CN117402675A - Grape essence, heating non-combustible smoking material, preparation method of heating non-combustible smoking material and cigarette product - Google Patents

Grape essence, heating non-combustible smoking material, preparation method of heating non-combustible smoking material and cigarette product Download PDF

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Publication number
CN117402675A
CN117402675A CN202311454887.7A CN202311454887A CN117402675A CN 117402675 A CN117402675 A CN 117402675A CN 202311454887 A CN202311454887 A CN 202311454887A CN 117402675 A CN117402675 A CN 117402675A
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China
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parts
powder
grape
heating non
grape essence
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CN202311454887.7A
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Inventor
岳浩杰
胡佳伟
王华文
况利平
赵波洋
赵贯云
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Dongguan Jichun Biotechnology Co ltd
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Dongguan Jichun Biotechnology Co ltd
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Priority to CN202311454887.7A priority Critical patent/CN117402675A/en
Publication of CN117402675A publication Critical patent/CN117402675A/en
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    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B15/00—Chemical features or treatment of tobacco; Tobacco substitutes, e.g. in liquid form
    • A24B15/10—Chemical features of tobacco products or tobacco substitutes
    • A24B15/16—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes
    • A24B15/167—Chemical features of tobacco products or tobacco substitutes of tobacco substitutes in liquid or vaporisable form, e.g. liquid compositions for electronic cigarettes
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24B—MANUFACTURE OR PREPARATION OF TOBACCO FOR SMOKING OR CHEWING; TOBACCO; SNUFF
    • A24B3/00—Preparing tobacco in the factory
    • A24B3/14—Forming reconstituted tobacco products, e.g. wrapper materials, sheets, imitation leaves, rods, cakes; Forms of such products
    • A—HUMAN NECESSITIES
    • A24—TOBACCO; CIGARS; CIGARETTES; SIMULATED SMOKING DEVICES; SMOKERS' REQUISITES
    • A24D—CIGARS; CIGARETTES; TOBACCO SMOKE FILTERS; MOUTHPIECES FOR CIGARS OR CIGARETTES; MANUFACTURE OF TOBACCO SMOKE FILTERS OR MOUTHPIECES
    • A24D1/00—Cigars; Cigarettes
    • A24D1/18—Selection of materials, other than tobacco, suitable for smoking
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0007—Aliphatic compounds
    • C11B9/0015—Aliphatic compounds containing oxygen as the only heteroatom
    • C—CHEMISTRY; METALLURGY
    • C11—ANIMAL OR VEGETABLE OILS, FATS, FATTY SUBSTANCES OR WAXES; FATTY ACIDS THEREFROM; DETERGENTS; CANDLES
    • C11B—PRODUCING, e.g. BY PRESSING RAW MATERIALS OR BY EXTRACTION FROM WASTE MATERIALS, REFINING OR PRESERVING FATS, FATTY SUBSTANCES, e.g. LANOLIN, FATTY OILS OR WAXES; ESSENTIAL OILS; PERFUMES
    • C11B9/00—Essential oils; Perfumes
    • C11B9/0061—Essential oils; Perfumes compounds containing a six-membered aromatic ring not condensed with another ring

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  • Chemical & Material Sciences (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Engineering & Computer Science (AREA)
  • Oil, Petroleum & Natural Gas (AREA)
  • Wood Science & Technology (AREA)
  • Organic Chemistry (AREA)
  • General Chemical & Material Sciences (AREA)
  • Manufacture Of Tobacco Products (AREA)
  • Cigarettes, Filters, And Manufacturing Of Filters (AREA)

Abstract

The application provides grape essence, a cigarette product, a heating non-combustion smoke material and a preparation method thereof. The grape essence comprises the following preparation raw materials in parts by weight: 10 to 20 parts of grape extract, 10 to 20 parts of blackcurrant extract, 3 to 7 parts of ethyl heptanoate, 2 to 10 parts of methyl anthranilate, 1 to 2 parts of myricetin, 1 to 2 parts of sweet orange oil, 1 to 3 parts of ethyl butyrate, 2 to 5 parts of ethyl acetate, 2 to 5 parts of ethyl butyrate, 3 to 6 parts of ethyl propionate, 2 to 5 parts of WS-23, 1 to 2 parts of menthol, 5 to 10 parts of ethanol, 2 to 5 parts of caprylic capric glyceride and 20 to 30 parts of propylene glycol. The grape essence can restore grape fragrance and generate pleasant grape smell, so that fragrance and taste close to natural grape juice can be released when the heating non-burning smoke material is heated, and the smoking pleasure and comfort of consumers are improved.

