005516 engineering process Methods 0.000 description 11
- KRKNYBCHXYNGOX-UHFFFAOYSA-N citric acid Chemical compound OC(=O)CC(O)(C(O)=O)CC(O)=O KRKNYBCHXYNGOX-UHFFFAOYSA-N 0.000 description 9
- 150000001735 carboxylic acids Chemical class 0.000 description 7
- 230000008569 process Effects 0.000 description 7
- 238000001723 curing Methods 0.000 description 6
- 239000000835 fiber Substances 0.000 description 6
- 239000011347 resin Substances 0.000 description 6
- 229920005989 resin Polymers 0.000 description 6
- KDYFGRWQOYBRFD-UHFFFAOYSA-N succinic acid Chemical compound OC(=O)CCC(O)=O KDYFGRWQOYBRFD-UHFFFAOYSA-N 0.000 description 6
- 239000004744 fabric Substances 0.000 description 5
- OGIDPMRJRNCKJF-UHFFFAOYSA-N titanium oxide Inorganic materials [Ti]=O OGIDPMRJRNCKJF-UHFFFAOYSA-N 0.000 description 5
- 238000006555 catalytic reaction Methods 0.000 description 3
- 229960005137 succinic acid Drugs 0.000 description 3
- 239000004753 textile Substances 0.000 description 3
- 229920000742 Cotton Polymers 0.000 description 2
- OFOBLEOULBTSOW-UHFFFAOYSA-N Propanedioic acid Natural products OC(=O)CC(O)=O OFOBLEOULBTSOW-UHFFFAOYSA-N 0.000 description 2
- 239000012752 auxiliary agent Substances 0.000 description 2
- 230000000740 bleeding effect Effects 0.000 description 2
- 229910052799 carbon Inorganic materials 0.000 description 2
- 239000000084 colloidal system Substances 0.000 description 2
- 238000004134 energy conservation Methods 0.000 description 2
- 230000032050 esterification Effects 0.000 description 2
- 238000005886 esterification reaction Methods 0.000 description 2
- 230000008595 infiltration Effects 0.000 description 2
- 238000001764 infiltration Methods 0.000 description 2
- VZCYOOQTPOCHFL-UPHRSURJSA-N maleic acid Chemical compound OC(=O)\C=C/C(O)=O VZCYOOQTPOCHFL-UPHRSURJSA-N 0.000 description 2
- 239000011976 maleic acid Substances 0.000 description 2
- 230000002688 persistence Effects 0.000 description 2
- 238000006116 polymerization reaction Methods 0.000 description 2
- VZCYOOQTPOCHFL-UHFFFAOYSA-N trans-butenedioic acid Natural products OC(=O)C=CC(O)=O VZCYOOQTPOCHFL-UHFFFAOYSA-N 0.000 description 2
- YNJLPAALXOVAPF-UHFFFAOYSA-N OC(O)C(=CO)O Chemical group OC(O)C(=CO)O YNJLPAALXOVAPF-UHFFFAOYSA-N 0.000 description 1
- 238000003848 UV Light-Curing Methods 0.000 description 1
- XSQUKJJJFZCRTK-UHFFFAOYSA-N Urea Chemical compound NC(N)=O XSQUKJJJFZCRTK-UHFFFAOYSA-N 0.000 description 1
- 239000003513 alkali Substances 0.000 description 1
- 230000000680 avirulence Effects 0.000 description 1
- 239000002585 base Substances 0.000 description 1
- 230000008901 benefit Effects 0.000 description 1
- -1 brightener Substances 0.000 description 1
- 239000004202 carbamide Substances 0.000 description 1
- 125000003178 carboxy group Chemical group [H]OC(*)=O 0.000 description 1
- 238000010382 chemical cross-linking Methods 0.000 description 1
- 238000006243 chemical reaction Methods 0.000 description 1
- 239000002131 composite material Substances 0.000 description 1
- 238000004132 cross linking Methods 0.000 description 1
- 230000007423 decrease Effects 0.000 description 1
- 230000007812 deficiency Effects 0.000 description 1
- 238000011161 development Methods 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 238000007599 discharging Methods 0.000 description 1
- 238000005265 energy consumption Methods 0.000 description 1
- 239000003344 environmental pollutant Substances 0.000 description 1
- 125000002887 hydroxy group Chemical group [H]O* 0.000 description 1
- 230000010534 mechanism of action Effects 0.000 description 1
- 230000004048 modification Effects 0.000 description 1
- 238000012986 modification Methods 0.000 description 1
- 238000000465 moulding Methods 0.000 description 1
- 230000003287 optical effect Effects 0.000 description 1
- 239000003504 photosensitizing agent Substances 0.000 description 1
- 231100000719 pollutant Toxicity 0.000 description 1
- 239000003223 protective agent Substances 0.000 description 1
- 230000035484 reaction time Effects 0.000 description 1
