CN117618471A - Scorpio traditional Chinese medicine decoction pieces and preparation method thereof - Google Patents
Scorpio traditional Chinese medicine decoction pieces and preparation method thereof Download PDFInfo
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- CN117618471A CN117618471A CN202311760964.1A CN202311760964A CN117618471A CN 117618471 A CN117618471 A CN 117618471A CN 202311760964 A CN202311760964 A CN 202311760964A CN 117618471 A CN117618471 A CN 117618471A
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- 238000002360 preparation method Methods 0.000 title claims abstract description 21
- 239000003814 drug Substances 0.000 title claims abstract description 17
- 241000522620 Scorpio Species 0.000 title claims description 60
- 239000009490 scorpio Substances 0.000 title claims description 60
- 241000239226 Scorpiones Species 0.000 claims abstract description 41
- XLYOFNOQVPJJNP-UHFFFAOYSA-N water Substances O XLYOFNOQVPJJNP-UHFFFAOYSA-N 0.000 claims description 47
- 238000001035 drying Methods 0.000 claims description 39
- 150000003839 salts Chemical class 0.000 claims description 22
- CURLTUGMZLYLDI-UHFFFAOYSA-N Carbon dioxide Chemical compound O=C=O CURLTUGMZLYLDI-UHFFFAOYSA-N 0.000 claims description 20
- 238000005406 washing Methods 0.000 claims description 18
- 238000004108 freeze drying Methods 0.000 claims description 15
- 238000000034 method Methods 0.000 claims description 15
- 238000002791 soaking Methods 0.000 claims description 12
- 239000012535 impurity Substances 0.000 claims description 11
- 238000007605 air drying Methods 0.000 claims description 10
- 229910002092 carbon dioxide Inorganic materials 0.000 claims description 10
- 239000001569 carbon dioxide Substances 0.000 claims description 10
- 230000018044 dehydration Effects 0.000 claims description 10
- 238000006297 dehydration reaction Methods 0.000 claims description 10
- 235000016257 Mentha pulegium Nutrition 0.000 claims description 5
- 244000246386 Mentha pulegium Species 0.000 claims description 5
- 235000004357 Mentha x piperita Nutrition 0.000 claims description 5
- 238000009835 boiling Methods 0.000 claims description 5
- 235000001050 hortel pimenta Nutrition 0.000 claims description 5
- 238000001914 filtration Methods 0.000 claims description 3
- 239000000706 filtrate Substances 0.000 claims description 2
- 238000011056 performance test Methods 0.000 description 10
- 239000002352 surface water Substances 0.000 description 8
- 238000007710 freezing Methods 0.000 description 7
- 230000008014 freezing Effects 0.000 description 7
- 230000000052 comparative effect Effects 0.000 description 6
- 239000000284 extract Substances 0.000 description 6
- 239000007789 gas Substances 0.000 description 6
- LFQSCWFLJHTTHZ-UHFFFAOYSA-N Ethanol Chemical compound CCO LFQSCWFLJHTTHZ-UHFFFAOYSA-N 0.000 description 5
- IJGRMHOSHXDMSA-UHFFFAOYSA-N Atomic nitrogen Chemical compound N#N IJGRMHOSHXDMSA-UHFFFAOYSA-N 0.000 description 4
- 201000010099 disease Diseases 0.000 description 4
- 208000037265 diseases, disorders, signs and symptoms Diseases 0.000 description 4
- 230000000694 effects Effects 0.000 description 4
- 229940079593 drug Drugs 0.000 description 3
- 239000002398 materia medica Substances 0.000 description 3
- 238000003672 processing method Methods 0.000 description 3
- 235000006679 Mentha X verticillata Nutrition 0.000 description 2
- 235000002899 Mentha suaveolens Nutrition 0.000 description 2
- 235000001636 Mentha x rotundifolia Nutrition 0.000 description 2
- 241001481692 Mesobuthus martensii Species 0.000 description 2
- 210000001015 abdomen Anatomy 0.000 description 2
- 239000002253 acid Substances 0.000 description 2