Description

Grape essence, heating non-combustible smoking material, preparation method of heating non-combustible smoking material and cigarette product
Technical Field
The application belongs to the technical field of cigarettes, and particularly relates to a grape essence, a heating non-combustion smoking material, a preparation method of the heating non-combustion smoking material and a cigarette product.
Background
The heating non-combustion cigarette products in the market at present mostly adopt tobacco powder or plant husk powder as a filler in the heating non-combustion smoke section, tobacco extract is used as a source of aroma in the heating non-combustion smoke section to blend cigarette taste, and the tobacco powder and the tobacco extract are used for blending, so that the taste is pure, but the nicotine content is unchanged, and the consumer still can produce addiction phenomenon.
Therefore, researchers research a 0-nicotine heating non-combustible cigarette, but the current 0-nicotine heating non-combustible cigarette has the defects of insufficient aroma and poor taste, and cannot meet the taste requirement of consumers for smoking the cigarette.
Disclosure of Invention
The embodiment of the application provides grape essence, a heating non-combustible smoke material, a preparation method thereof and a cigarette product, so as to solve the problems of insufficient aroma and poor taste of the traditional 0-nicotine heating non-combustible cigarette.
In a first aspect, an embodiment of the present application provides a grape essence, where the grape essence includes: 10 to 20 parts of grape extract, 10 to 20 parts of blackcurrant extract, 3 to 7 parts of ethyl heptanoate, 2 to 10 parts of methyl anthranilate, 1 to 2 parts of myricetin, 1 to 2 parts of sweet orange oil, 1 to 3 parts of ethyl butyrate, 2 to 5 parts of ethyl acetate, 2 to 5 parts of ethyl butyrate, 3 to 6 parts of ethyl propionate, 2 to 5 parts of WS-23, 1 to 2 parts of menthol, 5 to 10 parts of ethanol, 2 to 5 parts of caprylic capric glyceride and 20 to 30 parts of propylene glycol.
In a second aspect, embodiments of the present application further provide a heating non-combustion smoking material, where the smoking material includes, in parts by weight: 60-80 parts of plant powder base material without nicotine, 15-25 parts of grape essence, 2-5 parts of propylene glycol, 10-25 parts of glycerol, 2-5 parts of water, 1-2 parts of sodium carboxymethyl cellulose and 5-10 parts of caprylic/capric glyceride; wherein the grape essence is the grape essence.
Optionally, the plant powder base material is selected from one or more of lophatherum gracile powder, lily powder, platycodon grandiflorum powder, jasmine powder, hawthorn powder, red date powder, eugenol powder and rose powder; and/or the number of the sieving meshes of the plant powder bottom material is 100-200 meshes; and/or the water content of the plant powder bottom material is 5% +/-0.5%.
Optionally, the heated non-combustible smoking material has a moisture content of 5% ± 0.5%; and/or the heated non-combustible smoking material is particulate.
Optionally, the heating non-combustion fuming material is cylindrical particles, and the diameter of the cylindrical particles is 1-3 mm and the height of the cylindrical particles is 1-3 mm.
In a third aspect, embodiments of the present application further provide a method for preparing a heated non-combustible smoking material, the method for preparing a heated non-combustible smoking material comprising the steps of: uniformly mixing preparation raw materials of the heating non-combustion fuming material to obtain a mixture, wherein the preparation raw materials of the heating non-combustion fuming material comprise the following components in parts by mass: 60-80 parts of plant powder base material without nicotine, 15-25 parts of grape essence, 2-5 parts of propylene glycol, 10-25 parts of glycerol, 2-5 parts of water, 1-2 parts of sodium carboxymethylcellulose and 5-10 parts of caprylic/capric glyceride, wherein the grape essence is the grape essence; molding the mixture to obtain a pretreated material; and drying the pretreated material to obtain the heating non-combustion fuming material.