- 238000011084 recovery Methods 0.000 description 1
- 238000009281 ultraviolet germicidal irradiation Methods 0.000 description 1
- 239000003643 water by type Substances 0.000 description 1
- 210000002268 wool Anatomy 0.000 description 1
Landscapes
- Treatment Of Fiber Materials (AREA)
- Chemical Or Physical Treatment Of Fibers (AREA)
Abstract
The invention provides a jeans garment shaping liquid as well as a preparation method and an application thereof in an ultraviolet light photocatalytic shaping and finishing method and relates to a jeans garment shaping liquid. The jeans garment shaping liquid comprises the following components in percentage by weight: 5.0-15.0 percent of polycarboxylic acid, 3.0-9.0 percent of sodium hypophosphite, 0.1-2.0 percent of Fe<3+>doped nanometer titanium dioxide, 1.0-5.0 percent of penetrating agents, 2.0-5.0 percent of formaldehyde-free environmentally-friendly stiffening agents, 3.0-5.0 percent of smooth brighteners and 59.0-85.9 percent of water. The invention also relates to the jeans garment ultraviolet light photocatalytic shaping and finishing method by adopting the shaping liquid, which comprises the following steps of: carrying out plasma radiation treatment on a part of a jeans garment required to be shaped, spraying the shaping liquid onto the treated part of the jeans garment, pre-drying on a drying tunnel-type drying oven and crinkling the treated part of the jeans garment; then carrying out photocatalytic shaping on the treated parts; and finally washing and drying. The method is high in catalytic efficiency, is environmental-friendly and energy-saving and is high in production efficiency. The finished jeans garment is durable, is good in shaping effect and good in handfeel and gloss, is environmental-friendly and generates no formaldehyde emission.
Description
Technical field
The present invention relates to a kind of jeans style keeping liquid and preparation method thereof, and in the purposes of ultraviolet light photocatalysis typing method for sorting, it belongs to textiles auxiliary agent and after-finishing of textile products technical field.
Background technology
Having invented article one twill cowboy trousers from 19th-century Levi Strauus begins; Jeans are firmly got liking of consumers in general with its characteristic such as rough, simple, graceful naturally, comfortable, wear-resisting; Become people's a kind of main consumer goods, its demand is considerable.Arrangement is the critical process of giving the jeans individual style behind the cowboy, is determining the height of a jean added value, also is the effective means that improves cowboy's added value of product.Jeans ready-made clothes typing (claiming in the industry that cowboy crumples) is one of important step of putting in order behind the cowboy.At present; Aspect the jeans ready-made clothes crumpled, traditional cowboy crumpled technology and is: and preparation style keeping liquid---dipping (normal temperature, 10-15min) or spray (60-70 ℃ of---dehydration---baker prebake; 15-25min)---crumple — — oven and bake (145-155 ℃; 20-40min), wherein style keeping liquid adopts dihydroxymethyl dihydroxy ethylene base urea (2D resin) and modification 2D resin mostly, and auxiliary agent such as composite bleeding agent, brightener, stiffening agent is as the jeans style keeping liquid.Present denim garment crumples technology and exists energy consumption high, length consuming time, and there are problems such as formaldehyde release in the jeans after the typing arrangement.Along with people's is to the attention further of ecological environmental protection, and exploitation is taken avirulence with lining, and nuisanceless pollution becomes the trend of cowboy's industry development in the production process for the environment-friendly type jeans on basis.Therefore developing the energy-conservation jeans shaping technology of low-carbon environment-friendly can have a difficult problem to be solved for the jeans technical staff.
