CN117122547A - 一种不含推进剂清爽保湿防晒喷雾及其制备方法 - Google Patents
一种不含推进剂清爽保湿防晒喷雾及其制备方法 Download PDFInfo
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- CN117122547A CN117122547A CN202311252596.XA CN202311252596A CN117122547A CN 117122547 A CN117122547 A CN 117122547A CN 202311252596 A CN202311252596 A CN 202311252596A CN 117122547 A CN117122547 A CN 117122547A
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Abstract
本发明涉及日用化学品生产技术领域,具体为一种不含推进剂清爽保湿防晒喷雾及其制备方法。本发明所制备的防晒喷雾巧妙地搭配增稠剂、乳化剂、防晒剂,温和无刺激,肤感清爽不油腻,具有较好的稳定性,可以达到细密的喷雾效果,无推进剂,不易燃易爆,安全性高,还可以带上火车、高铁和飞机,异地携带方便;对紫外线UVA和UVB均有显著的的防护作用,可以满足绝大部分日常生活环境下的需求,防晒功效优异;采用普通喷雾瓶包装,包装和灌装设备要求简单,更经济适用。
Description
技术领域
本发明属于日化化妆品技术领域,具体涉及一种不含推进剂清爽保湿防晒喷雾。
背景技术
过度暴晒会损伤表皮细胞,活化酪氨酸酶,加速色素合成,破坏皮肤的保湿功能、弹力纤维,使皮肤变得干燥,产生细纹;强烈照射下,还会造成肌肤发炎、灼伤。为防止出现以上问题,人们会涂抹防晒产品、使用防晒衣等物品、食用防晒食物等来阻隔或吸收紫外线。
防晒喷雾是近年来涌现的简便型防晒产品,对比传统防晒产品,随身携带一只,可以弥补长时间在户外无法重抹防晒乳的问题,同时没有一般防晒品油腻、厚重的肤感,难以涂抹均匀、防晒效果下降等问题。目前市面上防晒喷雾是将内容物封装于具有阀门系统和一定压力的耐压容器中,使用时借助推进剂压力将内容物呈雾状物喷出,其中大部分采用丁烷、异丁烷、丙烷等易燃易爆炸挥发性推进剂,存在重大安全隐患,易造成安全事故,并且不能带上火车、高铁、飞机等交通工具,异地携带不方便;此外还有部分二元包装防晒喷雾采用安全无污染的压缩空气或氮气作为推进剂,存储在囊袋与罐子之间,挤压气囊使料体喷出,安全可异地携带,但是对设备、包装要求较高,经济适用性不强。
发明内容
为解决上述背景技术中提出问题,本发明提供一种不含推进剂清爽保湿防晒喷雾及其制备方法,本发明提供的一种不含推进剂清爽保湿防晒喷雾不仅具有良好的防晒效果、补水保湿效果,温和无刺激,肤感清爽不油腻,无推进剂,不易燃易爆,安全性高,还可以带上火车、高铁和飞机,异地携带方便,采用普通喷雾瓶包装,可以达到细密的喷雾效果,包装和灌装设备要求简单,更经济适用。
为实现上述目的,本发明提供如下技术方案。
一种不含推进剂清爽保湿防晒喷雾,所述防晒喷雾按重量百分数计,由以下组份组成:
A组分:0.35%鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、2.5%甲氧基肉桂酸乙基己酯、1.5%角鲨烷、1.5%棕榈酸乙基己酯、0.5%硅油、1.2~2%二氧化钛;
B组分:1.5%辛酸/癸酸甘油三酯、1~3%奥克三唑;
C组分:5%丙二醇、5%甘油、0.1%羟苯甲酯、0.18%C20-22醇磷酸酯、0.12%C20-22醇、0.06%三乙醇胺、余量为去离子水;
D组分:0.1%丙烯酸(酯)类/C10-30烷醇交联共聚物、0.3%菊粉月桂基氨基甲酸酯;
E组分:0.1%三乙醇胺、2.5%芦芭油、0.5%红没药醇、0.5%姜根提取物、0.54%苯氧乙醇、0.06%乙基己基甘油、0.06%香精。
一种如上所述不含推进剂清爽防晒喷雾及其制备方法,具体包括以下步骤:
S1:油锅消毒,将A组分中鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、甲氧基肉桂酸乙基己酯、角鲨烷、棕榈酸乙基己酯、硅油、钛白粉加入油锅,开启搅拌,分散均匀,启动加热,加热至温度为80~83℃;
S2:另准备容器将B组分辛酸/癸酸甘油三酯、奥克三唑加入,搅拌加热至温度为80~83℃,溶解完全;
S3:将溶解好的步骤2中物料加入步骤1油锅中;
S4:将C组分丙二醇、甘油、羟苯甲酯、C20-22醇磷酸酯、C20-22醇、三乙醇胺、去离子水加入乳化锅,启动搅拌,搅拌速度为15-20Hz,启动加热,加热至温度为80~85℃,搅拌至物料完全溶解;
S5:将D组分丙烯酸(酯)类/C10-30烷醇交联共聚物、菊粉月桂基氨基甲酸酯搅拌加入至步骤4物料中,启动搅拌,搅拌速度为15-20Hz,抽真空,真空度控制在-0.03~-0.06Mpa,启动均质,均质速度为50Hz,均质时间为3-5min至物料完全溶解;
S6:抽真空,真空度控制在-0.03~-0.06Mpa,启动搅拌,搅拌速度为20-30Hz,将步骤3中溶解完全的料体从油锅内缓慢抽入到乳化锅内,启动均质,均质速度为50Hz,均质时间为5-8min;
S7:启动降温,降温至43~47℃,将E组分三乙醇胺、芦芭油、红没药醇、姜根提取物、苯氧乙醇、乙基己基甘油、香精加入到乳化锅,抽真空,真空度控制在-0.03~-0.06Mpa,启动搅拌,搅拌速度为15-25Hz,启动均质,均质速度为50Hz,均质时间为2min,均质停止后,继续搅拌15min;
S8:性能检测,将混合好的物料取样检测,从外观上判断其均匀度、光亮度,并涂抹感受细腻程度,然后做理化检测和稳定性测试,合格后方可进行批量生产;
S9:过滤出料,将检测合格后的物料进行过滤,过滤后得到半成品,然后放置静置间备用。
本发明采用物理防晒剂和化学防晒剂相互配合,全波段化学防晒剂奥克三唑与纳米二氧化钛复配有效提高防晒喷雾气雾剂的防晒性能,并且纳米二氧化钛能够均匀喷洒,避免防晒堆积发白,红没药醇、姜根提取物能够有效抑制化学防晒剂的刺激性,避免过敏等副作用,芦芭油增强肤感和润滑性,具有强大的锁水能力,还能稳定乳液。
本发明采用丙烯酸(酯)类/C10-30烷醇交联共聚物作为增稠剂,对粉体有良好的悬浮力,提高配方稳定性,清爽不黏腻,剪切变稀,经喷雾瓶可形成细密喷雾。
本发明采用鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、C20-22醇磷酸酯、C20-22醇、菊粉月桂基氨基甲酸酯构成乳化剂,在油水界面形成双电层,利用电荷作用使得液滴之间产生相互排斥,提高乳液乳化效果和乳化稳定性。
与现有技术相比,本发明的有益效果是:
(1)本发明提供一种不含推进剂清爽保湿防晒喷雾,对紫外线UVA和UVB均有显著的的防护作用,可以满足绝大部分日常生活环境下的需求,防晒功效优异;
(2)本发明一种不含推进剂清爽保湿防晒喷雾具有优异的补水功效,温和无刺激,肤感清爽不油腻,具有较好的稳定性;
(3)本发明提供的一种不含推进剂清爽保湿防晒喷雾,保证了轻柔细密的雾化喷出状态,无推进剂,不易燃易爆,安全性高,还可以带上火车、高铁和飞机,异地携带方便;
(4)本发明提供的一种不含推进剂清爽保湿防晒喷雾,采用普通喷雾瓶包装,可以达到细密的喷雾效果,包装和灌装设备要求简单,更经济适用。
具体实施方式
本发明提供一种不含推进剂清爽保湿防晒喷雾及其制备方法,为使本发明的目的、技术方案及效果更加清楚、明确,以下对本发明进一步详细说明。应当理解,此处所描述的具体实施例仅仅用以解释本发明,并不用于限定本发明。
实施例一
一种不含推进剂清爽保湿防晒喷雾,防晒喷雾按重量百分数计,由以下组份组成:
A组分:0.35%鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、2.5%甲氧基肉桂酸乙基己酯、1.5%角鲨烷、1.5%棕榈酸乙基己酯、0.5%硅油、1.2%二氧化钛。
B组分:1.5%辛酸/癸酸甘油三酯、1%奥克三唑。