Optionally, the plant powder base material is selected from one or more of lophatherum gracile powder, lily powder, platycodon grandiflorum powder, jasmine powder, hawthorn powder, red date powder, eugenol powder and rose powder.
Optionally, the drying the pretreated material includes: and drying the pretreatment material until the water content is 5+/-0.5%.
Optionally, the drying the pretreated material includes: drying the pretreatment material at the temperature of 30-80 ℃ for 1-5 h; and placing the dried pretreatment material under a constant temperature and humidity environment for 24-32 h, so that the water content of the pretreatment material is 5% +/-0.5%, the temperature of the constant temperature and humidity environment is 20-25 ℃ and the humidity is 35-45 RH%.
In a fourth aspect, embodiments of the present application also provide a smoking article comprising the heated non-combustible smoking material described above, or a smoking article comprising the heated non-combustible smoking material produced by the method of manufacture described above.
The grape essence comprises, by mass, 10-20 parts of grape extract, 10-20 parts of blackcurrant extract, 3-7 parts of ethyl heptanoate, 2-10 parts of methyl anthranilate, 1-2 parts of myricetin, 1-2 parts of sweet orange oil, 1-3 parts of ethyl butyrate, 2-5 parts of ethyl acetate, 2-5 parts of ethyl butyrate, 3-6 parts of ethyl propionate, 2-5 parts of WS-23, 1-2 parts of menthol, 5-10 parts of ethanol, 2-5 parts of caprylic/capric glyceride and 20-30 parts of propylene glycol, and can reduce grape aroma to generate pleasant grape smell. The grape essence is used for preparing the heating non-burning smoke material, and fragrance and taste close to natural grape juice can be released when the smoke material is heated, so that smoke of a cigarette product containing the smoke material is clean, the aftertaste is long, sour and sweet grape smell is provided, meanwhile, the light mint cooling taste is kept, the mouth-by-mouth taste attenuation is less, pleasure and comfort of a consumer in the whole smoking process are improved, and the taste requirement of the consumer can be met.
Drawings
In order to more clearly illustrate the technical solutions in the embodiments of the present application, the drawings that are required to be used in the description of the embodiments will be briefly described below. It is obvious that the drawings in the following description are only some embodiments of the present application, and that other drawings may be obtained from these drawings without inventive effort to a person skilled in the art. Wherein like reference numerals refer to like parts throughout the following description.
Fig. 1 is a flowchart of a method for preparing a heated non-combustible smoking material according to an embodiment of the present application.
Detailed Description
The technical solutions in the embodiments of the present application will be clearly and completely described below with reference to the drawings in the embodiments of the present application. It will be apparent that the described embodiments are only some, but not all, of the embodiments of the present application. All other embodiments, which can be made by those skilled in the art based on the embodiments herein without making any inventive effort, are intended to be within the scope of the present application.
The embodiment of the application provides grape essence, which comprises the following preparation raw materials in parts by mass: 10 to 20 parts of grape extract, 10 to 20 parts of blackcurrant extract, 3 to 7 parts of ethyl heptanoate, 2 to 10 parts of methyl anthranilate, 1 to 2 parts of myricetin, 1 to 2 parts of sweet orange oil, 1 to 3 parts of ethyl butyrate, 2 to 5 parts of ethyl acetate, 2 to 5 parts of ethyl butyrate, 3 to 6 parts of ethyl propionate, 2 to 5 parts of WS-23, 1 to 2 parts of menthol, 5 to 10 parts of ethanol, 2 to 5 parts of caprylic capric glyceride and 20 to 30 parts of propylene glycol.
The grape essence provided by the embodiment of the application can reduce grape fragrance and generate pleasant grape smell, and WS-23 and menthol are added into the grape essence, so that the grape essence also has a mint cooling effect. Through being used for preparing the heating non-combustion smoking material with grape essence of this application, can release the fragrance and the taste that are close to natural grape juice when the smoking material heats, and WS-23 and menthol that add in the grape essence have fine heat resistance, can not volatilize fast under the heating temperature of the heating non-combustion smoking material for the flue gas of the cigarette goods that contains this smoking material is clean, the aftertaste is long, has sour and sweet grape smell, keeps the cool taste of light mint simultaneously, and the decay of mouth-by-mouth taste is less, has promoted consumer's pleasant sensation, comfort level in whole smoking in-process, can satisfy consumer's taste demand.
