CN1191047C - Additives composition for domestic chemical products, preparation method and application thereof - Google Patents

Abstract

The present invention relates to an additive composition used for daily chemical products, which comprises 25 to 45 wt% of aloe, 10 to 30 wt% of lanolin, 5 to 18 wt% of vitamin E, 14 to 25 wt% of maifanite and 14 to 25 wt% of titanium dioxide. The additive composition can be applied to bath fluid, facial cleanser, shampoo, masques, skin nourishing cream and other daily chemical products to improve the skin protection function of the daily chemical products. The present invention also relates to a preparation method of the additive composition.

Description

Be used for compositions of additives, preparation method and the application of daily chemical products

The present invention relates to a kind of compositions of additives that is used for daily chemical products and preparation method thereof, particularly, the compositions of additives that is used for daily chemical products that the present invention relates to mainly comprises Aloe, lanoline, vitamin E, Maifanitum and titanium dioxide.In bathings such as this compositions of additives can be applied to bath gel, cleanly shows, shampoo, facial film, emollient cream and the cosmetic product, can protect skin effectively.

Known in bathing and cosmetic product, need to add various additives, skin care promotes the cell growth, removes black speck, plays the effect of nutrition and protection skin.The skin health care cream for beauty that Chinese patent application prospectus CN1133171A has introduced with preparations such as Aloe, Radix Angelicae Sinensis, essence is used to remove black speck; CN1214242A has introduced with the bathing of the prevented dermatosis of twenties kind of plant such as Cortex Phellodendri preparation, sexually transmitted disease (STD) and has revealed; CN1194825 has introduced Nyctereutes procyonoides oil skincare product, is characterized in preventing skin aging; CN1128654 has introduced the protective skin cream that crease-resistant function is arranged.U.S. Pat P4369180 and US4704280 have introduced the face cosmetic of multivitamin combination.JP11005724A and JP10194935A have introduced the shampoo that promotes natural on-off cycles of hair growth.

The document of readding does not relate to Aloe, lanoline, vitamin E, Maifanitum and titanium dioxide is prepared compositions of additives, and is applied in the report in cosmetics of everyday use field.

The purpose of this invention is to provide a kind of compositions of additives that is used for daily chemical products; said composition comprises Aloe, lanoline, vitamin E, Maifanitum and titanium dioxide, and skin care can be provided simultaneously, promotes the metabolism of Skin Cell; eliminate black speck, the effect of nutrition and protection skin.

Compositions of additives comprises the Aloe of 25-45% (weight), the lanoline of 10-30% (weight), the vitamin E of 5-18% (weight), the Maifanitum of 14-25% (weight), 14-25% (weight) titanium dioxide.

Maifanitum and titanium dioxide are powder particle, and the Maifanitum mean diameter is the 0.05-10 micron, and the mean diameter of titanium dioxide is the 0.05-10 micron.

The present invention also provides the method for making this compositions of additives, and described method comprises the following steps:

(1) mix homogeneously in a container with maifanite powder and titania powder;

(2) lanoline is added in the reactor, keep 50 ℃ and stirred 30 minutes;

(3) be equipped with in the reactor of lanoline slowly joining step (2) under Maifanitum that obtains in the step (1) and the titanium dioxide mixture stirring, finished reinforced process in 1 hour, stir speed (S.S.) is 50 rev/mins;

(4) with in vitamin E and the disposable reactor that joins in the step (3) of Aloe, turn off heater, stir, finish whole process for preparation after 1.5 hours.

Can obtain this compositions of additives through above four steps.Be characterized in moistening, preserve moisture, whiten, when the ratio of nutrition, sun-proof, especially Maifanitum and titanium dioxide is higher effect more obvious.

This compositions of additives contains Aloe, lanoline, vitamin E, Maifanitum and titanium dioxide, makes through heating up several times, mixing in reactor.Medical experiment shows that Aloe, lanoline are the natural penetrating agent of human body skin, the moisturizing agent of epidermis cell, promotor of cell growth.Scientific research shows, when the particle size of Maifanitum and titanium dioxide is little during to the submicron order of magnitude or nanometer scale, specific surface area increases greatly, and photocatalysis is obvious, in the time of sun-proof, has deodorizing sterilizing effect preferably; Contain the required trace element of a certain amount of human body skin in the Maifanitum simultaneously, can be slightly soluble in the cosmetics of everyday use, skin is had Nutrition, promote the metabolism of some materials in the Skin Cell; The adding of vitamin E is nutrition and protection skin better.In the cosmeticses of everyday use such as this compositions of additives can be applied in bath gel, cleanly shows, shampoo, facial film, emollient cream; alleviate surfactant in these cosmeticses of everyday use to the stimulation of skin; promote the blood circulation and the metabolism of Skin Cell; moisten and skin nutrition; prevent ultraviolet radiation, protect skin better.At the function of different bathings and cosmetic product, the ratio of other composition in the proportioning of each component and the product makes the product that makes have functions peculiar separately in the adjusting compositions of additives.

