CN1088728C - Natural plant pure yellow pigment for blanket kind and preparation and using method thereof - Google Patents
Natural plant pure yellow pigment for blanket kind and preparation and using method thereof Download PDFInfo
- Publication number
- CN1088728C CN1088728C CN98102234A CN98102234A CN1088728C CN 1088728 C CN1088728 C CN 1088728C CN 98102234 A CN98102234 A CN 98102234A CN 98102234 A CN98102234 A CN 98102234A CN 1088728 C CN1088728 C CN 1088728C
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- China
- Prior art keywords
- yellow pigment
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- pure yellow
- natural plant
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- Legal status (The legal status is an assumption and is not a legal conclusion. Google has not performed a legal analysis and makes no representation as to the accuracy of the status listed.)
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Classifications
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- C—CHEMISTRY; METALLURGY
- C09—DYES; PAINTS; POLISHES; NATURAL RESINS; ADHESIVES; COMPOSITIONS NOT OTHERWISE PROVIDED FOR; APPLICATIONS OF MATERIALS NOT OTHERWISE PROVIDED FOR
- C09B—ORGANIC DYES OR CLOSELY-RELATED COMPOUNDS FOR PRODUCING DYES, e.g. PIGMENTS; MORDANTS; LAKES
- C09B61/00—Dyes of natural origin prepared from natural sources, e.g. vegetable sources
Abstract
The present invention relates to natural plant pure yellow pigment for blanket kinds and a preparation and using method thereof, which belongs to the field of preparing, bleaching and dyeing of natural plant pigment of blanket kinds. At present, pure yellow pigment is not extracted out from natural plants. According to the ratio of the weight, 100 shares of gardenia fruit powders, three to five shares of 3% acetic acids and 2000 to 2200 shares of cold water are put in a reaction vessel, heated to 50 DEG C, soaked for 100 to 140 minutes and filtered; filtrate is statically positioned, and clear liquids at the upper layer are exhausted after the filtrate is layered; dyeing liquids at the lower layer is boiled and concentrated to pure yellow pigment liquids with the concentration of 50% to 70%; one share of the pure yellow pigment liquids, double salt solution of 3% aluminum potassium sulfate with water, and 30 to 35 shares of water of 30 DEG C are dissolved in the vessel. Seven shares of animal fibers or nine shares of silk fibers are put in the vessel, soaked for 60 to 80 minutes and boiled for 30 to 40 minutes; when temperatures are decreased to 90 DEG C, the vessel is cleaned by cold water and dried.
Description
A kind of natural plant pure yellow pigment for blanket kind and preparation thereof and using method belong to the blanket class with the preparation of natural plant pigment and bleaching and dyeing the field, are applicable to bleachinging and dyeing of fibers such as carpet, tapestry, seat blanket.
China's blanket class is produced, and the historical data record according to finding starts from Chinese end, until bright clear, dyes with natural phant always.Owing to the development of science and technology in modern age, natural phant dyeing is replaced by chemical staining gradually.Thereby traditional plant pigments extracts and the fiber bleaching and dyeing process is also lost thereupon.But,, easily make fabric fading if bleaching and dyeing process control is improper because chemical dye can cause very big pollution to environment in preparation and use.Therefore, people are in rising trend always to the demand that adopts the blanket based article that the extraction pigment is bleachinged and dyeing from natural phant.The blanket class of plant dyeing fibrage in the existing market is not owing to true yellow successfully extracts from natural phant as yet, so can not produce a kind of blanket class that adopts natural plant pigment to bleaching and dyeing fibrage fully.
The object of the present invention is to provide a kind of natural plant pure yellow pigment for blanket kind and preparation thereof and using method.
The object of the present invention is achieved like this, by weight with 100 parts of cape jasmines fruit powder, 3～5 part 3% acetate, 2000～2200 parts of cold water add in the reactor progressively heats to 50 ℃, soaks after 100～140 minutes, filters, leave standstill filtrate, after treating the filtrate layering, discharge supernatant liquid, lower floor's dye solution is boiled to be concentrated into concentration be 50～70% true yellow pigment solution.During use, by weight with 1 part of true yellow pigment solution, 0.03 the moisture complex salt solution of～0.04 part 3% aluminum potassium sulfate, 30～35 parts of 30 ℃ of water are dissolved in the reactor jointly, drop into 7 parts of animal fibres or 9 parts of silk fibers, soak after 60～80 minutes, boiled 30～40 minutes, when temperature is reduced to 90 ℃, clean with cold water, loose colour promptly is the true yellow fiber that has no apricot pink or grass green tendency after cleaning.True yellow pigment with inventive method is extracted can also mix use with other natural plant dye, bleaching and dyeing by present method, obtaining being different from the blanket class fiber of true yellow color, thereby makes the blanket class that the natural plant pigment is bleachinged and dyeing.
The present invention extracts the true yellow pigment from natural phant, and in order to bleaching and dyeing animal and plant fiber, thereby be developed into to adopt fully and from natural phant, extract the blanket class that pigment is bleachinged and dyeing fibrage, fill up the infull blank of present natural phant coloured fibre look kind, developed " green " product of pollution-free pure natural.