Illustratively, in the preparation raw materials of the grape essence, the grape extract and the blackcurrant extract can be 10 parts, 11 parts, 12 parts, 13 parts, 14 parts, 15 parts, 16 parts, 17 parts, 18 parts, 19 parts or 20 parts respectively, the ethyl heptanoate can be 3 parts, 4 parts, 5 parts, 6 parts or 7 parts, the methyl anthranilate can be 2 parts, 3 parts, 4 parts, 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts, the myricetin can be 1 part or 2 parts, the sweet orange oil can be 1 part or 2 parts, the ethyl butyrate can be 1 part, 2 parts or 3 parts, ethyl acetate may be 1 part, 2 parts, 3 parts, 4 parts or 5 parts, ethyl butyrate may be 1 part, 2 parts, 3 parts, 4 parts or 5 parts, ethyl propionate may be 3 parts, 4 parts, 5 parts or 6 parts, WS-23 may be 2 parts, 3 parts, 4 parts or 5 parts, menthol may be 1 part or 2 parts, ethanol may be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts, caprylic/capric glyceride may be 2 parts, 3 parts, 4 parts or 5 parts, propylene glycol may be 20 parts, 21 parts, 22 parts, 23 parts, 24 parts, 25 parts, 26 parts, 27 parts, 28 parts, 29 parts or 30 parts, and may be specifically set according to actual needs.
The embodiment of the application also provides a heating non-combustion fuming material, which comprises the following preparation raw materials in parts by mass: 60-80 parts of plant powder base material without nicotine, 15-25 parts of grape essence, 2-5 parts of propylene glycol, 10-25 parts of glycerol, 2-5 parts of water, 1-2 parts of sodium carboxymethyl cellulose and 5-10 parts of caprylic/capric glyceride; wherein the grape essence is the grape essence. It can be understood that the heating non-combustion smoking material provided by the embodiment of the application has no addictive component nicotine in the preparation raw materials, and the heating non-combustion smoking material can be used for preparing the 0-nicotine cigarette product, so that the purpose of no addictive hazard is achieved.
The grape essence can reduce grape aroma and generate pleasant grape smell, WS-23 and menthol added in the grape essence also have a lasting mint cooling effect, and fragrance and taste close to natural grape juice can be released when the non-combustion smoke material is heated by adding the grape essence into the non-combustion smoke material, so that smoke of a cigarette product containing the heated non-combustion smoke material is clean, the aftertaste is long, sour and sweet grape smell is achieved, meanwhile, the light mint cooling taste is kept, the mouth-by-mouth taste attenuation is less, the pleasure and comfort of a consumer in the whole smoking process are improved, and the taste requirement of the consumer can be met.
For example, in the preparation raw materials of the heating non-combustible smoking material, the plant powder base material free of nicotine can be 60 parts, 62 parts, 65 parts, 68 parts, 70 parts, 72 parts, 75 parts, 78 parts or 80 parts, the grape essence can be 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts or 25 parts, the propylene glycol can be 2 parts, 3 parts, 4 parts or 5 parts, the glycerol can be 10 parts, 12 parts, 15 parts, 18 parts, 20 parts, 22 parts or 25 parts, the water can be 2 parts, 3 parts, 4 parts or 5 parts, the sodium carboxymethyl cellulose can be 1 part or 2 parts, the caprylic capric glyceride can be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts, and the preparation can be specifically set according to practical requirements.
Optionally, the plant powder base material can be selected from one or more of Lophatherum gracile powder, bulbus Lilii powder, radix Platycodi powder, flos Jasmini sambac powder, fructus crataegi powder, fructus Jujubae powder, flos Caryophylli powder and flos Rosae Rugosae powder. According to the method, one or more of lophatherum gracile powder, lily powder, platycodon grandiflorum powder, jasmine powder, hawthorn powder, red date powder, clove powder and rose powder are used as plant powder base materials, the plant powder base materials are blended according to the characteristics of various plant powder, and the proper plant powder base material formula can better release grape fragrance of grape essence, so that consumers can obtain better smoking experience.
Optionally, the plant powder substrate is sieved with 100-200 meshes, for example, 100 meshes, 110 meshes, 120 meshes, 130 meshes, 140 meshes, 150 meshes, 160 meshes, 170 meshes, 180 meshes, 190 meshes or 200 meshes, etc.