- 239000003795 chemical substances by application Substances 0.000 description 2
- 238000001514 detection method Methods 0.000 description 2
- 229910001873 dinitrogen Inorganic materials 0.000 description 2
- 238000004090 dissolution Methods 0.000 description 2
- 230000004048 modification Effects 0.000 description 2
- 238000012986 modification Methods 0.000 description 2
- 239000000047 product Substances 0.000 description 2
- 239000004575 stone Substances 0.000 description 2
- 208000011580 syndromic disease Diseases 0.000 description 2
- 230000002195 synergetic effect Effects 0.000 description 2
- 238000012360 testing method Methods 0.000 description 2
- 206010010904 Convulsion Diseases 0.000 description 1
- 240000007594 Oryza sativa Species 0.000 description 1
- 235000007164 Oryza sativa Nutrition 0.000 description 1
- 239000004480 active ingredient Substances 0.000 description 1
- QVGXLLKOCUKJST-UHFFFAOYSA-N atomic oxygen Chemical compound [O] QVGXLLKOCUKJST-UHFFFAOYSA-N 0.000 description 1
- 230000009286 beneficial effect Effects 0.000 description 1
- 230000037396 body weight Effects 0.000 description 1
- 239000003153 chemical reaction reagent Substances 0.000 description 1
- 238000004140 cleaning Methods 0.000 description 1
- 230000036461 convulsion Effects 0.000 description 1
- 238000007598 dipping method Methods 0.000 description 1
- 239000013505 freshwater Substances 0.000 description 1
- 235000011389 fruit/vegetable juice Nutrition 0.000 description 1
- 238000003306 harvesting Methods 0.000 description 1
- 229910052757 nitrogen Inorganic materials 0.000 description 1
- 239000001301 oxygen Substances 0.000 description 1
- 229910052760 oxygen Inorganic materials 0.000 description 1
- 238000012545 processing Methods 0.000 description 1
- 235000009566 rice Nutrition 0.000 description 1
- 239000002689 soil Substances 0.000 description 1
- 239000002904 solvent Substances 0.000 description 1
- 230000008961 swelling Effects 0.000 description 1
- 230000035922 thirst Effects 0.000 description 1
- 231100000419 toxicity Toxicity 0.000 description 1
- 230000001988 toxicity Effects 0.000 description 1
- 239000003053 toxin Substances 0.000 description 1
- 231100000765 toxin Toxicity 0.000 description 1
Abstract
The invention discloses a scorpion traditional Chinese medicine decoction piece and a preparation method thereof, and relates to the technical field of traditional Chinese medicine decoction piece preparation.
Description
Technical Field
The invention relates to the technical field of preparation of traditional Chinese medicine decoction pieces, in particular to scorpion traditional Chinese medicine decoction pieces and a preparation method thereof.
Background
The Scorpio is dried body of Buthus martensii Karsch Buthus martensii Karsch of Buthus martensii Karsch, and can be used for treating diseases caused by various reasons, such as convulsion, pyocutaneous disease, swelling toxin, rheumatism, etc. The scorpion needs to be processed to remove toxicity and then can be used as a medicine, and the traditional literature records that various processing methods such as cleaning, salt processing and the like are adopted for the scorpion, so that salt-processed scorpion is common in modern times. The light Scorpio is prepared by removing silt from Scorpio, decocting in boiling water until the body becomes stiff, taking out, placing in ventilated place, and drying in the shade or sun. The commodity circulation is called "fresh water cargo" or "light scorpion". The salt Scorpio is prepared by removing silt from Scorpio, decocting in boiling salt water until the body is stiff, taking out, placing in ventilated place, and drying in the shade or sun.