To the problem that natural fabric textiles typing arrangement back fabric exists formaldehyde to discharge, study at present more be with polybasic carboxylic acid as solidifying and setting liquid, replace traditional 2D resin.The polybasic carboxylic acid style keeping liquid is through the hydroxyl generation esterification on carboxyl and the fiber, forms chemical crosslinking, thereby plays the purpose of typing, and this finishing technique needs high temperature, and the typing effect is slightly poorer than the setting agent of 2D resinae.The required reaction time of UV-curing technology is short, and it is much lower compared with traditional hot setting to consume energy.In the prior art, the existing esterification that adopts ultraviolet light to replace high temperature is used for the anti-crease finishing of common cotton, rarely has as cowboy to crumple the ultraviolet light polymerization style keeping liquid.A.Nazari etc. report among the 371:10-16 (2009) that at periodical Applied Catalysis A:General adopting BTCA and citric acid is setting agent; Inferior sodium phosphate is a catalyst; Nano titanium oxide is the arrangement that photochemical catalyst is used for byssus, has contrasted ultraviolet light polymerization, these three kinds of curing modes of hot setting and ultraviolet light-hot setting; Discovery is under ultraviolet light-hot setting mode, and the creasy recovery angle of the byssus of treated mistake is maximum.Cheng-Chi Chen etc. are at periodical J Sol-Gel Sci Techn, and report among the 40:31-38 (2006) under ultraviolet light conditions, adopts nano titanium oxide catalysis butanedioic acid to the COTTON FABRIC arrangement of finalizing the design.Cheng-Chi Chen etc. report in periodical Applied Catalysis A:General 293:171-179 (2005); With BTCA, maleic acid, butanedioic acid and citric acid under the effect of catalyst nano titanium dioxide; Through UV-irradiation and electron radiation, the typing effect of the fabric after finding to handle is: BTCA＞maleic acid＞citric acid＞butanedioic acid.Majid Montazer etc. are at periodical Colloids and Surfaces A:Physicochem.Eng.Aspects; Report among the 375:1-11 (2011); Nano titanium oxide is carried out ultra sonic bath with BTCA and is applied in the wool fabric as a kind of colloid; The result shows that the woolen hygroscopicity of handling through nano titanium oxide increases, and alkali solubility decreases.Chinese patent publication number CN 101768868A; Open day on July 7th, 2010; The patent of invention name is called " a kind of resin style keeping liquid and adopt the cowboy of this resin style keeping liquid to crumple process ", and it is the denim garment style keeping liquid that this application case discloses with water polyacrylic acid 50-150g, photosensitizer 0.1-1.0g, fiber protective agent 5-25g, bleeding agent 1-5g, adopts the ultraviolet light ultraviolet curing process to realize that jeans crumple arrangement; Its mechanism of action is to utilize photocatalysis to cause the crosslinking curing of water polyacrylic acid; The effect of typing is played on the covered fiber surface, and its weak point is that the jeans after the typing arrangement exist feel poor; Molding resin might come off in follow-up water-washing process, the persistence of influence typing.