Alternatively, the water content of the plant powder base material is 5% ± 0.5%, for example, 4.5%, 4.6%, 4.7%, 4.8%, 4.9%, 5%, 5.1%, 5.2%, 5.3%, 5.4%, or 5.5%, etc.
Alternatively, the heated non-combustible smoking material may have a moisture content of 5% ± 0.5%, for example 4.5%, 4.6%, 4.7%, 4.8%, 4.9%, 5%, 5.1%, 5.2%, 5.3%, 5.4% or 5.5%, etc.
Alternatively, the heated non-combustible smoking material may be in particulate, filamentary or sheet form. For example, the heated non-combustible smoking material may be cylindrical particles having a diameter of 1mm to 3mm and a height of 1mm to 3mm. By way of example, the height of the cylindrical pellets may be 1mm, 1.5mm, 2mm, 2.5mm, 3mm, etc., and the diameter of the cylindrical pellets may be 1mm, 1.5mm, 2mm, 2.5mm, 3mm, etc.
Referring to fig. 1, the embodiment of the application further provides a preparation method of the heating non-combustion smoke material, which includes the following steps:
step S100: uniformly mixing the preparation raw materials of the heating non-combustion fuming material to obtain a mixture, wherein the preparation raw materials of the heating non-combustion fuming material comprise the following components in parts by mass: 60-80 parts of plant powder base material without nicotine, 15-25 parts of grape essence, 2-5 parts of propylene glycol, 10-25 parts of glycerol, 2-5 parts of water, 1-2 parts of sodium carboxymethylcellulose and 5-10 parts of caprylic/capric glyceride, wherein the grape essence is the grape essence;
step S200: molding the mixture to obtain a pretreated material;
step S300: and drying the pretreated material to obtain the heating non-burning fuming material.
Illustratively, in step S100, the nicotine-free plant powder base material may be 60 parts, 62 parts, 65 parts, 68 parts, 70 parts, 72 parts, 75 parts, 78 parts or 80 parts, the grape essence may be 15 parts, 16 parts, 17 parts, 18 parts, 19 parts, 20 parts, 21 parts, 22 parts, 23 parts, 24 parts or 25 parts, the propylene glycol may be 2 parts, 3 parts, 4 parts or 5 parts, the glycerol may be 10 parts, 12 parts, 15 parts, 18 parts, 20 parts, 22 parts or 25 parts, the water may be 2 parts, 3 parts, 4 parts or 5 parts, the sodium carboxymethylcellulose may be 1 part or 2 parts, the caprylic/capric glyceride may be 5 parts, 6 parts, 7 parts, 8 parts, 9 parts or 10 parts, and may be specifically set according to practical requirements.
Optionally, in step S100, the plant powder base material is selected from one or more of lophatherum gracile powder, lily powder, platycodon root powder, jasmine powder, hawthorn powder, red date powder, clove powder and rose powder.
Specifically, the preparation steps of the plant powder base material can be as follows: pulverizing the raw materials of the plant powder base material, sieving the plant powder base material with 100-200 meshes, uniformly premixing the plant powder base material with 100-200 meshes obtained by sieving, placing the plant powder base material in a constant temperature and constant humidity environment for 24-32 h, wherein the humidity of the constant temperature and constant humidity environment is 35-45 RH% and the temperature is 20-25 ℃, and the water content of the plant powder base material is 5+/-0.5%.
Optionally, in step S200, the mixture is subjected to a molding process, and the obtaining the pretreated material includes: the mixture is passed through a pore plate with the aperture of 1 mm-3 mm to form a mixture column, the mixture column is cut to prepare cylindrical particles with the diameter of 1 mm-3 mm and the height of 1 mm-3 mm, and the obtained cylindrical particles are the pretreatment material. Alternatively, the mixture may be placed in a granulator (e.g., a screw extrusion granulator) to be granulated to obtain cylindrical granules having a diameter of 1mm to 3mm and a height of 1mm to 3mm, and the obtained cylindrical granules are the pretreated material.
In other embodiments, shaping the mixture to obtain a pre-treated material may also include: processing the mixture into filaments to obtain a filament-shaped pretreated material; alternatively, the mixture is processed into a sheet form to obtain a sheet-like pretreated material.
