CN117982395A - Skin-beautifying and anti-aging mask and preparation method thereof - Google Patents

Skin-beautifying and anti-aging mask and preparation method thereof Download PDF

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Publication number
CN117982395A
CN117982395A CN202311805085.6A CN202311805085A CN117982395A CN 117982395 A CN117982395 A CN 117982395A CN 202311805085 A CN202311805085 A CN 202311805085A CN 117982395 A CN117982395 A CN 117982395A
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component
skin
percent
water
aging
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陈来成
邹洁
杨荣鑫
丁红
杨占红
何秋星
李嘉琳
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Guangzhou Mashanghui Biotechnology Co ltd
Fujian Jingzhilian Biotechnology Co ltd
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Guangzhou Mashanghui Biotechnology Co ltd
Fujian Jingzhilian Biotechnology Co ltd
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Priority to CN202311805085.6A priority Critical patent/CN117982395A/en
Publication of CN117982395A publication Critical patent/CN117982395A/en
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Abstract

The invention belongs to the technical field of cosmetics, and discloses a skin-beautifying and anti-aging mask and a preparation method thereof. The facial mask comprises: a component: polyhydric alcohol, thickener, antioxidant and water; and the component B comprises the following components: neutralizing agent, humectant and water; and C, component: alpha-arbutin and water; and D, component: glycerol glucoside, 1.2-hexanediol, and herba Anoectochili Roxburghii enzymatic hydrolysate. The preparation method comprises the following steps: preparing anoectochilus formosanus enzymatic hydrolysate fermentation extract; adding an antioxidant into the polyol, dispersing, adding a thickener and water, and mixing to obtain a component A; sequentially adding a water-soluble humectant and a neutralizing agent into the component A, and mixing to obtain a mixed material; adding water-soluble alpha-arbutin into the mixed material, then adding the materials in the component D, and mixing to obtain the product. The mask provided by the invention contains the anoectochilus formosanus enzymatic hydrolysate fermentation extract, so that the effects of relieving, repairing, resisting the primary aging, lightening spots, brightening skin and the like are enhanced; the addition of the components such as the alpha-arbutin can effectively promote the tension, moisturize and whiten skin.

Description

Skin-beautifying and anti-aging mask and preparation method thereof
Technical Field
The invention belongs to the technical field of cosmetics, and particularly relates to a skin-beautifying and anti-aging mask and a preparation method thereof.
Background
Along with the improvement of living standard, people pay more attention to the selection of skin care and beauty products and skin care and beauty methods while paying more attention to the health of people. The facial mask is one of common products for beautifying and protecting skin, and has good effects in cleaning, moisturizing, whitening, controlling oil, relieving, tightening and the like. The existing novel mask mainly comprises polypeptide components, and skin cells are deeply cured by the polypeptide components, so that skin is relieved and repaired; however, it is difficult to achieve a soothing repair of the skin by only a single polypeptide component against damaged skin cells.
Therefore, it is necessary to provide a facial mask which can effectively relieve and repair facial skin, thereby achieving the effects of beautifying the skin and resisting the premature aging.
Disclosure of Invention
The present invention aims to solve at least one of the technical problems in the prior art described above. Therefore, the invention provides a skin-beautifying and anti-aging facial mask, which can clean, moisturize, whiten, tighten and resist aging facial skin and achieves the purposes of beautifying and resisting the aging by efficiently utilizing the anoectochilus formosanus enzymatic hydrolysate fermentation extract.
The invention also provides a preparation method of the skin-beautifying and anti-aging facial mask.
According to one aspect of the invention, a skin-care and anti-aging facial mask is provided, which comprises the following components in percentage by weight of the total weight of the skin-care and anti-aging facial mask:
a component: 4.50 to 8.00 percent of polyalcohol, 0.15 to 0.45 percent of thickener, 0.30 to 0.80 percent of antioxidant and 60.00 to 90.00 percent of water;
And the component B comprises the following components: 0.10 to 1.00 percent of neutralizer, 0.02 to 0.15 percent of humectant and 2.50 to 13.50 percent of water;
And C, component: alpha-arbutin 0.08-0.15%, water 1.00-5.00%;
And D, component: 0.25 to 0.35 percent of glyceroglycosides, 0.10 to 0.60 percent of 1, 2-hexanediol and 1.00 to 10.00 percent of anoectochilus formosanus enzymatic hydrolysate fermentation extract.