In conjunction with the embodiments, specify as follows to technical scheme of the present invention:
Embodiment 1: with 1 kilogram in cape jasmine fruit powder, 3% acetate 30 grams in 20 kilograms of adding reactors of cold water, progressively are warming up to 50 ℃, soak after 100 minutes, filter, leave standstill filtrate, after treating the filtrate layering, discharge supernatant liquid, lower floor's dye solution is boiled to be concentrated into concentration be 50% true yellow pigment solution.During use, with 100 gram true yellow pigment solutions, the moisture complex salt solution of aluminum potassium sulfate of 3 grams 3%, 3 kilograms 30 ℃ water is dissolved in the reactor jointly, drop into 700 gram animal fibres, soak after 60 minutes, boil 30 minutes after, when temperature is reduced to 90 ℃, clean with cold water, loose colour promptly is the true yellow fiber that has no apricot pink or grass green tendency after cleaning.
Embodiment 2: with 1 kilogram in cape jasmine fruit powder, and 3% acetate, 40 grams, 21 kilograms of cold water add in the reactor, progressively are warming up to 50 ℃, soak after 120 minutes, filter, leave standstill filtrate, after treating the filtrate layering, discharge supernatant liquid, lower floor's dye solution is boiled to be concentrated into concentration be 60% true yellow pigment solution.During use, with 100 gram true yellow pigment solutions, the moisture complex salt solution of aluminum potassium sulfate of 4 grams 3%, 3.2 kilograms of 30 ℃ of water are dissolved in the reactor jointly, drop into 900 gram silk fibers, soak after 70 minutes, boiled 35 minutes, when temperature is reduced to 90 ℃, clean with cold water, loose colour promptly is the true yellow fiber that has no apricot pink or grass green tendency after cleaning.
Embodiment 3: with 1 kilogram in cape jasmine fruit powder, and 3% acetate, 50 grams, 22 kilograms of adding reactors of cold water, progressively heat soak 140 minutes to 50 ℃ after, filter, leave standstill filtrate, discharge supernatant liquid after waiting to filter layering, lower floor's dye solution is boiled to be concentrated into concentration be 70% true yellow pigment juice.During use, with 100 gram true yellow pigment solutions, the moisture complex salt solution of aluminum potassium sulfate of 4 grams 3% is poured in the reactor, drop into 700 gram animal fibres, soak after 80 minutes, be heated to boiling 40 minutes, when temperature is reduced to 90 ℃, clean with cold water, loose colour promptly is the true yellow fiber that has no apricot pink or grass green tendency after cleaning.
Claims (2)
1. the preparation method of a natural plant pure yellow pigment for blanket kind, it is characterized in that by weight with 100 parts of cape jasmines fruit powder, 3-5 part weight percent is 3% acetate, and 2000～2200 parts of cold water add in the reactor, progressively heat to 50 ℃, soak after 100～140 minutes, filter, leave standstill filtrate, treat the filtrate layering after, discharge supernatant liquid, lower floor's dye solution is boiled to be concentrated into concentration be 50～70% true yellow pigment solution.
2. the using method of a natural plant pure yellow pigment for blanket kind, it is characterized in that by weight with 1 part of true yellow pigment solution according to the method preparation of claim 1,0.03 the moisture complex salt solution of～0.04 part 3% aluminum potassium sulfate, 30～35 parts of 30 ℃ of water are dissolved in the reactor jointly, drop into 7 parts of animal fibres or 9 parts of silk fibers, soak after 60～80 minutes, boiled 30～40 minutes, and when temperature is reduced to 90 ℃, cleaned drying with cold water.
Priority Applications (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98102234A CN1088728C (en) | 1998-06-09 | 1998-06-09 | Natural plant pure yellow pigment for blanket kind and preparation and using method thereof |
Applications Claiming Priority (1)
| Application Number | Priority Date | Filing Date | Title |
|---|---|---|---|
| CN98102234A CN1088728C (en) | 1998-06-09 | 1998-06-09 | Natural plant pure yellow pigment for blanket kind and preparation and using method thereof |
Publications (2)
| Publication Number | Publication Date |
|---|---|
| CN1204667A CN1204667A (en) | 1999-01-13 |
| CN1088728C true CN1088728C (en) | 2002-08-07 |
Family
ID=5217218
Family Applications (1)
| Application Number | Title | Priority Date | Filing Date |
|---|---|---|---|
| CN98102234A Expired - Fee Related CN1088728C (en) | 1998-06-09 | 1998-06-09 | Natural plant pure yellow pigment for blanket kind and preparation and using method thereof |
Country Status (1)
| Country | Link |
|---|---|
| CN (1) | CN1088728C (en) |
Families Citing this family (3)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN102061632B (en) * | 2010-11-19 | 2013-04-10 | 南京工业大学 | Dyeing process of natural organic dye extracted from safflowers |
| CN102094341B (en) * | 2010-12-07 | 2016-01-13 | 江南大学 | A kind of colouring method of real silk fabrics by extracting pigment from phytolacca by ultrasonic technology |
| CN105113288B (en) * | 2015-09-08 | 2017-12-08 | 重庆欧荣莱汽车配件有限公司 | A kind of method for carrying out natural dyeing to fiber using carotenoid |
Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1097437A (en) * | 1993-07-12 | 1995-01-18 | 于浩 | The production method of corn yellow OB |
-
1998
- 1998-06-09 CN CN98102234A patent/CN1088728C/en not_active Expired - Fee Related
Patent Citations (1)
| Publication number | Priority date | Publication date | Assignee | Title |
|---|---|---|---|---|
| CN1097437A (en) * | 1993-07-12 | 1995-01-18 | 于浩 | The production method of corn yellow OB |
Also Published As
| Publication number | Publication date |
|---|---|
| CN1204667A (en) | 1999-01-13 |
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