Optionally, in step S300, the drying treatment of the pretreated material includes: the pretreated material is dried to a moisture content of 5% ± 0.5%. Illustratively, the pretreatment material may be dried to a moisture content of 4.5%, 4.6%, 4.7%, 4.8%, 4.9%, 5%, 5.1%, 5.2%, 5.3%, 5.4%, or 5.5%, etc.
Specifically, in step S300, the drying treatment of the pretreated material may include: the pretreated material is dried for 1 to 5 hours at the temperature of between 30 and 80 ℃; and placing the dried pretreatment material for 24-32 h under a constant temperature and humidity environment, so that the water content of the pretreatment material is 5% +/-0.5%, the temperature of the constant temperature and humidity environment is 20-25 ℃ and the humidity is 35-45 RH%.
Illustratively, the pretreatment material may be dried at a temperature of 30 ℃, 35 ℃, 40 ℃, 45 ℃, 50 ℃, 55 ℃, 60 ℃, 65 ℃, 70 ℃, 75 ℃, or 80 ℃ for 1h, 1.5h, 2h, 2.5h, 3h, 3.5h, 4h, 4.5h, or 5h, etc.; the dried pretreatment material can be placed under the constant temperature and humidity environment for 24 hours, 25 hours, 26 hours, 27 hours, 28 hours, 29 hours, 30 hours, 31 hours or 32 hours, the temperature of the constant temperature and humidity environment can be 20 ℃, 21 ℃, 22 ℃, 23 ℃, 24 ℃ or 25 ℃, and the humidity of the constant temperature and humidity environment can be 35RH%, 36RH%, 37RH%, 38RH%, 39RH%, 40RH%, 41RH%, 42RH%, 43RH%, 44RH% or 45RH%.
Embodiments of the present application also provide a smoking article comprising the heated non-combustible smoking material described above, or a smoking article comprising a heated non-combustible smoking material produced by the method of manufacture described above. Because the cigarette product adopts all the technical schemes of all the embodiments, the cigarette product at least has all the beneficial effects brought by the technical schemes of the embodiments, and the description is omitted here.
Technical solutions and technical effects of the present application will be described in detail through specific examples and comparative examples, and the following examples are only some examples of the present application, and are not intended to limit the present application in any way.
Example 1
Example 1 provides a heated non-combustible smoking material and a heated non-combustible cigarette.
The preparation method of the heating non-burning smoke generating material comprises the following steps:
according to the parts by weight, 80 parts of plant powder base material, 15 parts of grape essence, 2 parts of propylene glycol, 20 parts of glycerol, 2 parts of water, 2 parts of sodium carboxymethylcellulose and 5 parts of caprylic/capric glyceride are uniformly stirred, and then are made into cylindrical particles with the diameter of 1mm and the height of 2mm through a pore plate with the aperture of 1mm, the cylindrical particles are dried in a hot air drying box at 50 ℃ for 4 hours, and then are placed in a constant temperature and humidity box for 24 hours, the humidity between the constant temperature and the constant humidity is 45RH% and the temperature is 25 ℃, so that the heating non-combustion smoke material with the water content of 5.3% is obtained.
Wherein, according to the parts by weight, plant powder foundation material includes: 80 parts of lily powder, 2 parts of lophatherum gracile powder, 5 parts of jasmine powder, 2 parts of hawthorn powder, 3 parts of red date powder, 5 parts of clove powder and 3 parts of rose powder.
The grape essence comprises the following preparation raw materials in parts by weight: 15 parts of grape extract, 15 parts of blackcurrant grape extract, 3 parts of ethyl heptanoate, 10 parts of methyl anthranilate, 1 part of myricetin, 1 part of sweet orange oil, 2 parts of ethyl butyrate, 3 parts of ethyl acetate, 3 parts of ethyl butyrate, 5 parts of WS-23, 2 parts of menthol, 4 parts of ethyl propionate, 5 parts of ethanol, 5 parts of caprylic-capric glyceride and 30 parts of propylene glycol.
And filling the heating non-combustible fuming material into a paper tube to obtain the heating non-combustible cigarette.