According to a preferred embodiment of the invention, there is at least the following advantageous effect:
The anoectochilus formosanus (Anoectochilus roxburghii) is perennial herb of the orchidaceae, also called anoectochilus formosanus, radix polygoni multiflori, anoectochilus formosanus, herba polygoni multiflori, and the like, is rich in yield, is a large amount of resources, has mild and sweet flavor, has been widely used as medicine and food homologous plants in people, has pharmacological effects of anti-inflammatory, liver protection, immunoregulation, calming, pain relieving, blood sugar reducing, blood fat reducing and the like, and is called as medicine king. The active ingredients of anoectochilus formosanus, namely the anoectochilus formosanus enzymatic hydrolysate fermentation extract, are added into the mask, so that the effects of relieving and repairing the mask, resisting the primary aging, lightening spots, brightening skin and the like are enhanced; in addition, the addition of the active ingredients such as the alpha-arbutin, the glyceroglycosides and the like ensures that after the facial mask disclosed by the invention is used, the facial skin of a user can be effectively lifted, moisturized and whitened.
In some embodiments of the present invention, the polyol comprises, in percent of each component based on the total weight of the skin-care, anti-aging mask: 2.00 to 4.00 percent of methyl propylene glycol and 2.50 to 4.00 percent of butanediol.
In some embodiments of the present invention, the thickener comprises, in percent of each component based on the total weight of the skin-care, anti-aging mask: 0.10 to 0.30 percent of xanthan gum and 0.05 to 0.15 percent of carbomer.
In some embodiments of the invention, the antioxidant is p-hydroxyacetophenone.
In some embodiments of the invention, the neutralizing agent is triethanolamine.
In some embodiments of the invention, the humectant is sodium hyaluronate.
In some embodiments of the invention, the anoectochilus formosanus enzymatic hydrolysate fermentation extract is prepared by combined fermentation of the anoectochilus formosanus enzymatic hydrolysate by lactic acid bacteria and microzyme.
In some embodiments of the invention, the water is selected from deionized water.
According to still another aspect of the present invention, there is provided a method for preparing the skin-care, anti-aging facial mask, comprising the steps of:
s1: preparing anoectochilus formosanus enzymatic hydrolysate fermentation extract;
s2: adding an antioxidant into the polyol, heating and dispersing, adding a thickener and water, and mixing to obtain a component A;
S3: adding a humectant dissolved by water in the component B into the component A, adding a neutralizing agent, and mixing to obtain a mixed material;
S4: adding alpha-arbutin which is dissolved in water in the component C in advance into the mixed material, and mixing; then adding the glucosyl glycoside, 1, 2-hexanediol and the anoectochilus formosanus enzymatic hydrolysate fermentation extract into the component D, and mixing to obtain the skin-beautifying and anti-aging facial mask.
In some embodiments of the invention, the method for preparing the anoectochilus roxburghii enzymatic hydrolysate fermentation extract in step S1 comprises the following steps:
a1: mixing herba Anoectochili powder with water, performing water bath and centrifugation, collecting precipitate, and drying to obtain herba Anoectochili residue;
A2: pulverizing the anoectochilus formosanus residue, mixing with a cellulase solution, and performing enzymolysis to obtain anoectochilus formosanus enzymolysis liquid;
A3: inoculating lactobacillus seed solution and saccharomycete seed solution into the anoectochilus formosanus enzymolysis solution, fermenting, centrifuging, taking supernatant, and freeze-drying to obtain the anoectochilus formosanus enzymolysis solution fermentation extract.
In some embodiments of the present invention, before step A1, the method further comprises the steps of: drying herba Anoectochili Roxburghii, and pulverizing to obtain herba Anoectochili Roxburghii powder.
