CN1204668A - Natural plant bright red pigment for blanket kind and preparation and using method thereof - Google Patents
Natural plant bright red pigment for blanket kind and preparation and using method thereof Download PDFInfo
- Publication number
- CN1204668A CN1204668A CN 98102235 CN98102235A CN1204668A CN 1204668 A CN1204668 A CN 1204668A CN 98102235 CN98102235 CN 98102235 CN 98102235 A CN98102235 A CN 98102235A CN 1204668 A CN1204668 A CN 1204668A
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- red pigment
- bright red
- natural plant
- parts
- blanket
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
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- Chemical & Material Sciences (AREA)
- Organic Chemistry (AREA)
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Abstract
A bright red pigment for blanket or carpet is prepared from madder or Sufang wood dust through immersing it in cold water for 3-5 hr, addition of 3% wood alcohol as medium, filter, removing supernatant, heating to 18-22 deg.C, enclosing container, natural ferment at emp not lower 10 deg.C for 65-79 hr, and boiling to concentrate it to 50-70% of concentration to obtain bright red pigment liquid. Its application approach includes mixing the bright red pigment liquid with 5% tannic acid and water at 40 deg.C, immersing animal fibre or silk fibre, boiling, keeping the temp at 70-90 deg.C for 60-75 min, rinsing and centrifugal drying.
Description
A kind of natural plant bright red pigment for blanket kind and preparation thereof and using method belong to the blanket class with the preparation of natural plant pigment and bleaching and dyeing the field, are applicable to bleachinging and dyeing of fibers such as carpet, tapestry, seat blanket.
China's blanket class is produced, and the historical data record according to finding starts from Chinese end, up to bright clear, adopts natural phant dyeing always.Owing to the development of science and technology in modern age, natural phant dyeing is replaced by chemical staining gradually.Thereby traditional plant pigments extracts and the fiber bleaching and dyeing process is also lost thereupon.But,, easily make fabric fading if bleaching and dyeing process control is improper because chemical dye can cause very big pollution to environment in preparation and use.The blanket class of the accidental plant dyeing fibrage in market in the present age, but successfully from natural phant, do not extract as yet owing to primary colours are bright red, so can not produce a kind of blanket class that adopts natural plant pigment to bleaching and dyeing fibrage fully.
The object of the invention is to provide a kind of natural plant bright red pigment for blanket kind and preparation and using method.
The present invention seeks to realize like this, by weight with 100 portions of madders or Soviet Union's a tree, used in making timber for boats wood chip with the cold water soak of submergence amount 3～5 hours, adding 5～7 parts of weight percents and be 3% another name for is media, filter, leave standstill the filtrate layering after, discharge supernatant liquid, be warming up to 18～22 ℃, closed container.Boil through spontaneous fermentation in 65～79 hours, concentration is brought up to 50～70%, obtain bright red pigment liquid.During use, by weight with 1 part of bright red pigment liquid, 25～30 parts of 40 ℃ of water, 0.03～0.05 part of 5% Weibull put into reactor, drops into 5 parts of animal fibres or 6 parts of silk fibers, boils 20～30 minutes, soaks 60～75 minutes at 70～90 ℃.Rinsing dries.The bright red pigment that extracts with the inventive method can mix use with other natural plant dye and bleaching and dyeing as stated above to obtain other color fiber.
The present invention extracts bright red pigment from natural phant, and be used for bleachinging and dyeing animal and plant fiber, thereby be developed into to adopt fully and from natural phant, extract the blanket class that pigment is bleachinged and dyeing fibrage, fill up the infull blank of present natural phant coloured fibre look kind, developed " green " product of free of contamination pure natural.
In conjunction with the embodiments, specify as follows to technical scheme of the present invention:
Embodiment 1: 1 kilogram of madder or Soviet Union's a tree, used in making timber for boats wood chip with the cold water soak of submergence amount 3 hours, are added 50 gram weight per-cents and are 3% another name for, filter, leave standstill the filtrate layering after, lower floor's dye solution is placed reactor, be warming up to 18 ℃, closed container.Through spontaneous fermentation in 79 hours, boil that to be concentrated into concentration be 50% to make bright red pigment liquid.Restrain the bright red pigment liquid with 100 during use, 2.5 kilograms of 40 ℃ of water, 3 grams, 5% Weibull is put into reactor, drops into 500 gram animal fibres, boils 25 minutes, soaks 1 hour at 70 ℃, washs to dry.
Embodiment 2: with 1 kilogram of madder or Soviet Union's a tree, used in making timber for boats wood chip, with the cold water soak of submergence amount 4 hours, adding 60 gram weight per-cents and be 3% another name for was media, filters, leave standstill filtrate, after the layering, lower floor's dye solution is placed reactor, be warming up to 20 ℃, when envrionment temperature is not less than 10 ℃, closed container boils through spontaneous fermentation in 72 hours that to be concentrated into concentration be 60%, makes bright red pigment liquid.Restrain the bright red pigment liquid with 100 during use, 2.8 kilograms of 40 ℃ of water, 4 grams, 5% Weibull is put into reactor, puts into 600 gram silk fibers, boils 25 minutes, soaks 70 minutes the washing drying at 80 ℃.