The clothes although exploitation environment-friendly type cowboy finalizes the design earn widespread respect, and the optical catalysed environment protection type jeans style keeping liquid and the typing method for sorting thereof that can be used for reality at present are actually rare; Up to the present, also do not find to adopt with doped F e
3+The type nano titanium oxide is a photochemical catalyst, and the polybasic carboxylic acid of environment friendly aldehyde-free etc. prepare the finalize the design report of clothes aspect of environment-friendly type cowboy for jeans style keeping liquid and typing method for sorting thereof.
Summary of the invention
The objective of the invention is to overcome the deficiency of above-mentioned prior art existence, and a kind of jeans style keeping liquid is provided; This jeans style keeping liquid possesses environmental protection, the jeans good hand touch after the typing arrangement, and the typing back is not easy to come off in water-washing process, and the preferable advantage of persistence of typing.
Another object of the present invention is to provide a kind of preparation jeans style keeping liquid method; This preparation method is simple and easy, quick.
A purpose more of the present invention is to provide the purposes of a kind of above-mentioned jeans style keeping liquid in ultraviolet light photocatalysis typing method for sorting; Adopt environment-friendly type jeans style keeping liquid, utilization ultraviolet light photocatalysis curing process replaces traditional high temperature curing process and prepares environmental protection, environment-friendly type cowboy energy-conservation, efficient, stable performance the clothes of finalizing the design.
The technical solution of jeans style keeping liquid of the present invention is following.
A kind of jeans style keeping liquid is characterized in that, it comprise following each component and the quality percentage composition following:
Above-mentioned jeans style keeping liquid can also have following technical measures.
Described polybasic carboxylic acid can be a kind of in BTCA or the polyacrylic acid.
The present invention prepares the method for above-mentioned jeans style keeping liquid, it is characterized in that, it comprises the steps:
At first, take by weighing medicine by each component and the mass percent thereof of above-mentioned jeans style keeping liquid, subsequent use;
Then, from the above-mentioned medicine that takes by weighing, take out polybasic carboxylic acid and ortho phosphorous acid and receive, and add Fe
3+Doped nano titanium dioxide, and then add entry, stir;
At last, add penetrating agent JFC, formaldehydeless environmental protection stiffening agent and level and smooth brightener, mixed liquor mixed and dispersed under high-speed stirred or ultrasonic wave condition is even, prepare said jeans style keeping liquid.
The purposes of a kind of jeans style keeping liquid in jeans ultraviolet light photocatalysis typing method for sorting is characterized in that, may further comprise the steps:
Steps A, at first, the position that jeans need be finalized the design are carried out plasma radiation and are handled, and its irradiation voltage is 10kV-15kV, and exposure time is between the 30s-180s;
Step B, employing high-pressure spray gun spray regime are sprayed style keeping liquid to the jeans position after processing of step A, and liquid application rate is 1-3kg/m
2
Step C, the jeans after will passing through step B and handling are in the prebake of drying tunnel formula baker, and the preliminary drying temperature is 60-80 ℃, and the preliminary drying time is between the 3-5min;
Step D, the position of jeans after step C handles crumpled processing, crumple to handle and adopt iron to crumple or cylinder crumples;
Step e, employing tunnel type uviol lamp photocatalysis equipment carry out the photocatalysis typing to the position of jeans after step D handles to be handled, and plant capacity is between 1kW-5kW, and the jean feeding speed is 10-30m/min, and shaping time is 10min-25min;
Step F, with the washing of jeans after step e is handled, oven dry.
Beneficial effect of the present invention is following:
(1) jeans style keeping liquid of the present invention; Adopt polybasic carboxylic acid to replace traditional 2D resinae style keeping liquid, this style keeping liquid does not contain formaldehyde, has solved the problem that jeans formaldehyde discharges; And polybasic carboxylic acid with fiber on hydroxyl generation esterification; Solved being prone to after the arrangement of general ultraviolet light style keeping liquid and come off, the problem of durable-modelling property difference is good through jeans typing effect and durable-modelling property after this style keeping liquid arrangement.Adopt Fe in addition
3+Doped nano titanium dioxide than single nano titanium oxide photocatalyst, has the catalytic efficiency height as photochemical catalyst, the characteristics that the catalysis time is short.