Specifically, the anoectochilus formosanus powder is prepared by vacuum drying the anoectochilus formosanus at 45-55 ℃, crushing the anoectochilus formosanus in a traditional Chinese medicinal material crusher and sieving the crushed anoectochilus formosanus with a 60-mesh screen.
In some embodiments of the invention, the anoectochilus roxburghii powder in step A1 is mixed with the water in a ratio of 1: 100-4: 100 solid-to-liquid ratio.
In some embodiments of the invention, the temperature of the water bath of step A1 is 75-90℃for 3-3.5 hours.
In some embodiments of the invention, the centrifugation in step A1 is performed at a rotational speed of 7000 to 7500r/min for a period of 5 to 5.5min.
In some embodiments of the invention, the anoectochilus roxburghii residue in step A2 is crushed and then mixed with the cellulase solution according to a ratio of 1: 50-4: 50 solid to liquid ratio.
In some embodiments of the invention, the cellulase solution has a mass percent concentration of 0.35 to 0.55%.
In some embodiments of the invention, the conditions of the enzymatic hydrolysis in step A2 are: and (3) in a constant temperature shaking table at 45-55 ℃, 160-200 rpm, and carrying out enzymolysis for 5-7h.
In some embodiments of the present invention, step A3 is preceded by the step of activating the bacterial species: inoculating lactobacillus plantarum Mls-34 into MRS liquid culture medium according to an inoculum size of 1-3% v/v, standing and culturing for 12-14 h at 35-40 ℃ and carrying out passage for 2 times to prepare lactobacillus seed liquid; inoculating Saccharomyces cerevisiae CC-1 into PDA liquid culture medium in the inoculation amount of 1-3% v/v, standing and culturing at 28-35 deg.c for 24-26 hr, and passage 2 times to obtain the saccharomycete seed liquid.
In some embodiments of the present invention, step A3 is preceded by the further step of: sterilizing the anoectochilus formosanus enzymolysis solution at 120-123 ℃ for 15-18 min.
In some embodiments of the invention, the conditions of the fermentation of step A3 include: fermenting in a constant temperature incubator at 27-34 ℃ for 70-80 h.
In some embodiments of the invention, the centrifugation conditions of step A3 comprise: centrifuging at 4-6 deg.c for 5-7 min at 7000-7200 r/min.
In some embodiments of the present invention, step S2 adds the antioxidant into butanediol, heats to 65-75 ℃ for dispersion, then adds the thickener, the methyl propylene glycol and 80-90 ℃ water, and homogenizes for 3-5 min at 2500-3000 r/min to obtain the component A.
In some embodiments of the present invention, step S3 reduces the stirring speed when the temperature is reduced to 60-70 ℃, adds the humectant, in which the component B is dissolved in water, to the component a, then adds the neutralizing agent, and mixes the mixture.
In some embodiments of the present invention, step S4 adds the α -arbutin dissolved in the C component in advance with water at 55 to 65 ℃ to the mixture, and mixes them.
In some embodiments of the invention, step S4 is performed after the temperature is reduced to below 45 ℃, the glucosinolate, the 1, 2-hexanediol and the anoectochilus formosanus enzymatic hydrolysate fermentation extract in the component D are added, and the skin-beautifying and anti-aging mask is obtained after mixing and discharging.
Drawings
The invention is further described with reference to the accompanying drawings and examples, in which:
FIG. 1 is a graph showing the results of inhibition test of tyrosinase activity by skin care, anti-aging mask 2 and formulation matrix set in the test example of the present invention; wherein the sample group represents the skin-care and anti-aging mask 2; a. the different lower case letters of b, c and d represent differences in inhibition of tyrosinase between sample concentrations (p < 0.05).
Detailed Description
The following detailed description of embodiments of the invention, which are described with reference to the accompanying drawings, are exemplary only, and are not to be construed as limiting the invention.
In the description of the present invention, unless explicitly defined otherwise, terms such as centrifugation, fermentation, etc. should be construed broadly, and those skilled in the art can reasonably ascertain the specific meaning of the terms in the present invention by combining the specific contents of the technical solutions.