C组分:5%丙二醇、5%甘油、0.1%羟苯甲酯、0.18%C20-22醇磷酸酯、0.12%C20-22醇、0.06%三乙醇胺、余量为去离子水。
D组分:0.1%丙烯酸(酯)类/C10-30烷醇交联共聚物、0.3%菊粉月桂基氨基甲酸酯。
E组分:0.1%三乙醇胺、2.5%芦芭油、0.5%红没药醇、0.5%姜根提取物、0.54%苯氧乙醇、0.06%乙基己基甘油、0.06%香精。
一种不含推进剂清爽保湿防晒喷雾的制备工艺,包括以下步骤:
S1:油锅消毒,将A组分中鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、甲氧基肉桂酸乙基己酯、角鲨烷、棕榈酸乙基己酯、硅油、钛白粉加入油锅,开启搅拌,分散均匀,启动加热,加热至温度为80~83℃;
S2:另准备容器将B组分辛酸/癸酸甘油三酯、奥克三唑加入,搅拌加热至温度为80℃,溶解完全;
S3:将溶解好的步骤2中物料加入步骤1油锅中;
S4:将C组分丙二醇、甘油、羟苯甲酯、C20-22醇磷酸酯、C20-22醇、三乙醇胺、去离子水加入乳化锅,启动搅拌,搅拌速度为20Hz,启动加热,加热至温度为80℃,搅拌至物料完全溶解;
S5:将D组分丙烯酸(酯)类/C10-30烷醇交联共聚物、菊粉月桂基氨基甲酸酯搅拌加入至步骤4物料中,启动搅拌,搅拌速度为20Hz,抽真空,真空度控制在-0.03~-0.06Mpa,启动均质,均质速度为50Hz,均质时间为3min至物料完全溶解;
S6:抽真空,真空度控制在-0.03~-0.06Mpa,启动搅拌,搅拌速度为30Hz,将步骤3中溶解完全的料体从油锅内缓慢抽入到乳化锅内,启动均质,均质速度为50Hz,均质时间为5min;
S7:启动降温,降温至43~47℃,将E组分三乙醇胺、芦芭油、红没药醇、姜根提取物、苯氧乙醇、乙基己基甘油、香精加入到乳化锅,抽真空,真空度控制在-0.03~-0.06Mpa,启动搅拌,搅拌速度为25Hz,启动均质,均质速度为50Hz,均质时间为2min,均质停止后,继续搅拌15min;
S8:性能检测,将混合好的物料取样检测,从外观上判断其均匀度、光亮度,并涂抹感受细腻程度,然后做理化检测和稳定性测试,合格后方可进行批量生产;
S9:过滤出料,将检测合格后的物料进行过滤,过滤后得到半成品,然后放置静置间备用。
实施例二
本实施例中防晒喷雾的制备工艺与实施例1相同,不同之处在于各原料的配比略有不同,具体如下:
一种高含量淀粉柔润温和洁面乳,洁面乳按重量百分数计,由以下组份组成:
A组分:0.35%鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、2.5%甲氧基肉桂酸乙基己酯、1.5%角鲨烷、1.5%棕榈酸乙基己酯、0.5%硅油、2%二氧化钛。
B组分:1.5%辛酸/癸酸甘油三酯、3%奥克三唑。
C组分:5%丙二醇、5%甘油、0.1%羟苯甲酯、0.18%C20-22醇磷酸酯、0.12%C20-22醇、0.06%三乙醇胺、余量为去离子水。
D组分:0.1%丙烯酸(酯)类/C10-30烷醇交联共聚物、0.3%菊粉月桂基氨基甲酸酯。
E组分:0.1%三乙醇胺、2.5%芦芭油、0.5%红没药醇、0.5%姜根提取物、0.54%苯氧乙醇、0.06%乙基己基甘油、0.06%香精。
对比例1:与实施例1的不同之处在于,本实施例中丙烯酸(酯)类/C10-30烷醇交联共聚物0.06%、E相三乙醇胺0.06%;
对比例2:与实施例1的不同之处在于,本实施例中采用等量的聚丙烯酰胺(和)C13-14异链烷烃(和)月桂醇聚醚-7替换菊粉月桂基氨基甲酸酯;
对比例3:与实施例1的不同之处在于,本实施例中二氧化钛2.5%;
对比例4:与实施例1的不同之处在于,本实施例中奥克三唑4%;
对比例5:与实施例1配方相同,不同之处在于,本实施例中C、D相同时加入主锅分散,再加入E相三乙醇胺,搅拌速度20Hz,启动加热,加热至温度为80℃,将A、B相慢慢抽入主锅,启动均质,均质速度为50Hz,均质时间为5min,然后降温至43℃,加入剩余E相成分。
