CN117309673A - Cigar dynamic suction resistance detection method - Google Patents

Cigar dynamic suction resistance detection method Download PDF

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Publication number
CN117309673A
CN117309673A CN202311053123.7A CN202311053123A CN117309673A CN 117309673 A CN117309673 A CN 117309673A CN 202311053123 A CN202311053123 A CN 202311053123A CN 117309673 A CN117309673 A CN 117309673A
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China
Prior art keywords
dynamic
suction
mouth
cigar
test sample
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Pending
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CN202311053123.7A
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Chinese (zh)
Inventor
王珵珵
王乐
刘阳
朱文魁
张佳巍
胡庆文
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China Tobacco Sichuan Industrial Co Ltd
Zhengzhou Tobacco Research Institute of CNTC
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China Tobacco Sichuan Industrial Co Ltd
Zhengzhou Tobacco Research Institute of CNTC
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Application filed by China Tobacco Sichuan Industrial Co Ltd, Zhengzhou Tobacco Research Institute of CNTC filed Critical China Tobacco Sichuan Industrial Co Ltd
Priority to CN202311053123.7A priority Critical patent/CN117309673A/en
Publication of CN117309673A publication Critical patent/CN117309673A/en
Pending legal-status Critical Current

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    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N7/00Analysing materials by measuring the pressure or volume of a gas or vapour
    • G01N7/10Analysing materials by measuring the pressure or volume of a gas or vapour by allowing diffusion of components through a porous wall and measuring a pressure or volume difference
    • G01N7/12Analysing materials by measuring the pressure or volume of a gas or vapour by allowing diffusion of components through a porous wall and measuring a pressure or volume difference the diffusion being followed by combustion or catalytic oxidation
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N15/00Investigating characteristics of particles; Investigating permeability, pore-volume or surface-area of porous materials
    • G01N15/08Investigating permeability, pore-volume, or surface area of porous materials
    • G01N15/082Investigating permeability by forcing a fluid through a sample
    • G01N15/0826Investigating permeability by forcing a fluid through a sample and measuring fluid flow rate, i.e. permeation rate or pressure change
    • GPHYSICS
    • G01MEASURING; TESTING
    • G01NINVESTIGATING OR ANALYSING MATERIALS BY DETERMINING THEIR CHEMICAL OR PHYSICAL PROPERTIES
    • G01N31/00Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods
    • G01N31/12Investigating or analysing non-biological materials by the use of the chemical methods specified in the subgroup; Apparatus specially adapted for such methods using combustion

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  • Chemical & Material Sciences (AREA)
  • Physics & Mathematics (AREA)
  • Life Sciences & Earth Sciences (AREA)
  • Health & Medical Sciences (AREA)
  • Biochemistry (AREA)
  • Analytical Chemistry (AREA)
  • General Health & Medical Sciences (AREA)
  • General Physics & Mathematics (AREA)
  • Immunology (AREA)
  • Pathology (AREA)
  • Combustion & Propulsion (AREA)
  • Engineering & Computer Science (AREA)
  • Chemical Kinetics & Catalysis (AREA)
  • Fluid Mechanics (AREA)
  • Dispersion Chemistry (AREA)
  • Molecular Biology (AREA)
  • Manufacturing Of Cigar And Cigarette Tobacco (AREA)

Abstract

The invention discloses a cigar dynamic suction resistance detection method, which obtains the fluctuation condition of the dynamic suction resistance of a whole leaf cigar during the combustion process by measuring the dynamic suction resistance of the whole leaf cigar, obtains the dynamic data of each cigar when each cigar burns for a certain length, and provides convenience for research and analysis of relevant indexes such as the dynamic suction resistance, the density and the like of the whole leaf cigar product.