In the description of the present invention, reference to the term "one embodiment," "some embodiments," etc., means that a particular feature, material, or characteristic described in connection with the embodiment is included in at least one embodiment of the present invention. In this specification, schematic representations of the above terms do not necessarily refer to the same embodiment. Furthermore, the particular features, materials, or characteristics may be combined in any suitable manner in any one or more embodiments.
The test methods used in the examples are conventional methods unless otherwise specified; the materials, reagents and the like used, unless otherwise specified, are those commercially available.
The raw material sources are as follows:
Picking anoectochilus formosanus from greenhouse planting bases (batch number: 2023022603) of Jing lotus anoectochilus formosanus professional cooperation in south Jing county of Fujian province;
lactobacillus plantarum Mls-34 (CICC 22199) and Saccharomyces cerevisiae (CICC 1346) were purchased from China industry microbiological culture Collection center.
Example 1
The skin-care and anti-aging mask 1 is prepared in the embodiment, and comprises the following components in percentage by weight of the total weight of the skin-care and anti-aging mask 1:
A component: 3.00% of butanediol, 3.00% of methyl propylene glycol, 0.15% of xanthan gum, 0.08% of carbomer, 0.50% of p-hydroxyacetophenone and 84.82% of deionized water;
And the component B comprises the following components: triethanolamine 0.30%, sodium hyaluronate 0.05%, deionized water 5.00%;
And C, component: alpha-arbutin 0.10%, deionized water 1.00%;
And D, component: 0.30% of glucosyl, 0.20% of 1, 2-hexanediol and 1.50% of anoectochilus formosanus enzymatic hydrolysate fermentation extract.
The preparation process comprises the following steps:
(1) Preparing anoectochilus formosanus enzymatic hydrolysate fermentation extract: vacuum drying anoectochilus formosanus at 45-55 ℃, then putting the anoectochilus formosanus into a traditional Chinese medicinal material pulverizer for pulverizing, and sieving the anoectochilus formosanus with a 60-mesh screen to obtain anoectochilus formosanus powder;
mixing anoectochilus roxburghii powder with deionized water according to a proportion of 4: mixing the materials at a solid-liquid ratio of 100, treating for 3h in a water bath at 90 ℃, centrifuging for 5min at 7000r/min, collecting precipitate, and oven drying to obtain anoectochilus formosanus residue;
Pulverizing residue of herba Anoectochili in a traditional Chinese medicinal material pulverizer, sieving with 60 mesh sieve, and placing the pulverized residue of herba Anoectochili in a triangular flask according to the weight ratio of 1:50 solid-liquid ratio, adding cellulose enzyme solution with mass percent concentration of 0.35%, and carrying out enzymolysis for 6 hours at 200rpm in a constant temperature shaking table at 55 ℃ to obtain anoectochilus formosanus enzymatic hydrolysate;
Resuscitates the glycerol freezing tube of lactobacillus plantarum Mls-34 at room temperature, inoculates the glycerol freezing tube in MRS liquid culture medium with an inoculum size of 3% v/v, and carries out stationary culture for 12 hours at 35 ℃, and then carries out passage for 2 times to prepare lactobacillus seed liquid; resuscitates the glycerin freezing tube of the saccharomyces cerevisiae CC-1 at room temperature, inoculates the glycerin freezing tube into PDA liquid culture medium with the inoculum size of 3 percent v/v, and carries out stationary culture for 24 hours at 35 ℃, and the glycerin freezing tube is passaged for 2 times to prepare yeast seed liquid;
Sterilizing the anoectochilus formosanus enzymolysis liquid at 121 ℃ for 15min, inoculating lactobacillus seed liquid and saccharomycete seed liquid into the anoectochilus formosanus enzymolysis liquid at the same time in an ultra-clean workbench, and fermenting for 72h in a constant-temperature incubator at 34 ℃. After fermentation is finished, centrifuging the fermentation liquor for 2 times (7000 r/min,4 ℃ and 5 min), taking supernatant, and freeze-drying to obtain freeze-dried powder, thus obtaining the anoectochilus formosanus enzymatic hydrolysate fermentation extract.