As for the processing method of scorpion, the recipe of the Chinese medicinal herb is firstly carried by the book of the Chinese medicinal herb, and the recipe of the Chinese medicinal herb is dried by fire when the Chinese medicinal herb is collected. "records in the book of the syndrome type: time of harvest. This is done by the people who are all forced to dry and die. "materia medica derived meaning: the Jinqingzhongshan stone is caught under the fire, and the Jinqingzhongshan stone is forced to be dried under the fire or is sun-dried in the sun. When the scorpion is thirsty and hot, the scorpion is fed with green mud, and the scorpion is killed by fire in the abdomen, so that the scorpion is dark in color and is sold with the intention of body weight. The doctor is familiar with the soil. "" Ben Cao Meng Gan (materia Medica of Ben Cao Meng): the Jinshijia's collection is not time-consuming, and the heat thirst is forced by the first day. The green mud is fed to fill the abdomen and the fire is burned to death. The red-colored rice is easy to sell. Weight and benefit. The disease-curing agents are known as soil-removing agents. With the whole recipe, stir-baked to brown again. "compendium of materia Medica: for patients with the syndrome of wind-damp disease, they are usually eaten with salt mud and are used as medicines for curing foot. For all cases, the drugs used in the present invention are scorpions, while the drugs used in the present invention are tail scorpions, so-called scorpion tips. ".
However, the existing processing method has low extract content, so that further improvement on the preparation method is needed.
Disclosure of Invention
The invention aims to at least solve one of the technical problems in the prior art and provides scorpion traditional Chinese medicine decoction pieces and a preparation method thereof.
The technical scheme of the invention is as follows:
a method for preparing Scorpio decoction pieces comprises removing impurities from Scorpio, washing with salt, drying for the first time, moistening in herba Menthae water, and drying for the second time.
As a preferable scheme of the invention, the first drying method is to dehydrate the scorpion after salt washing at low temperature, then dry the scorpion with cold air and finally freeze-dry the scorpion.
As a preferable scheme of the invention, the water content of the scorpion after low-temperature dehydration is at least 30wt%, and the water content of the surface of the scorpion after cold air drying is 5-10wt%.
As a preferable scheme of the invention, the temperature of the low-temperature dehydration is 30-50 ℃, and the temperature of the cold air drying is 5-10 ℃.
As a preferable mode of the present invention, the temperature of the freeze-drying is-20 to 10 ℃.
As a preferable scheme of the invention, the preparation method of the peppermint water comprises the following steps: adding folium Menthae into boiling water, soaking in sealed condition, filtering, and collecting filtrate.
As a preferable mode of the present invention, carbon dioxide gas is introduced at the same time as the moistening.
The invention also discloses a scorpion traditional Chinese medicine decoction piece which is prepared by adopting any one of the preparation methods.
The beneficial effects of the invention are as follows:
according to the preparation method of the scorpion traditional Chinese medicine decoction pieces, the scorpion is dehydrated at low temperature and then dried by cold air, so that the scorpion has different gradient water contents from inside to outside, the surface water content is lower than the internal water content, then in freeze drying, the internal water content is higher than the surface, the surface is less frozen, the internal is more frozen, the internal moisture frost heaving effect is improved, the cell breakage rate is improved, the dissolution of effective components is facilitated, moreover, the structure of the scorpion after freeze drying is sparse, the subsequent moistening of mint leaves is facilitated, and the synergistic effect of the scorpion and the internal water content is more excellent; finally, carbon dioxide gas is introduced during moistening, and the peppermint water and the scorpion have better moistening effect because the carbon dioxide is weak acid.
Detailed Description
Embodiments of the present invention are described in detail below. The following examples are illustrative only and are not to be construed as limiting the invention. The examples are not to be construed as limiting the specific techniques or conditions described in the literature in this field or as per the specifications of the product. The reagents or apparatus used were conventional products commercially available without the manufacturer's attention.
It should be noted that: the performance test method is as follows.
(1) The water content is not more than 20.0 percent (the second method of the fourth edition general rule 0832 of the year 2020 edition of Chinese pharmacopoeia).
(2) The total ash content is not more than 17.0 percent (the fourth edition of the general rule 2302 in the 2020 edition of Chinese pharmacopoeia).
The detection of the acid insoluble ash content is not more than 3.0 percent (the fourth edition of general rule 2302 in the 2020 edition of Chinese pharmacopoeia).