Embodiment 3: with 1 kilogram of madder or Soviet Union's a tree, used in making timber for boats wood chip with the cold water soak of submergence amount 5 hours, adding 70 gram weight per-cents is that 3% another name for is a media, filter, leave standstill filtrate, after the layering, lower floor's dye solution is placed reactor, be warming up to 22 ℃, be not less than 10 ℃ through spontaneous fermentation in 65 hours in envrionment temperature, boil that to be concentrated into concentration be 70%, make bright red pigment liquid, during use, with 100 gram bright red pigment liquid, 3 kilograms of 40 ℃ of water, 5 grams, 5% Weibull is put into reactor, put 600 gram silk fibers, boiled 30 minutes, and soaked 75 minutes at 90 ℃, washing dries.
Claims (5)
1. natural plant bright red pigment for blanket kind, it is characterized in that by weight with 100 parts of madder or Soviet Union's a tree, used in making timber for boats wood chips, place reactor, with the cold water soak of submergence amount 3～5 hours, add 5～7 parts of weight percents and be 3% another name for, filter, leave standstill filtrate, after treating the filtrate layering, discharge supernatant liquid, lower floor's dye solution is heated to 18-22 ℃, stop heating, closed container, after spontaneous fermentation in 65～79 hours, boil again be concentrated into concentration be 50%-70% bleaching and dyeing natural plant bright red pigment for blanket kind liquid.
2. the preparation method of a natural plant bright red pigment for blanket kind, it is characterized in that by weight with 100 parts of madder or Soviet Union's a tree, used in making timber for boats wood chips, place reactor, cold water with the submergence amount steeped 3～5 hours, add 5～7 parts of weight percents and be 3% another name for, filter, leave standstill filtrate, after treating the filtrate layering, discharge supernatant liquid, lower floor's dye solution is heated to 18～22 ℃ stops heating, closed container, after spontaneous fermentation in 65～79 hours, boil again be concentrated into concentration be 50%～70% bleaching and dyeing natural plant bright red pigment for blanket kind liquid.
3. the using method of a natural plant bright red pigment for blanket kind is characterized in that by weight with 1 part of bright red pigment liquid, 25～30 parts of 40 ℃ of water, and 0.03～0.05 part 5% Weibull is put into reactor.Drop into 5 parts of animal fibres or 6 parts of silk fibers, boiled 20～30 minutes, soaked 60～75 minutes at 70～90 ℃, washing dries.
4. it is characterized in that and to transfer going out to be different from other color blanket class fiber bleaching and dyeing liquids of big red color with other natural plant dye by the described a kind of natural plant bright red pigment for blanket kind of claim 1.
5. press the method for the described a kind of natural plant bright red pigment for blanket kind of claim 4 and other natural plant dye accent to using, it is characterized in that by weight with 1 part of accent to good pigment solution, 25～30 parts of 40 ℃ of water, 0.03～0.05 part of 5% Weibull put into reactor, drop into 5 parts of animal fibres or 6 parts of silk fibers, boiled 20～30 minutes, and soaked 60～75 minutes at 70～90 ℃, the clear water washing dries.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98102235A CN1088729C (en) | 1998-06-09 | 1998-06-09 | Natural plant bright red pigment for blanket kind and preparation and using method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98102235A CN1088729C (en) | 1998-06-09 | 1998-06-09 | Natural plant bright red pigment for blanket kind and preparation and using method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1204668A true CN1204668A (en) | 1999-01-13 |
| CN1088729C CN1088729C (en) | 2002-08-07 |
Family
ID=5217219
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98102235A Expired - Fee Related CN1088729C (en) | 1998-06-09 | 1998-06-09 | Natural plant bright red pigment for blanket kind and preparation and using method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1088729C (en) |
Cited By (4)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100358950C (en) * | 2006-02-21 | 2008-01-02 | 海澜集团公司 | Madder dye extracting process and its usage in dyeing mercerized wool and mercerized wool fabric |
| CN102061632A (en) * | 2010-11-19 | 2011-05-18 | 南京工业大学 | Dyeing process of natural organic dye extracted from safflower |
| CN102094341A (en) * | 2010-12-07 | 2011-06-15 | 江南大学 | Method for dyeing real silk fabrics by extracting pigment from phytolacca by ultrasonic technology |
| CN107337935A (en) * | 2017-06-30 | 2017-11-10 | 李斌 | A kind of Preparation method and use of madder red pigment |
Family Cites Families (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1035512C (en) * | 1992-11-20 | 1997-07-30 | 辽宁省农业科学院高粱研究所 | Preparation for natural pigment sorghum red |
-
1998
- 1998-06-09 CN CN98102235A patent/CN1088729C/en not_active Expired - Fee Related
Cited By (6)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN100358950C (en) * | 2006-02-21 | 2008-01-02 | 海澜集团公司 | Madder dye extracting process and its usage in dyeing mercerized wool and mercerized wool fabric |
| CN102061632A (en) * | 2010-11-19 | 2011-05-18 | 南京工业大学 | Dyeing process of natural organic dye extracted from safflower |
| CN102061632B (en) * | 2010-11-19 | 2013-04-10 | 南京工业大学 | Dyeing process of natural organic dye extracted from safflower |
| CN102094341A (en) * | 2010-12-07 | 2011-06-15 | 江南大学 | Method for dyeing real silk fabrics by extracting pigment from phytolacca by ultrasonic technology |
| CN102094341B (en) * | 2010-12-07 | 2016-01-13 | 江南大学 | A kind of colouring method of real silk fabrics by extracting pigment from phytolacca by ultrasonic technology |
| CN107337935A (en) * | 2017-06-30 | 2017-11-10 | 李斌 | A kind of Preparation method and use of madder red pigment |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1088729C (en) | 2002-08-07 |
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