(2) Adding antioxidant (0.50% of p-hydroxyacetophenone) into 3.00% of butanediol, heating to 65-75 ℃ for uniform dispersion, adding thickener (0.15% of xanthan gum and 0.08% of carbomer) and 3.00% of methyl propylene glycol, adding 84.82% of deionized water at 80-90 ℃ and homogenizing for 5min at 3000r/min to obtain the component A.
(3) When the temperature is reduced to 60-70 ℃, the stirring speed is reduced, the component B is added into the component A, the humectant (0.05% sodium hyaluronate) which is completely dissolved by 5.00% deionized water is added, and then the neutralizer (0.30% triethanolamine) is added, and the mixture is obtained after uniform stirring.
(4) Adding 0.10% of alpha-arbutin which is dispersed and dissolved in the component C by 1.00% of deionized water at 55-65 ℃ into the mixed material, and uniformly stirring; and (3) after the temperature is reduced to below 45 ℃, adding 0.30% of glyceroglycosides, 0.20% of 1, 2-hexanediol and 1.50% of anoectochilus formosanus enzymatic hydrolysate fermentation extract into the component D, stirring uniformly, and discharging to obtain the skin-beautifying and anti-aging mask 1.
Example 2
The skin-care and anti-aging mask 2 is prepared in the embodiment, and comprises the following components in percentage by weight of the total weight of the skin-care and anti-aging mask 2:
a component: 3.00% of butanediol, 3.00% of methyl propylene glycol, 0.15% of xanthan gum, 0.08% of carbomer, 0.50% of p-hydroxyacetophenone and 82.62% of deionized water;
And the component B comprises the following components: triethanolamine 0.50%, sodium hyaluronate 0.05%, deionized water 5.00%;
And C, component: alpha-arbutin 0.10%, deionized water 1.00%;
And D, component: 0.30% of glucosyl, 0.20% of 1, 2-hexanediol and 3.50% of anoectochilus formosanus enzymatic hydrolysate fermentation extract.
The specific preparation process is the same as in example 1.
Example 3
The skin-care and anti-aging mask 3 is prepared in the embodiment, and comprises the following components in percentage by weight of the total weight of the skin-care and anti-aging mask 3:
A component: 3.00% of butanediol, 3.00% of methyl propylene glycol, 0.15% of xanthan gum, 0.08% of carbomer, 0.50% of p-hydroxyacetophenone and 80.41% of deionized water;
And the component B comprises the following components: triethanolamine 0.70%, sodium hyaluronate 0.06%, deionized water 5.00%;
And C, component: alpha-arbutin 0.10%, deionized water 1.00%;
And D, component: 0.30% of glucosyl, 0.20% of 1, 2-hexanediol and 5.50% of anoectochilus formosanus enzymatic hydrolysate fermentation extract.
The specific preparation process is the same as in example 1.
Example 4
The skin-care and anti-aging mask 4 is prepared in the embodiment, and comprises the following components in percentage by weight of the total weight of the skin-care and anti-aging mask 4:
a component: 3.00% of butanediol, 3.00% of methyl propylene glycol, 0.15% of xanthan gum, 0.08% of carbomer, 0.50% of p-hydroxyacetophenone and 78.22% of deionized water;
and the component B comprises the following components: triethanolamine 0.90%, sodium hyaluronate 0.05%, deionized water 5.00%;
And C, component: alpha-arbutin 0.10%, deionized water 1.00%;
And D, component: 0.30% of glucosyl, 0.20% of 1, 2-hexanediol and 7.50% of anoectochilus formosanus enzymatic hydrolysate fermentation extract.
The specific preparation process is the same as in example 1.
Test examples
The efficacy of the skin-beautifying and anti-aging mask prepared in the example is tested in the test example.
1. The relaxing effect of the mask is tested:
50 subjects with symptoms of burning sensation, redness, stinging and itching on the skin and intolerance on the skin of the face are screened, and the subjects are subjected to four points of evaluation on the following four points, namely, relieving the burning sensation of the skin, improving the redness of the skin, relieving the stinging and itching on the skin and improving the tolerability of the skin, by referring to the standard of the table 1 after 2,4 weeks (28 days) of using the skin-beautifying and anti-aging mask prepared in the example 2, and the specific results are shown in the table 2.