Embodiment 1

According to the formulation compositions of additives in the following table 1, preparation method comprises the following steps:

(1) mean diameter is respectively maifanite powder and titania powder mix homogeneously in a container of 0.05 micron and 0.1 micron;

(2) lanoline is packed in the reactor, keep 50 ℃ and stirred 30 minutes;

(3) Maifanitum that obtains in the step (1) and titanium dioxide mixture are slowly joined step (2) and be equipped with in the reactor of lanoline, finished reinforced process in 1 hour, the range request that fed in raw material constantly stirs, and stir speed (S.S.) is 50 rev/mins;

(4) join in the step (3) in the reactor vitamin E and Aloe are disposable, can remove heater this moment, but will constantly stir, and can finish whole process for preparation after 1.5 hours, can obtain this compositions of additives.

Embodiment 2-4

Prepare the compositions of additives of embodiment 2-4 according to the mode of embodiment 1, the component and the content thereof of the compositions of additives of each embodiment are listed in table 1.Difference is: the mean diameter of Maifanitum is respectively 5 microns, 0.1 micron and 10 microns among the embodiment 2-4; The mean diameter of titanium dioxide is respectively 5 microns, 0.05 micron and 10 microns.

Table 1

Embodiment	Component (% weight)
						Aloe	Lanoline	Vitamin E	Maifanitum	Titanium dioxide
	1	25	30	15	15						15
2						45	13	14	14	14
	3	35	10	18	18						19
4						30	15	5	25	25

Embodiment 5

The prepared with additive compositions bath gel that makes with embodiment 1.The proportioning of other component of additive and bath gel is listed in the table below 2, and its preparation method is: add deionized water in reactor, be warming up to 75 ℃.Stir on one side, Yi Bian add ether alcohol sulfate (hereinafter referred to as AES), coconut oleoyl amine diethanolamine (hereinafter referred to as 6501), alkyl polyglucoside, cocamido propyl betaine (hereinafter referred to as CAB) successively, stir speed (S.S.) is 50 rev/mins.After the uniform dissolution, be cooled to 45 ℃ gradually, add the compositions of additives that embodiment 1 makes, behind the homodisperse, add citric acid, antiseptic and essence, continue to be stirred to evenly.Obtain containing the bath gel of this compositions of additives.

Table 2

Component	% (weight)
		Embodiment 1 additive	3.5
Alkyl polyglucoside	10
		AES	15
6501	3
		CAB	6
Essence	0.1
		Citric acid	In right amount
Antiseptic	In right amount
		Deionized water	Add to 100%

The bath gel of being prepared is faintly acid, and is non-stimulated to skin, uses back skin that smooth sensation is arranged, and skin care is arranged, and promotes the function of skin cell metabolism.

Embodiment 6

With clean the showing of prepared with additive compositions that embodiment 2 makes, its prescription is listed in table 3.The clean preparation method of showing is: add deionized water in reactor, be warming up to 75 ℃.Stir on one side, Yi Bian add lauric acid diethyl amide, alkyl polyglucoside, CAB, sorbitol successively, stir speed (S.S.) is 50 rev/mins.After the uniform dissolution, be cooled to 45 ℃ gradually, add compositions of additives, vitamin D, glutamic acid, serine that embodiment 2 makes, behind the homodisperse, add citric acid, antiseptic and essence, continue to be stirred to evenly.Obtaining containing the clean of this compositions of additives shows.

Table 3

Component	% (weight)
		The compositions of additives of embodiment 2	7
Margarita powder (10 microns of mean diameters)	1
		CAB	8
The lauric acid diethanolamine	7
		Sorbitol	1
Alkyl polyglucoside	20
		Vitamin D	0.5
Glutamic acid	0.2
		Serine	0.2
Essence	0.1
		Citric acid	In right amount
Antiseptic	In right amount
		Deionized water	Add to 100%

Add the compositions of additives of embodiment 2 preparations, clean the showing of preparation is faintly acid, and be non-stimulated to skin.Titanium dioxide in the additive combination compositions and Maifanitum have photocatalysis and Nutrition, can remove facial colour spot and dirt effectively and have germ-resistant function, and blood circulation and the metabolism that promotes Skin Cell had certain effect.

Embodiment 7

With the prepared with additive compositions shampoo that embodiment 3 makes, its prescription is listed in table 4.The preparation method of shampoo is: add deionized water in reactor, be warming up to 75 ℃.Stir on one side, Yi Bian add AES, 6501, CAB, oleoyl aminoacid sodium (being designated hereinafter simply as LEMEPON A) successively, stir speed (S.S.) is 50 rev/mins.After the uniform dissolution, add emulsified silicone oil, climbazole, zinc pyrithione (being designated hereinafter simply as ZPT) again, all after the dissolving, be cooled to 45 ℃ gradually, add compositions of additives, the vitamin B of preparation among the embodiment 3 ₅, behind the homodisperse, add citric acid, antiseptic and essence, continue to be stirred to evenly.Obtain containing the shampoo of this compositions of additives.