Examples 2 to 17
Examples 2 to 17 are basically the same as example 1, except that: the plant powder base material has different formulas and the grape essence has different mass parts of the preparation raw materials. The specific formula of the plant powder base material is shown in table 1, the specific mass parts of the preparation raw materials of the grape essence are shown in table 2, and the plant powder base material and the grape essence adopted in each of examples 2-17 are shown in table 3.
The heating non-combustible smoking materials of examples 2 to 17 were respectively filled into different paper tubes, to obtain heating non-combustible cigarettes of examples 2 to 17.
Examples 18 to 32
Examples 18 to 32 are basically the same as example 1, except that: the parts by mass of the partially prepared raw materials of the heated non-combustible smoking material are different, and the specific parts by mass of each prepared raw material are shown in table 4.
The heating non-combustible smoking materials of examples 18 to 32 were respectively filled into different paper tubes, to obtain heating non-combustible cigarettes of examples 18 to 32.
TABLE 1 formula of plant powder base material
TABLE 2 preparation of grape essence
TABLE 3 preparation of smoking Material of examples 2-17
TABLE 4 preparation raw materials for smoking materials of examples 18-32
The heated non-combustible cigarettes prepared in examples 1 to 32 were taken, the sample B was a heated non-combustible sample sold under the trade name IQOS cartridge by Feimo International Co., ltd, the sample C was a hundred fruit series purple grape 0 nicotine cigarette sold by Meyer technology Co., ltd, 20 professional tobacco sensory evaluators were selected to evaluate the sensory effects of the 34 samples, the evaluation indexes are shown in Table 5, and the sensory effect evaluation results are shown in Table 6.
The evaluation requirements are as follows:
1. the people who evaluate the suction are highly concentrated and cannot be disturbed or influenced by the environment.
2. The evaluation room is clean and silent, and has no noise. The people to be assessed need to judge alone and can not talk with each other so as not to influence the judgment of other people.
3. The evaluation room needs to be well ventilated, and has no foreign odor interference. The person who evaluates the medicine needs not to apply cosmetics with fragrance and medicines such as wanjinli oil, rheumatism ointment, essential balm and the like; the odor emitted by kerosene, gasoline flowers and plants, chemicals and the like cannot be generated in the evaluation chamber; and the ventilation device is started to timely remove smoke, so that the freshness of indoor air is ensured.
4. The temperature and humidity of the suction chamber should be appropriate. The temperature of the evaluating and sucking chamber is 18-25 ℃, and the relative humidity of air is kept between 55% and 70%; the temperature should not be too high (> 30 ℃) or too low (< 10 ℃) nor should the relative humidity of the air be too high (> 75%) or too low (< 30%), which would otherwise affect the sensitivity of the sense organ.
5. The same type of stabilizing heater must be chosen for the appliance to evaluate and to calibrate already through mouthfeel.
6. Coffee, milk and fruit flavored beverages must not be consumed during the evaluation to avoid affecting taste sensitivity.
TABLE 5 evaluation index
TABLE 6 sensory Effect evaluation results
As can be seen from Table 6, the sensory effect evaluation of the heated non-combustible cigarettes of examples 1 to 32 was superior to that of sample C, and the heated non-combustible cigarettes of examples 1 to 32 had the advantages of less unpleasant taste, comfortable smoking feeling, coordinated aroma, long lasting aroma, comfortable aftertaste and less irritation to the throat, and more satisfied the consumer's needs in aroma and taste.
From table 6, it can be seen that the sensory effect evaluation of the heated non-combustible cigarettes of examples 1 to 32 in terms of aftertaste, comfort, fragrance harmonic schedule, fragrance durability, and miscellaneous taste are all relatively close to that of sample C, so that it can be seen that the 0-nicotine heated non-combustible cigarettes of examples 1 to 32 have the substitution capability of the conventional cigarettes, can meet the smoking cessation demands of some consumers, and can meet the taste demands of consumers.
In the foregoing embodiments, the descriptions of the embodiments are emphasized, and for parts of one embodiment that are not described in detail, reference may be made to related descriptions of other embodiments.
In the description of the present application, the terms "first," "second," and the like are used for descriptive purposes only and are not to be construed as indicating or implying relative importance or implicitly indicating the number of technical features indicated. Thus, features defining "first," "second," etc. may explicitly or implicitly include one or more features. The term "and/or" includes any and all combinations of one or more of the associated listed items.