Description

Cigar dynamic suction resistance detection method
Technical Field
The invention relates to the technical field of cigars, in particular to a cigar dynamic resistance detection method.
Background
The resistance to smoking is one of the key factors affecting the internal quality of cigarettes and is also an important factor directly affecting the consumer's smoking experience. The dynamic smoke resistance of the whole leaf rolled cigar is usually measured by YC/T461-2013 definition and standard condition of cigar smoking machine for routine analysis, and the dynamic smoke resistance of the cigarette can be measured. By measuring the dynamic suction resistance of the whole leaf cigar, the fluctuation condition of the dynamic suction resistance of the whole leaf cigar in the combustion process can be known. Different from the traditional cigarettes, the internal tobacco shred filling property is uniform, the number of the suction ports is fixed, and the number of the suction ports is usually 7-10, but the number of the suction ports of the whole-leaf cigar rolled by the same specification is greatly different due to various factors such as raw material varieties, manual rolling, manufacturing process and the like. In this case, when the difference in the number of suction ports of the whole leaf rolled cigar products of the same specification is large, it is difficult to perform research and analysis of the related indexes such as dynamic suction resistance and density. Therefore, a reasonable dynamic resistance detection method needs to be established to solve the similar problems, and the method has important significance for the research and analysis of the whole leaf cigar rolling.
Disclosure of Invention
The invention aims to solve the problems and provide a cigar dynamic suction resistance detection method which satisfies the correlation analysis of relevant indexes such as the dynamic suction resistance of the whole leaf rolled cigar products with the same specification under the condition that the suction ports of the whole leaf rolled cigar products with the same specification are greatly different.
The invention realizes the above purpose through the following technical scheme:
the cigar dynamic suction resistance detection method comprises the following steps:
step 1, placing a test cigarette in an environment with the temperature of 20+/-2 ℃ and the humidity of 62+/-5%, and carrying out balancing treatment for at least 48 hours;
step 2, setting equipment parameters according to the test sample: duration of suction: 1.5s, aspiration frequency: 40 s/bite;
step 3, selecting M samples to be fixed on a holder of the smoking machine one by one, wherein the angle formed by a longitudinal axis of the test sample and a horizontal plane is as follows: the end of the cigarette butt is lower than the other end by not more than 10 degrees and higher than the other end by not more than 5 degrees; igniting the test samples by using a hand-held electric igniter without contacting or pre-burning the test samples, wherein the ignition of each test sample reaches the combustion of the whole end face of the combustion end of the test sample;
and 4, performing axial data processing on the mouth-by-mouth dynamic suction resistance data and the burning length of the mouth-by-mouth burning cone of each test sample to obtain dynamic suction resistance data when each test sample burns with the same length.
Further, in the step 2, the smoking machine is a limited suction type smoking machine, the connecting pipeline between the smoke catcher and the suction mechanism should have as small airflow resistance as possible, the pressure drop of the total circulating pipeline between the end of the cigarette butt and the suction mechanism is not more than 300PA before suction, the total volume of all the suction channels is not more than 125mL, and the catcher filter disc needs to be replaced before each test, and the flow is calibrated.
In the step 3, in the testing process, the length of the cigarette combustion cone after each port of suction is measured and recorded; after the test sample is sucked into the N ports, when the combustion cone reaches the same position mark of each test sample butt, the suction is manually stopped, and the air is prevented from being continuously sucked through cigars; and obtaining the mouth-by-mouth dynamic suction resistance data of M test samples and the mouth-by-mouth combustion cone combustion length data of each test sample.
In the step 4, the axial data processing method is as follows: according to the test requirement, setting a same burning length L of each opening, taking the average value (X1+X2)/2 of the nearest two dynamic resistance data (X1 and X2) at each L length to obtain the dynamic data at the current L length, and finally obtaining the dynamic data of each cigarette at each burning length L.
The invention has the beneficial effects that:
according to the cigar dynamic suction resistance detection method, the fluctuation condition of the dynamic suction resistance of the whole leaf cigar in the combustion process is obtained through measuring the dynamic suction resistance of the whole leaf cigar, dynamic data of each cigar in a certain length are obtained, and convenience is provided for research and analysis of relevant indexes such as the dynamic suction resistance and the density of the whole leaf cigar.
Drawings
In order to more clearly illustrate the technical solutions of the embodiments of the present invention, the following description will briefly explain the practical drawings required in the embodiments or the prior art description, and it is obvious that the drawings in the following description are only some embodiments of the present invention, and other drawings can be obtained according to these drawings without inventive effort for a person skilled in the art.
Figure 1 shows a dynamic suction resistance diagram of each mouth of a cigarette A.
Figure 2 shows the dynamic suction resistance diagram of cigarettes A at the same distance.
Figure 3 shows a dynamic suction resistance diagram for each mouth of a cigarette B.
Figure 4 shows the dynamic suction resistance diagram of cigarettes B at the same distance.
Figure 5 is a graph of dynamic draw resistance per mouth of a cigarette C.
Figure 6 shows the dynamic resistance drawing of cigarettes C at the same distance.
Detailed Description
In order to make the objects, technical solutions and advantages of the present invention more apparent, the technical solutions of the present invention will be described in detail below. It will be apparent that the described embodiments are only some, but not all, embodiments of the invention. All other embodiments, based on the examples herein, which are within the scope of the invention as defined by the claims, will be within the scope of the invention as defined by the claims.
Example 1
The test selection product is a full leaf rolled cigar in great wall (10 branches 132 made in secret) of cigar factory in great wall of Sichuan, the specification is 110mm in length, 47mm in circumference, 6.3g in weight and 12mm in diameter of the tail opening;
step one: the cigar with the specification is placed in the same experimental environment (the temperature is 20+/-2 ℃ and the humidity is 62+/-5%) for 48 hours of balancing treatment;
step two: setting equipment parameters according to the diameter of a test sample to be 31 mL/port of suction capacity, 40 s/port of suction interval and 1.5s of suction time;
step three: m samples are selected and are fixed on a smoking machine clamp holder one by one, the test samples are ignited by using a hand-held electric igniter without contacting or pre-burning the test samples, and the ignition of each test sample must reach the combustion of the whole end face of the combustion end of the test sample; in the test process, measuring and recording the length of the cigarette combustion cone after each port is sucked; after the test sample was drawn through the N port, the drawing was manually terminated until the length of the butt remained 30mm, preventing continued drawing of air through the cigar; obtaining mouth-by-mouth dynamic suction resistance data of M test samples and mouth-by-mouth combustion cone combustion length data of each test sample;
step four: performing axial data processing on the mouth-by-mouth dynamic suction resistance data and the burning length of the mouth-by-mouth burning cone of each test sample by using a difference averaging method to obtain dynamic suction resistance data when each test sample burns for the same length; the axial data processing method comprises the following steps: according to the test requirement, setting a same burning length L of each opening, taking the average value (X1+X2)/2 of the nearest two dynamic resistance data (X1 and X2) at each L length to obtain the dynamic data at the current L length, and finally obtaining the dynamic data of each cigarette at each burning length L.
As shown in fig. 1-6: the test sample is three cigarettes with the length of 110mm, and after each cigarette burns for 80mm, the suction is stopped, and the number of suction ports of the cigarette A, B, C is 100, 84 and 96 respectively. According to the length of each test sample after suction and the dynamic suction resistance data, the average difference method of the two nearest dynamic suction resistance data at each 1mm length is adopted to obtain the current dynamic data at 1mm, and finally the dynamic data of three cigarettes at each 1mm length are obtained.
The foregoing is merely illustrative of the present invention, and the present invention is not limited thereto, and any person skilled in the art will readily recognize that variations or substitutions are within the scope of the present invention. Therefore, the protection scope of the present invention shall be subject to the protection scope of the claims. In addition, the specific features described in the above embodiments may be combined in any suitable manner, and in order to avoid unnecessary repetition, various possible combinations are not described further. Moreover, any combination of the various embodiments of the invention can be made without departing from the spirit of the invention, which should also be considered as disclosed herein.