性能测试:分别对实施例1~2及对比例1~5制备的防晒喷雾进行如下性能检测:
稳定性测试:取实施例1~2、对比例1~5样品静置于-10℃和45℃的环境中,每周取出观察是否出现异常,试验期为1个月,试验期结束后,取出试验样品并恢复至室温(25±2℃),观察试验样品的外观,并记录;取实施例1~2、对比例1~5样品,用离心管称量相同物料量放置于离心机,设置转速2000r/min,时间30min,启动离心机,结束后取出离心管,观察外观,并记录,具体情况如下表1所示;
组别 | 离心测试外观 | -10℃环境试验外观 | 45℃环境试验外观 |
实施例1 | 均匀未分层 | 均匀未分层 | 均匀未分层 |
实施例2 | 均匀未分层 | 均匀未分层 | 均匀未分层 |
对比例1 | 分层明显 | 分层明显 | 分层明显 |
对比例2 | 均匀未分层 | 均匀未分层 | 均匀未分层 |
对比例3 | 均匀未分层 | 均匀未分层 | 均匀未分层 |
对比例4 | 均匀未分层 | 均匀未分层 | 均匀未分层 |
对比例5 | 分层明显 | 均匀未分层 | 分层明显 |
结论:从表1可以看出;7个样品中对比例1、对比例5样品外观均有分层,增稠剂的添加量和工艺操作顺序会影响产品的稳定性。
刺激性测试:按照《SN/T 2329-2009化妆品眼刺激性/腐蚀性的鸡胚绒毛尿囊试验》对实施例1~2及对比例2~4样品进行刺激性测试,所得测试数据记录于表3,验评判标准见表2:
终点评分 | 刺激性分类 |
ES≤12 | 无/轻刺激性 |
12<ES<16 | 中度刺激性 |
ES≥16 | 强刺激性/腐蚀性 |
表3刺激性测试结果:
检测项目 | 实施例1 | 实施例2 | 对比例2 | 对比例3 | 对比例4 |
ES总和 | 1 | 2 | 2 | 1 | 5 |
结论:从表3可以看出;5个样品都显示为无/轻刺激性,但对比例4样品的ES总和明显高于其他样品,对比例4样品使用较多防晒剂,而防晒产品中的防晒剂,作为限量物质,本身是具有一定的刺激性的,所以随着防晒剂量增加,刺激性增加。
清爽、保湿效果测试:随机选取40名年龄为20~35岁的受试者,其中男性20名,女性20名;并将之随机等分为4组,每组各10人;并分别将之标记为实施例1~2及对比例2~3;然后分别让不同组的受试者使用与之组别相匹配的实施例1~2及对比例2~3所制备的防晒喷雾,使用40min后,使用测试仪Sebumeter和Corneometer CM825分别检测使用防晒喷雾前后的皮肤油脂含量和皮肤含水量,并记录每组志愿者皮肤水分、油分的平均值所得数据记录于下表4:
结论:从表4可以看出,实施例1~2和对比例2~3制得的防晒喷雾使用后皮肤的含水量均较使用前皮肤的含水量增加,含油量变化不明显,具有良好的保湿功效,肤感清爽,其中实施例1组皮肤含水量增加最多,含油量增加最低。
喷雾雾状效果测试:随机选取40名年龄为20~35岁的受试者,其中男性20名,女性20名;并将之随机等分为4组,每组各10人;并分别将之标记为实施例1~2及对比例2~3;然后分别让不同组的受试者使用与之组别相匹配的实施例1~2及对比例2~3所制备的防晒喷雾,让每组受试者使用相应组别防晒喷雾进行喷雾雾化效果测试,所得测试数据记录于表5:
结论:从表5可以看出,实施例1~2和对比例2~3制得的防晒喷雾,对比例2~3的喷雾效果不理想,乳化增稠剂的种类和二氧化钛的量会影响喷雾效果。
5、防晒效果测试:将实施例1~2及对比例2~4样品以2mg/cm2涂覆密度均匀涂敷于PMMA板上,使用SPF-290S紫外分光光度计进行扫描测试,所得测试数据记录于表6:
测试项目 | 实施例1 | 实施例2 |
SPF值 | 47 | 54 |
通过对比及分析相关数据可知,相比较于对比例,本发明所制备的防晒喷雾使用丙烯酸(酯)类/C10-30烷醇交联共聚物、鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、C20-22醇磷酸酯、C20-22醇、菊粉月桂基氨基甲酸酯作为增稠剂、乳化剂,温和无刺激,肤感清爽不油腻,具有较好的稳定性,可以达到细密的喷雾效果,无推进剂,不易燃易爆,安全性高,还可以带上火车、高铁和飞机,异地携带方便;此外,本发明所制备的防晒喷雾对紫外线UVA和UVB均有显著的的防护作用,可以满足绝大部分日常生活环境下的需求,防晒功效优,采用普通喷雾瓶包装,包装和灌装设备要求简单,更经济适用。