(2) jeans ultraviolet light photocatalysis typing method for sorting of the present invention; Adopt the ultraviolet light photocatalysis technology generations for high temperature curing process, reduced the damage of the jeans fiber that high temperature length consuming time brought, and shaping time higher temperatures technology is short; Low in the pollution of the environment, energy consumes low; Shorten the time that cowboy crumples technology on the whole, improved operating efficiency, reduced this technology cost.
(3) have again; In jeans ultraviolet light photocatalysis typing method for sorting; Using plasma irradiation carries out preliminary treatment to jeans, has increased the jeans fibers and active site setting agent, helps the chemical reaction of fiber and setting agent; Improve catalytic efficiency, strengthened the typing effect of jeans.
(4) in addition, fixed point high-pressure spray gun of the present invention sprays style keeping liquid technology, helps infiltration and the infiltration of style keeping liquid to jean; Shortened the time of last setting agent; This technology is only sprayed style keeping liquid to the jean position of needs typing, has reduced the use amount of jeans style keeping liquids greatly, and local typing does not influence the whole feel of denim; Practice thrift production cost, reduced the operation of the follow-up wash waters of jeans.
(5) the present invention adopts annular tunnel type uviol lamp photocatalysis equipment, has realized the semi-automation of jeans typing arrangement.
(6) jeans style keeping liquid of the present invention and ultraviolet light photocatalysis thereof typing method for sorting; Compare with traditional cowboy's setting process, significantly reduced the discharging of pollutant, improved working environment; Improved production efficiency; Practice thrift production cost, realized jeans environmental protection low-carbon energy-saving green production, improved the added value of jeans.
Description of drawings
Fig. 1 is jeans ultraviolet light photocatalysis typing finishing technique flow chart.
The specific embodiment
Below in conjunction with specific embodiment the present invention is done and to describe in further detail.
A kind of jeans style keeping liquid, it comprise following each component and the quality percentage composition following:
Wherein, the above-mentioned polybasic carboxylic acid of mentioning can be a kind of in BTCA or the polyacrylic acid.
The above-mentioned jeans style keeping liquid of a kind of preparation method is characterized in that it comprises the steps:
At first, take by weighing medicine by each component and the mass percent thereof of above-mentioned jeans style keeping liquid, subsequent use;
Then, from the above-mentioned medicine that takes by weighing, take out polybasic carboxylic acid and ortho phosphorous acid and receive, and add Fe
3+Doped nano titanium dioxide, and then add entry, stir;
At last, add penetrating agent JFC, formaldehydeless environmental protection stiffening agent and level and smooth brightener, mixed liquor mixed and dispersed under high-speed stirred or ultrasonic wave condition is even, prepare said jeans style keeping liquid.
A kind of jeans ultraviolet light photocatalysis typing method for sorting, that is: the purposes of above-mentioned jeans style keeping liquid in this method for sorting, it may further comprise the steps:
Steps A, at first, the position that jeans need be finalized the design are carried out plasma radiation and are handled, and its irradiation voltage is 10kV-15kV, and exposure time is between the 30s-180s;
Step B, employing high-pressure spray gun spray regime are sprayed style keeping liquid to the jeans position after processing of step A, and liquid application rate is 1-3kg/m
2
Step C, the jeans after will passing through step B and handling are in the prebake of drying tunnel formula baker, and the preliminary drying temperature is 60-80 ℃, and the preliminary drying time is between the 3-5min;
Step D, the position of jeans after step C handles crumpled processing, crumple to handle and adopt iron to crumple or cylinder crumples;
Step e, employing tunnel type uviol lamp photocatalysis equipment carry out the photocatalysis typing to the position of jeans after step D handles to be handled, and plant capacity is between 1kW-5kW, and the jean feeding speed is 10-30m/min, and shaping time is 10min-25min;
Step F, with the washing of jeans after step e is handled, oven dry.