(3) The extract detection is determined by hot dipping method under the condition of alcohol soluble extract determination method (general rule 2201 of four parts of the year 2020 edition of Chinese pharmacopoeia) and using ethanol as solvent, and the content of ethanol is not less than 18.0%.
Example 1
A method for preparing Scorpio decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, and drying in oven for the first time (no more than 80deg.C, 70deg.C in this example);
adding 0.8 times of boiling water into herba Menthae, soaking in sealed container for 15 min, filtering to remove residue, and squeezing juice to obtain herba Menthae water.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and drying for a second time (60deg.C or less, 55 deg.C in this example, 5 hr).
The performance of the resulting test specimens is shown in Table 1.
Table 1 results of the performance test of example 1
Example 2
A preparation method of Scorpio Chinese medicinal decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, drying in oven for the first time, specifically, dehydrating Scorpio after washing salt to water content of 50wt% at low temperature, drying with cold air to obtain Scorpio surface water content of 10wt%, and lyophilizing. The temperature of the low-temperature dehydration is 35 ℃, and the temperature of the cold air drying is 10 ℃. The freeze drying is performed by freezing at-20deg.C and then drying at 10deg.C.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and finally drying for 5 hr at a temperature of not higher than 60deg.C.
The performance of the resulting test specimens is shown in Table 2.
Table 2 results of the performance test of example 2
Example 3
A preparation method of Scorpio Chinese medicinal decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, drying in oven for the first time, specifically, dehydrating Scorpio after washing salt to 40wt% of water content at low temperature, drying with cold air to obtain Scorpio surface water content of 8wt%, and lyophilizing. The temperature of the low-temperature dehydration is 40 ℃, and the temperature of the cold air drying is 8 ℃. The freeze drying is performed by freezing at-20deg.C and then drying at 10deg.C.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and finally drying for 5 hr at a temperature of not higher than 60deg.C.
TABLE 3 results of Performance test of example 3
Example 4
A preparation method of Scorpio Chinese medicinal decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, drying in oven for the first time, specifically, dehydrating Scorpio after washing salt to water content of 50wt% at low temperature, drying with cold air to obtain Scorpio surface water content of 10wt%, and lyophilizing. The temperature of the low-temperature dehydration is 30 ℃, and the temperature of the cold air drying is 6 ℃. The freeze drying is performed by freezing at-20deg.C and then drying at 10deg.C.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and finally drying for 5 hr at a temperature of not higher than 60deg.C.
TABLE 4 results of Performance test of example 4
Example 5
A preparation method of Scorpio Chinese medicinal decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, drying in oven for the first time, specifically, dehydrating Scorpio after washing salt to water content of 30wt% at low temperature, drying with cold air to obtain Scorpio surface water content of 5wt%, and freeze drying. The temperature of the low-temperature dehydration is 35 ℃, and the temperature of the cold air drying is 5 ℃. The freeze drying is performed by freezing at-20deg.C and then drying at 10deg.C.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and finally drying for 5 hr at a temperature of not higher than 60deg.C.
TABLE 5 results of Performance test of example 5
Example 6
A preparation method of Scorpio Chinese medicinal decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, drying in oven for the first time, specifically, dehydrating Scorpio after washing salt to water content of 30wt% at low temperature, drying with cold air to obtain Scorpio surface water content of 5wt%, and freeze drying. The temperature of the low-temperature dehydration is 35 ℃, and the temperature of the cold air drying is 5 ℃. The freeze drying is performed by freezing at-20deg.C and then drying at 10deg.C.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and finally drying for 5 hr at a temperature of not higher than 60deg.C. And introducing carbon dioxide gas while moistening.
TABLE 6 results of Performance test of example 6
Example 7
A preparation method of Scorpio Chinese medicinal decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, drying in oven for the first time, specifically, dehydrating Scorpio after washing salt to water content of 30wt% at low temperature, drying with cold air to obtain Scorpio surface water content of 5wt%, and freeze drying. The temperature of the low-temperature dehydration is 35 ℃, and the temperature of the cold air drying is 5 ℃. The freeze drying is performed by freezing at-20deg.C and then drying at 10deg.C.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and finally drying for 5 hr at a temperature of not higher than 60deg.C. The method comprises the steps of moistening, introducing mixed gas of carbon dioxide gas and nitrogen gas, wherein the volume ratio of carbon dioxide to nitrogen gas is 1:3.