Table 4

Component	% (weight)
		The compositions of additives of embodiment 3	6.5
LEMEPONA	5
		AES	20
6501	4
		CAB	7
Emulsified silicone oil	2
		Climbazole	0.5
ZPT	0.2
		Vitamin B 5	0.5
Essence	0.1
		Citric acid	In right amount
Antiseptic	In right amount
		Deionized water	Add to 100%

The shampoo that adds the prepared with additive compositions of embodiment 3 preparations is faintly acid, and the bactericidal action of its distinctive prescription and climbazole, ZPT is obvious to the effect of hair debris removal itching relieving, emulsified silicone oil, LEMEPON A, V _B5The hair light is moistened.

Embodiment 8

With the prepared with additive compositions facial film that embodiment 4 makes, its prescription is listed in table 5.The preparation method of facial film is: add deionized water and polyvinyl alcohol in reactor, be warming up to 75 ℃ while stir, stir speed (S.S.) is 50 rev/mins.All after the dissolving, add glycerol, polyoxyethylene 20 sorbitan monolaurate successively, after the uniform dissolution, be cooled to 45 ℃ gradually, add the compositions of additives that embodiment 4 obtains, after stirring, add Sucus Cucumidis sativi, antiseptic, continue to be stirred to evenly.Obtain containing the facial film of this compositions of additives.

Table 5

Component	% (weight)
		The compositions of additives of embodiment 4	14
Glycerol	5
		Polyvinyl alcohol	15
Polyoxyethylene 20 sorbitan monolaurate	1.5
		Sucus Cucumidis sativi	3
Antiseptic	In right amount
		Deionized water	Add to 100%

The facial film that the compositions of additives of adding embodiment 4 preparations is made has the function of sterilization and skin nutrition; The component with photocatalysis that contains in this compositions of additives can promote the blood circulation and the metabolism of Skin Cell, makes skin of face pure white tender, eliminates tiny wrinkle.

Embodiment 9

According to the listed compositions of additives of the present invention of following table 6 and the prescription of other component, preparation emollient cream, compound method is as follows:

1), oil phase: add lanoline, vaseline, sorbitan monostearate (hereinafter referred to as class of department 60) successively, (2-(3 for UV absorbent UV-327,5-di-t-butyl-2-hydroxyl) phenyl-5-chlorinated benzotriazole), hexadeca-octadecyl alcohol, polydimethylsiloxane, keeping temperature of reaction kettle is 75 ℃, and stir speed (S.S.) is 50 rev/mins.

2), water: add deionized water in reactor, add polysorbate60, be warming up to 75 ℃, stir speed (S.S.) is 50 rev/mins.

3), mix: oil phase is put into water, continue to stir.

4), mix Maifanitum, titanium dioxide that particle mean size is respectively 0.1 micron and 0.05 micron, and glycerol, standby with the colloid mill porphyrize.

5) the, the 3rd) when temperature after the step is reduced to 60 ℃, with the 4th) the step prepared product adds the 3rd) in the mixed phase of step.Stir.

6), the 5th) be cooled to 45 ℃ gradually after the step, add Aloe, vitamin E, vitamin D, essence, antiseptic, continue to stir 15 minutes to evenly.Obtain containing emollient cream of this compositions of additives.

Table 6

Component	% (weight)
		Aloe	5％
Lanoline	5％
		Vitamin E	1％
Maifanitum	3％
		Titanium dioxide	3％
UV-327	1％
		Glycerol	10％
Vaseline	3％
		Hexadeca-octadecyl alcohol	6％
Polysorbate60	2％
		Class of department 60	2％
Polydimethylsiloxane	3％
		Vitamin D	0.5％
Essence	3％
		Antiseptic	In right amount
Deionized water	Add to 100%

Emollient cream that contains compositions of additives of the present invention of this embodiment preparation can make face pure white tender, and skin nutrition contains a large amount of ultraviolet light screeners and absorbent in the prescription of said composition, can prevent the injury of ultraviolet to skin effectively.

Claims (5)

1. compositions of additives that is used for daily chemical products, said composition comprises 25-45% weight Aloe, 10-30% weight lanoline, 5-18% weight vitamin E, 14-25% weight Maifanitum, 14-25% weight titanium dioxide.

2. the compositions of additives that is used for daily chemical products as claimed in claim 1, the mean diameter of described Maifanitum are the 0.05-10 micron.

3. the compositions of additives that is used for daily chemical products as claimed in claim 1, the mean diameter of described titanium dioxide are the 0.05-10 micron.

4. one kind prepares the described method that is used for the compositions of additives of daily chemical products of claim 1, and this method comprises the following steps:

(1) mix homogeneously in a container with maifanite powder and titania powder;

(2) lanoline is added in the reactor, keep 50 ℃ and stirred 30 minutes;

(3) be equipped with in the reactor of lanoline slowly joining step (2) under Maifanitum that obtains in the step (1) and the titanium dioxide mixture stirring, finished reinforced process in 1 hour, stir speed (S.S.) is 50 rev/mins;

(4) with in vitamin E and the disposable reactor that joins in the step (3) of Aloe, turn off heater, stir, finish whole process for preparation after 1.5 hours.

Among the claim 1-3 each described compositions of additives that is used for daily chemical products at bath gel, cleanly show, the application of shampoo, facial film and emollient cream cosmetics of everyday use.