Below illustrate:
Embodiment 1
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 5.0%, catalyst inferior sodium phosphate 3.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.1%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 85.9%.Jeans require position irradiation 30s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 60 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 2
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.1%, penetrating agent JFC 3.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 79.9%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 1kg/m
2Drying tunnel formula baker prebake temperature is 60 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 3
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 10.0%, catalyst inferior sodium phosphate 6.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.1%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 77.9%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 20min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 4
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 15.0%, catalyst inferior sodium phosphate 9.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 2.0%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y045.0%, level and smooth brightener KW-3015.0%, water 59.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 80 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 5
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.5%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 81.5%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 6
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 10.0%, catalyst inferior sodium phosphate 6.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 73.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 60 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 7
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 2.0%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent LT-Y045.0%, level and smooth brightener KW-3015.0%, water 74.0%.Jeans require position irradiation 30s under plasma device of typing, and radiation voltage is 15kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 80 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 5min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 8
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of style keeping liquid is: BTCA 10.0%, catalyst inferior sodium phosphate 6.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 2.0%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y045.0%, level and smooth brightener KW-3015.0%, water 67.0%.Jeans require position irradiation 180s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 80 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 5min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 9
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent LT-Y044.0%, level and smooth brightener KW-3014.0%, water 77.0%.Jeans require position irradiation 90s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 20min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 10
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y043.0%, level and smooth brightener KW-3013.0%, water 80.0%.Jeans require position irradiation 120s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 1kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 15min, the jean feeding speed is 25m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 11
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent YT-0712.0%, level and smooth brightener KW-3012.0%, water 81.0%.Jeans require position irradiation 150s under plasma device of typing, and radiation voltage is 13kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 15min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 12
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent YT-0715.0%, level and smooth brightener KW-3012.0%, water 79.0%.Jeans require position irradiation 180s under plasma device of typing, and radiation voltage is 12kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 13
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2%, formaldehydeless environmental protection stiffening agent LT-Y042%, level and smooth brightener KW-3012%, water 81.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 13kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 20m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 14
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.2%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y043.0%, level and smooth brightener KW-3012.0%, water 77.8%.Jeans require position irradiation 30s under plasma device of typing, and radiation voltage is 15kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 60 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 3kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 20min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 15
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 2.0%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3011.0%, water 81.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 80 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 10min, the jean feeding speed is 20m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 16
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: BTCA 7.5%, catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2%, formaldehydeless environmental protection stiffening agent LT-Y042%, level and smooth brightener KW-3012%, water 81.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 13kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2.5kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 15min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 17
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 5.0%, and catalyst inferior sodium phosphate 3.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.1%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 85.9%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 18
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1000) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.1%, penetrating agent JFC 3.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 79.9%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 1kg/m
2Drying tunnel formula baker prebake temperature is 60 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 19
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 10.0%, and catalyst inferior sodium phosphate 6.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.1%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 77.9%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 20min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 20
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 15.0%, and catalyst inferior sodium phosphate 9.0%, photochemical catalyst Fe