Table 1 self-scoring criteria (7-level scoring)
Table 2 evaluation results of soothing effects (n=50)
Table 2 shows that all scores averaged over 5.42 after 28 days of use, statistically more than 50% of subjects gave positive evaluation of the soothing effect of skin-care, anti-aging mask 2. Wherein, 82% of subjects who "release skin burning sensation" are identified on day 28; "improve skin redness" has 78% of subjects acceptance at day 28; "relieve stinging and itching" 76% of subjects received at day 28; "improving skin tolerance" was recognized by 82% of subjects on day 28. The mask prepared by the invention has good relieving effect.
2. And (3) testing whitening effect:
The whitening efficacy of the skin-beautifying, anti-aging mask 2 prepared in example 2 was studied by tyrosinase activity inhibition test according to the T/GDCA006-2021 standard. Specifically, the formula matrix group (without the anoectochilus formosanus enzymatic hydrolysate fermentation extract) is compared with the sample group (namely the skin-beautifying and anti-aging mask 2), and the result is shown in figure 1. FIG. 1 shows that the inhibition of tyrosinase activity by the sample group (skin-beautifying, anti-aging mask 2) gradually increases with increasing sample concentration. When the concentration of the sample is 1000 mug/mL, the inhibition rate of tyrosinase reaches the maximum value 73.21%, which is higher than 71.41% of standard kojic acid and 69.40% of the formula matrix group. The result shows that the skin-beautifying and anti-aging mask 2 has an inhibition effect on tyrosinase activity.
Melanin synthesis is affected by tyrosinase, which catalyzes the hydroxylation of L-tyrosine to dopa and the oxidation of dopa to dopaquinone, which forms the final reaction product melanin. The skin-beautifying and anti-aging mask 2 has an inhibition effect on tyrosinase activity, which indicates that the mask can slow down tyrosinase to catalyze L-tyrosine to be converted into dopaquinone, namely can inhibit melanin formation. It can be seen that the skin-care and anti-aging mask 2 has remarkable whitening effect.
3. Testing of anti-aging efficacy:
50 subjects were screened, and after the subjects used the skin-beautifying, anti-aging mask prepared in example 2 for 2,5 weeks (35 days), the questionnaire was filled out with reference to the standard of table 1, and the subjects were evaluated for 5 items of slowing down skin sagging, increasing skin elasticity, reducing wrinkles, brightening skin color, reducing acne marks, and collecting receipts, and the results are shown in table 3.
Table 3 results of anti-presage test of skin-care, anti-presage mask 2 (n=50)
Table 3 shows that the acceptance rates of 5 test items of relieving skin relaxation, increasing skin elasticity, reducing wrinkles, brightening skin color and reducing acne marks are respectively 80%, 74%, 76%, 84% and 78%, which shows that the skin care and anti-aging mask 2 has obvious effects of relieving skin relaxation and brightening skin color, and has general effects on other items. Therefore, the facial mask has good anti-aging effect.
While the embodiments of the present invention have been described in detail, the present invention is not limited to the above embodiments, and various changes can be made without departing from the spirit of the present invention within the knowledge of those skilled in the art. Furthermore, embodiments of the invention and features of the embodiments may be combined with each other without conflict.

Claims (10)

1. The skin-beautifying and anti-aging facial mask is characterized by comprising the following components in percentage by weight of the total weight of the skin-beautifying and anti-aging facial mask:
a component: 4.50 to 8.00 percent of polyalcohol, 0.15 to 0.45 percent of thickener, 0.30 to 0.80 percent of antioxidant and 60.00 to 90.00 percent of water;
And the component B comprises the following components: 0.10 to 1.00 percent of neutralizer, 0.02 to 0.15 percent of humectant and 2.50 to 13.50 percent of water;
And C, component: alpha-arbutin 0.08-0.15%, water 1.00-5.00%;
And D, component: 0.25 to 0.35 percent of glyceroglycosides, 0.10 to 0.60 percent of 1, 2-hexanediol and 1.00 to 10.00 percent of anoectochilus formosanus enzymatic hydrolysate fermentation extract.