TABLE 7 results of Performance test of example 7
Comparative example 1
A preparation method of Scorpio decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, and drying in oven (no more than 80deg.C, 70deg.C in this example).
Table 8 results of Performance test of comparative example 1
Comparative example 2
A method for preparing Scorpio decoction pieces comprises removing impurities from 3kg Scorpio, soaking Scorpio in 20 times of clear water for 1 hr, washing salt, draining, and drying in oven for the first time, specifically directly lyophilizing. The freeze drying is performed by freezing at-20deg.C and then drying at 10deg.C.
Then putting Scorpio in herba Menthae water, moistening for 24 hr, and finally drying for 5 hr at a temperature of not higher than 60deg.C.
Table 9 results of Performance test of comparative example 2
From the above examples and comparative examples, it is known that the extract content of the scorpion decoction pieces of the present invention is higher than that of the comparative examples, and the main reasons may be as follows: the method comprises the steps of firstly dehydrating at low temperature, then drying with cold air, so that the scorpion has different gradient water contents from inside to outside, the surface water content is lower than the internal water content, then in freeze drying, the internal water content is higher than the surface, the surface is less frozen, the internal is more frozen, the internal moisture frost heaving effect is improved, the cell breaking rate is improved, the dissolution of active ingredients is facilitated, moreover, the structure of the freeze-dried scorpion is sparse, the subsequent moistening of mint leaves is facilitated, and the synergistic effect of the two is more excellent; finally, carbon dioxide gas is introduced during the moistening, so that the moistening effect of peppermint water and scorpion can be better due to the weak acidity of the carbon dioxide, and the extract content of the embodiment 7 is optimal, possibly nitrogen is mixed into the carbon dioxide, so that the influence of oxygen on the extract is reduced in the atmosphere.
The above additional technical features can be freely combined and superimposed by a person skilled in the art without conflict.
The foregoing examples have shown only the preferred embodiments of the invention, which are described in more detail and are not to be construed as limiting the scope of the invention. It should be pointed out that various other corresponding changes and modifications can be made by those skilled in the art in light of the above description of the technical solution and the idea, and all such changes and modifications are intended to be within the scope of the invention as defined in the appended claims.
Claims (8)
1. A preparation method of scorpion traditional Chinese medicine decoction pieces is characterized by comprising the steps of removing impurities from scorpion, washing salt, drying for the first time, moistening in peppermint water, and drying for the second time.
2. The method for preparing the scorpion Chinese herbal pieces according to claim 1, wherein the first drying method is to dehydrate the salt-washed scorpion at low temperature, then dry the salt-washed scorpion with cold air, and finally freeze-dry the salt-washed scorpion.
3. The method for preparing Scorpio decoction pieces according to claim 2, wherein the water content of Scorpio after dehydration at low temperature is at least 30wt%, and the water content of Scorpio surface after cold air drying is 5-10wt%.
4. The scorpion traditional Chinese medicine decoction piece and the preparation method thereof according to claim 2, wherein the temperature of low-temperature dehydration is 30-50 ℃, and the temperature of cold air drying is 5-10 ℃.
5. The method for preparing scorpion decoction pieces according to claim 1, wherein the temperature of freeze-drying is-20-10 ℃.
6. The method for preparing the scorpion traditional Chinese medicine decoction pieces according to claim 1, wherein the method for preparing the peppermint water is as follows: adding folium Menthae into boiling water, soaking in sealed condition, filtering, and collecting filtrate.
7. The method for preparing Scorpio decoction pieces according to claim 1, wherein carbon dioxide gas is introduced while moistening.
8. A scorpion traditional Chinese medicine decoction piece, characterized in that the preparation method is adopted according to any one of claims 1-7.
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