3+Doped nano titanium dioxide 2.0%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y045.0%, level and smooth brightener KW-3015.0%, water 59.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 21
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.5%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 81.5%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 22
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1000) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3013.0%, water 77.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 60 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 23
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.1%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent LT-Y045.0%, level and smooth brightener KW-3015.0%, water 75.9%.Jeans require position irradiation 30s under plasma device of typing, and radiation voltage is 15kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 80 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 5min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 24
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 2.0%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y045.0%, level and smooth brightener KW-3015.0%, water 71.0%.Jeans require position irradiation 180s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 80 ℃, and the time is 3min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 5min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 25
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent LT-Y044.0%, level and smooth brightener KW-3014.0%, water 77.0%.Jeans require position irradiation 90s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 20min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 26
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y043.0%, level and smooth brightener KW-3013.0%, water 80.0%.Jeans require position irradiation 120s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 1kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 15min, the jean feeding speed is 25m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 27
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3012.0%, water 81.0%.Jeans require position irradiation 150s under plasma device of typing, and radiation voltage is 13kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 15min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 28
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 1.0%, formaldehydeless environmental protection stiffening agent LT-Y045.0%, level and smooth brightener KW-3012.0%, water 79.0%.Jeans require position irradiation 180s under plasma device of typing, and radiation voltage is 12kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 5kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 29
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2%, formaldehydeless environmental protection stiffening agent LT-Y042%, level and smooth brightener KW-3012%, water 81.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 13kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 3kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 25min, the jean feeding speed is 20m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 30
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 0.2%, penetrating agent JFC 5.0%, formaldehydeless environmental protection stiffening agent LT-Y043.0%, level and smooth brightener KW-3012.0%, water 77.8%.Jeans require position irradiation 30s under plasma device of typing, and radiation voltage is 15kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 60 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 3kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 20min, the jean feeding speed is 30m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 31
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 2.0%, penetrating agent JFC 2.0%, formaldehydeless environmental protection stiffening agent LT-Y042.0%, level and smooth brightener KW-3011.0%, water 81.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 10kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2kg/m
2Drying tunnel formula baker prebake temperature is 80 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 10min, the jean feeding speed is 20m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Embodiment 32
Jeans ultraviolet light photocatalysis typing finishing technique is: preparation jeans style keeping liquid → jeans plasma radiation processings → high-pressure spray gun is injected on the position of jeans requirement typing → drying tunnel formula baker prebake → jeans crumple processings → ultraviolet light photocatalysis finalize the design processing → washing, dry.
Wherein the mass percent of jeans style keeping liquid is: and polyacrylic acid (molecular weight is: 1800) 7.5%, and catalyst inferior sodium phosphate 4.5%, photochemical catalyst Fe
3+Doped nano titanium dioxide 1.0%, penetrating agent JFC 2%, formaldehydeless environmental protection stiffening agent LT-Y042%, level and smooth brightener KW-3012%, water 81.0%.Jeans require position irradiation 60s under plasma device of typing, and radiation voltage is 13kV, and high-pressure spray gun sprays the style keeping liquid that disposes on jeans liquid application rate is 2.5kg/m
2Drying tunnel formula baker prebake temperature is 70 ℃, and the time is 5min, crumples handle to adopt iron to crumple or cylinder crumples.Through 1kW tunnel type uviol lamp photocatalysis equipment ultraviolet light photocatalysis typing processing time 15min, the jean feeding speed is 10m/min.Washing at last, oven dry.Typing arrangement back jeans washing 20 times, typing effect no change.
Claims (4)
1. a jeans style keeping liquid is characterized in that, it comprise following each component and the quality percentage composition following:
2. according to the said jeans style keeping liquid of claim 1, it is characterized in that said polybasic carboxylic acid is BTCA or polyacrylic acid.
3. a method for preparing above-mentioned jeans style keeping liquid is characterized in that it comprises the steps:
At first, take by weighing medicine by each component and the mass percent thereof of above-mentioned jeans style keeping liquid, subsequent use;
Then, from the above-mentioned medicine that takes by weighing, take out polybasic carboxylic acid and ortho phosphorous acid and receive, and add Fe
3+Doped nano titanium dioxide, and then add entry, stir;
At last, add penetrating agent JFC, formaldehydeless environmental protection stiffening agent and level and smooth brightener, mixed liquor mixed and dispersed under high-speed stirred or ultrasonic wave condition is even, prepare said jeans style keeping liquid.