Claims (4)

1. The cigar dynamic suction resistance detection method is characterized by comprising the following steps of:
step 1, placing a test cigarette in an environment with the temperature of 20+/-2 ℃ and the humidity of 62+/-5%, and carrying out balancing treatment for at least 48 hours;
step 2, setting equipment parameters according to the test sample: duration of suction: 1.5s, aspiration frequency: 40 s/bite;
step 3, selecting M samples to be fixed on a holder of the smoking machine one by one, wherein the angle formed by a longitudinal axis of the test sample and a horizontal plane is as follows: the end of the cigarette butt is lower than the other end by not more than 10 degrees and higher than the other end by not more than 5 degrees; igniting the test samples by using a hand-held electric igniter without contacting or pre-burning the test samples, wherein the ignition of each test sample reaches the combustion of the whole end face of the combustion end of the test sample;
and 4, performing axial data processing on the mouth-by-mouth dynamic suction resistance data and the burning length of the mouth-by-mouth burning cone of each test sample to obtain dynamic suction resistance data when each test sample burns with the same length.
2. The method of claim 1, wherein in step 2, the smoking machine is a limited-suction smoking machine, the total pressure drop of the flow line between the end of the cigarette butt and the suction mechanism is not more than 300PA before suction, the total volume of all suction channels is not more than 125mL, the filter disc of the catcher is replaced before each test, and the flow rate is calibrated.
3. A method for detecting cigar dynamic resistance according to claim 1, wherein in step 3, the length of the cigarette combustion cone after each suction is measured and recorded during the test; after the test sample is sucked into the N ports, when the combustion cone reaches the same position mark of each test sample butt, the suction is manually stopped, and the air is prevented from being continuously sucked through cigars; and obtaining the mouth-by-mouth dynamic suction resistance data of M test samples and the mouth-by-mouth combustion cone combustion length data of each test sample.
4. The cigar dynamic resistance detection method according to claim 1, wherein in the step 4, the axial data processing method comprises: according to the test requirement, setting a same burning length L of each opening, taking the average value (X1+X2)/2 of the nearest two dynamic resistance data (X1 and X2) at each L length to obtain the dynamic data at the current L length, and finally obtaining the dynamic data of each cigarette at each burning length L.
CN202311053123.7A 2023-08-21 2023-08-21 Cigar dynamic suction resistance detection method Pending CN117309673A (en)

Priority Applications (1)

Application Number Priority Date Filing Date Title
CN202311053123.7A CN117309673A (en) 2023-08-21 2023-08-21 Cigar dynamic suction resistance detection method

Applications Claiming Priority (1)

Application Number Priority Date Filing Date Title
CN202311053123.7A CN117309673A (en) 2023-08-21 2023-08-21 Cigar dynamic suction resistance detection method

Publications (1)

Publication Number Publication Date
CN117309673A true CN117309673A (en) 2023-12-29

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Family Applications (1)

Application Number Title Priority Date Filing Date
CN202311053123.7A Pending CN117309673A (en) 2023-08-21 2023-08-21 Cigar dynamic suction resistance detection method

Country Status (1)

Country Link
CN (1) CN117309673A (en)

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