在本说明书的描述中,参考术语“一个实施例”、“示例”、“具体示例”等的描述意指结合该实施例或示例描述的具体特征、结构、材料或者特点包含于本发明的至少一个实施例或示例中。在本说明书中,对上述术语的示意性表述不一定指的是相同的实施例或示例。而且,描述的具体特征、结构、材料或者特点可以在任何的一个或多个实施例或示例中以合适的方式结合。
以上公开的本发明优选实施例只是用于帮助阐述本发明。优选实施例并没有详尽叙述所有的细节,也不限制该发明仅为所述的具体实施方式。显然,根据本说明书的内容,可作很多的修改和变化。本说明书选取并具体描述这些实施例,是为了更好地解释本发明的原理和实际应用,从而使所属技术领域技术人员能很好地理解和利用本发明。本发明仅受权利要求书及其全部范围和等效物的限制。
Claims (2)
1.一种不含推进剂清爽保湿防晒喷雾,其特征在于,所述防晒喷雾按重量百分数计,由以下组份组成:
A组分:0.35%鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、2.5%甲氧基肉桂酸乙基己酯、1.5%角鲨烷、1.5%棕榈酸乙基己酯、0.5%硅油、1.2~2%二氧化钛;
B组分:1.5%辛酸/癸酸甘油三酯、1~3%奥克三唑;
C组分:5%丙二醇、5%甘油、0.1%羟苯甲酯、0.18%C20-22醇磷酸酯、0.12%C20-22醇、0.06%三乙醇胺、余量为去离子水;
D组分:0.1%丙烯酸(酯)类/C10-30烷醇交联共聚物、0.3%菊粉月桂基氨基甲酸酯;
E组分:0.1%三乙醇胺、2.5%芦芭油、0.5%红没药醇、0.5%姜根提取物、0.54%苯氧乙醇、0.06%乙基己基甘油、0.06%香精。
2.如权利要求1所述的一种不含推进剂清爽防晒喷雾制备方法,其特征在于,具体包括以下步骤:
S1:油锅消毒,将A组分中鲸蜡基聚乙二醇/聚丙二醇-10/1二甲基硅氧烷、甲氧基肉桂酸乙基己酯、角鲨烷、棕榈酸乙基己酯、硅油、钛白粉加入油锅,开启搅拌,分散均匀,启动加热,加热至温度为80~83℃;
S2:另准备容器将B组分辛酸/癸酸甘油三酯、奥克三唑加入,搅拌加热至温度为80~83℃,溶解完全;
S3:将溶解好的步骤2中物料加入步骤1油锅中;
S4:将C组分丙二醇、甘油、羟苯甲酯、C20-22醇磷酸酯、C20-22醇、三乙醇胺、去离子水加入乳化锅,启动搅拌,搅拌速度为15-20Hz,启动加热,加热至温度为80~85℃,搅拌至物料完全溶解;
S5:将D组分丙烯酸(酯)类/C10-30烷醇交联共聚物、菊粉月桂基氨基甲酸酯搅拌加入至步骤4物料中,启动搅拌,搅拌速度为15-20Hz,抽真空,真空度控制在-0.03~-0.06Mpa,启动均质,均质速度为50Hz,均质时间为3-5min至物料完全溶解;
S6:抽真空,真空度控制在-0.03~-0.06Mpa,启动搅拌,搅拌速度为20-30Hz,将步骤3中溶解完全的料体从油锅内缓慢抽入到乳化锅内,启动均质,均质速度为50Hz,均质时间为5-8min;
S7:启动降温,降温至43~47℃,将E组分三乙醇胺、芦芭油、红没药醇、姜根提取物、苯氧乙醇、乙基己基甘油、香精加入到乳化锅,抽真空,真空度控制在-0.03~-0.06Mpa,启动搅拌,搅拌速度为15-25Hz,启动均质,均质速度为50Hz,均质时间为2min,均质停止后,继续搅拌15min;
S8:性能检测,将混合好的物料取样检测,从外观上判断其均匀度、光亮度,并涂抹感受细腻程度,然后做理化检测和稳定性测试,合格后方可进行批量生产;
S9:过滤出料,将检测合格后的物料进行过滤,过滤后得到半成品,然后放置静置间备用。
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