The grape essence, the cigarette product, the heating non-combustion fuming material and the preparation method thereof provided by the embodiment of the application are described in detail, the specific examples are used for describing the principle and the implementation mode of the application, and the description of the above examples is only used for helping to understand the method and the core idea of the application; meanwhile, as those skilled in the art will vary in the specific embodiments and application scope according to the ideas of the present application, the contents of the present specification should not be construed as limiting the present application in summary.

Claims (10)

1. The grape essence is characterized by comprising the following raw materials in parts by weight:
10 to 20 parts of grape extract, 10 to 20 parts of blackcurrant extract, 3 to 7 parts of ethyl heptanoate, 2 to 10 parts of methyl anthranilate, 1 to 2 parts of myricetin, 1 to 2 parts of sweet orange oil, 1 to 3 parts of ethyl butyrate, 2 to 5 parts of ethyl acetate, 2 to 5 parts of ethyl butyrate, 3 to 6 parts of ethyl propionate, 2 to 5 parts of WS-23, 1 to 2 parts of menthol, 5 to 10 parts of ethanol, 2 to 5 parts of caprylic capric glyceride and 20 to 30 parts of propylene glycol.
2. The heating non-combustion fuming material is characterized by comprising the following preparation raw materials in parts by weight:
60-80 parts of plant powder base material without nicotine, 15-25 parts of grape essence, 2-5 parts of propylene glycol, 10-25 parts of glycerol, 2-5 parts of water, 1-2 parts of sodium carboxymethyl cellulose and 5-10 parts of caprylic/capric glyceride;
wherein the grape essence is the grape essence of claim 1.
3. A heated non-combustible smoking material according to claim 2 wherein the plant meal base is selected from one or more of lophatherum gracile powder, lily powder, balloonflower powder, jasmine powder, hawthorn powder, red date powder, clove powder and rose powder;
and/or the number of the sieving meshes of the plant powder bottom material is 100-200 meshes;
and/or the water content of the plant powder bottom material is 5% +/-0.5%.
4. A heated non-combustible smoking material according to claim 2 having a moisture content of 5% ± 0.5%; and/or the heated non-combustible smoking material is particulate.
5. A heated non-combustible smoking material according to claim 4 in the form of cylindrical particles having a diameter of from 1mm to 3mm and a height of from 1mm to 3mm.
6. A method of preparing a heated non-combustible smoking material, the method comprising the steps of:
uniformly mixing preparation raw materials of the heating non-combustion fuming material to obtain a mixture, wherein the preparation raw materials of the heating non-combustion fuming material comprise the following components in parts by mass: 60-80 parts of plant powder base material without nicotine, 15-25 parts of grape essence, 2-5 parts of propylene glycol, 10-25 parts of glycerol, 2-5 parts of water, 1-2 parts of sodium carboxymethylcellulose and 5-10 parts of caprylic/capric glyceride, wherein the grape essence is the grape essence of claim 1;
molding the mixture to obtain a pretreated material;
and drying the pretreated material to obtain the heating non-combustion fuming material.
7. The preparation method according to claim 6, wherein the plant powder base material is one or more selected from Lophatherum gracile powder, bulbus Lilii powder, radix Platycodonis powder, jasmine powder, fructus crataegi powder, fructus Jujubae powder, flos Caryophylli powder, and flos Rosae Rugosae powder.
8. The method of preparing according to claim 6, wherein the drying the pretreated material comprises: and drying the pretreatment material until the water content is 5+/-0.5%.
9. The method of preparing according to claim 8, wherein the subjecting the pretreated material to a drying process comprises:
drying the pretreatment material at the temperature of 30-80 ℃ for 1-5 h; and placing the dried pretreatment material under a constant temperature and humidity environment for 24-32 h, so that the water content of the pretreatment material is 5% +/-0.5%, the temperature of the constant temperature and humidity environment is 20-25 ℃ and the humidity is 35-45 RH%.
10. A smoking article comprising a heated non-combustible smoking material according to any one of claims 1 to 5 or produced by the method of any one of claims 6 to 9.
CN202311454887.7A 2023-11-02 2023-11-02 Grape essence, heating non-combustible smoking material, preparation method of heating non-combustible smoking material and cigarette product Pending CN117402675A (en)

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