2. The skin care and anti-aging mask of claim 1, wherein the anoectochilus formosanus enzymatic hydrolysate fermentation extract is prepared by combined fermentation of the anoectochilus formosanus enzymatic hydrolysate by lactic acid bacteria and saccharomycetes.
3. The skin-care, anti-aging mask of claim 1, wherein the polyol comprises, in percent of the total weight of the skin-care, anti-aging mask: 2.00 to 4.00 percent of methyl propylene glycol and 2.50 to 4.00 percent of butanediol;
Preferably, the thickener comprises, in percentage by weight of each component based on the total weight of the skin-care, anti-aging mask: 0.10 to 0.30 percent of xanthan gum and 0.05 to 0.15 percent of carbomer;
preferably, the antioxidant is p-hydroxyacetophenone.
4. The skin-care, anti-aging mask of claim 1, wherein the neutralizing agent is triethanolamine;
Preferably, the humectant is sodium hyaluronate.
5. The method for preparing the skin-care and anti-aging mask according to any one of claims 1 to 4, which is characterized by comprising the following steps:
s1: preparing anoectochilus formosanus enzymatic hydrolysate fermentation extract;
s2: adding an antioxidant into the polyol, heating and dispersing, adding a thickener and water, and mixing to obtain a component A;
S3: adding a humectant dissolved by water in the component B into the component A, adding a neutralizing agent, and mixing to obtain a mixed material;
S4: adding alpha-arbutin which is dissolved in water in the component C in advance into the mixed material, and mixing; then adding the glucosyl glycoside, 1, 2-hexanediol and the anoectochilus formosanus enzymatic hydrolysate fermentation extract into the component D, and mixing to obtain the skin-beautifying and anti-aging facial mask.
6. The method according to claim 5, wherein the method for preparing the anoectochilus roxburghii enzymatic hydrolysate fermentation extract in step S1 comprises the following steps:
a1: mixing herba Anoectochili powder with water, performing water bath and centrifugation, collecting precipitate, and drying to obtain herba Anoectochili residue;
A2: pulverizing the anoectochilus formosanus residue, mixing with a cellulase solution, and performing enzymolysis to obtain anoectochilus formosanus enzymolysis liquid;
A3: inoculating lactobacillus seed solution and saccharomycete seed solution into the anoectochilus formosanus enzymolysis solution, fermenting, centrifuging, taking supernatant, and freeze-drying to obtain the anoectochilus formosanus enzymolysis solution fermentation extract.
7. The method according to claim 6, wherein the residue of Anoectochilus roxburghii in step A2 is crushed and then mixed with the cellulase solution according to the ratio of 1: 50-4: 50 solid to liquid ratio.
8. The preparation method according to claim 5, wherein step S2 comprises adding the antioxidant into butanediol, heating to 65-75deg.C for dispersion, adding the thickener, the methyl propylene glycol and 80-90deg.C water, homogenizing for 3-5 min at 2500-3500 r/min to obtain the component A.
9. The method according to claim 8, wherein the step S3 is performed by reducing the stirring speed when the temperature is reduced to 60 to 70 ℃, adding the humectant in which the component B is dissolved with water to the component a, adding the neutralizing agent, and mixing to obtain the mixed material.
10. The preparation method according to claim 9, wherein step S4 comprises adding the α -arbutin dissolved in the C component in advance with water at 55 to 65 ℃ to the mixture, and mixing; and (3) after the temperature is reduced to below 45 ℃, adding the glyceroglycosides, the 1, 2-hexanediol and the anoectochilus formosanus enzymatic hydrolysate fermentation extract into the component D, mixing, and discharging to obtain the skin-beautifying and anti-aging facial mask.
CN202311805085.6A 2023-12-26 2023-12-26 Skin-beautifying and anti-aging mask and preparation method thereof Pending CN117982395A (en)

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