4. the purposes of a jeans style keeping liquid in jeans ultraviolet light photocatalysis typing method for sorting is characterized in that, may further comprise the steps:
Steps A, at first, the position that jeans need be finalized the design are carried out plasma radiation and are handled, and its irradiation voltage is 10kV-15kV, and exposure time is between the 30s-180s;
Step B, employing high-pressure spray gun spray regime are sprayed style keeping liquid to the jeans position after processing of step A, and liquid application rate is 1-3kg/m
2
Step C, the jeans after will passing through step B and handling are in the prebake of drying tunnel formula baker, and the preliminary drying temperature is 60-80 ℃, and the preliminary drying time is between the 3-5min;
Step D, the position of jeans after step C handles crumpled processing, crumple to handle and adopt iron to crumple or cylinder crumples;
Step e, employing tunnel type uviol lamp photocatalysis equipment carry out the photocatalysis typing to the position of jeans after step D handles to be handled, and plant capacity is between 1kW-5kW, and the jean feeding speed is 10-30m/min, and shaping time is 10min-25min;
Step F, with the washing of jeans after step e is handled, oven dry.
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| CN201110365960.4A CN102517893B (en) | 2011-11-10 | 2011-11-10 | Jeans style keeping liquid and preparation method thereof, and the purposes in ultraviolet light photocatalysis sizing method for sorting |
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| CN102828376A (en) * | 2012-09-20 | 2012-12-19 | 广东省均安牛仔服装研究院 | Ultraviolet-light photo-curing shaping equipment for crumpling and shaping jeans and crumpling, shaping and finishing method with equipment |
| CN105385800A (en) * | 2015-12-28 | 2016-03-09 | 嘉兴学院 | Setting and finishing process for indumentum on fur |
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| US6500876B2 (en) * | 2000-03-31 | 2002-12-31 | Bayer Aktiengesellschaft | Coating composition containing UV-curable urethane (meth)acrylates containing isocyanate groups and urethane (meth)acrylates containing hydroxyl groups |
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| Publication number | Priority date | Publication date | Assignee | Title |
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| CN102828376A (en) * | 2012-09-20 | 2012-12-19 | 广东省均安牛仔服装研究院 | Ultraviolet-light photo-curing shaping equipment for crumpling and shaping jeans and crumpling, shaping and finishing method with equipment |
| CN105385800A (en) * | 2015-12-28 | 2016-03-09 | 嘉兴学院 | Setting and finishing process for indumentum on fur |
| CN107841579A (en) * | 2015-12-28 | 2018-03-27 | 嘉兴学院 | The sizing finishing technique of fleece on fur |
| CN107841579B (en) * | 2015-12-28 | 2020-08-14 | 嘉兴学院 | Shaping and finishing process of quilt on fur |
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| Publication number | Publication date |
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| CN102517893B (en) | 2016-01-20 |
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Free format text: FORMER OWNER: GUANGDONG HONGCHANG FABRIC + CLOTHING DESIGN HOLDING CO., LTD. FOSHAN SHUNE JUN-AN JEANS WEAR CREATIVE CENTER WUHAN TEXTILE UNIVERSITY Effective date: 20141009 |
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Effective date of registration: 20141009 Address after: Shunde District 528300 of Guangdong province Foshan City Jun'an Hongan Road No. 9 Applicant after: Guangdong Junan Jeans Research Institute Address before: Shunde District 528300 of Guangdong province Foshan City Jun'an Hongan Road No. 9 Applicant before: Guangdong Junan Jeans Research Institute Applicant before: Guangdong Hongchang Garment Creative Co., Ltd. Applicant before: Foshan Shune Jun-An Jeans Wear Creative Center Applicant before: Wuhan Textile University |
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Effective date of registration: 20161208 Address after: Shunde District 528300 of Guangdong province Foshan City Jun'an Hongan Road No. 9 Patentee after: Guangdong Junan Jeans Research Institute Patentee after: Wuhan Textile University Address before: Shunde District 528300 of Guangdong province Foshan City Jun'an Hongan Road No. 9 Patentee before: Guangdong Junan Jeans Research Institute |
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